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11. 发明授权

US5427835A Sulfopolymer/vanadium oxide antistatic compositions 失效
标题翻译：磺化聚合物/氧化钒抗静电组合物
公开(公告)号：US5427835A
公开(公告)日：1995-06-27
申请号：US893279
申请日：1992-06-04
申请人： Eric D. Morrison , David R. Boston , Steven T. Hedrick , William L. Kausch , Wayne K. Larson , Simon S. Fung
发明人： Eric D. Morrison , David R. Boston , Steven T. Hedrick , William L. Kausch , Wayne K. Larson , Simon S. Fung
IPC分类号： B32B9/00 , B32B27/12 , B32B27/18 , C08J7/04 , C09J7/02 , C09K3/16 , B32B33/00
CPC分类号： C09J7/02 , C09J7/0207 , C09K3/16 , Y10S428/90 , Y10S524/91 , Y10S524/911 , Y10S524/912 , Y10T428/23986 , Y10T428/31504 , Y10T428/31507 , Y10T428/31678 , Y10T428/31681 , Y10T428/31786 , Y10T428/3179 , Y10T442/2467
摘要： Aqueous-based mixtures comprising colloidal vanadium oxide and a dispersed sulfonated polymer impart antistatic properties to coatings on a substrate and to self-supporting articles. The preferred colloidal vanadium oxide is alkoxide derived and provides mixed valence vanadium oxide wherein the vanadium ions are typically +4 and +5. Preferred sulfopolymers include sulfopolyesters, sulfopolyurethanes, sulfopolyurethanes/ureas, sulfopolyester polyols, and sulfopolyols. Antistatic composite structures comprising colloidal vanadium oxide and a sulfopolymer are also disclosed.
摘要翻译：包含胶体氧化钒和分散的磺化聚合物的水基混合物赋予基材上的涂层和自支撑制品的抗静电性能。优选的胶态钒氧化物是衍生的醇盐，并提供混合价态的钒氧化物，其中钒离子通常为+4和+5。优选的磺基聚合物包括磺基聚酯，磺基聚氨酯，磺基聚氨酯/脲，磺基聚酯多元醇和磺基多元醇。还公开了包含胶体氧化钒和磺基聚合物的抗静电复合结构。

12. 发明授权

US4855384A Sulfonate-containing photopolymer systems 失效
标题翻译：含磺酸盐的光聚合物体系
公开(公告)号：US4855384A
公开(公告)日：1989-08-08
申请号：US156303
申请日：1988-02-12
申请人： Wayne K. Larson
发明人： Wayne K. Larson
IPC分类号： C08G18/46 , C08G18/60 , C08G18/67 , C08G18/81 , C08G63/688 , C08G69/48 , C08L67/06 , C09D167/06
CPC分类号： C09D167/06 , C08G18/4676 , C08G18/603 , C08G18/671 , C08G18/673 , C08G18/8108 , C08G18/8175 , C08G63/6884 , C08G69/48 , C08L67/06 , Y10T428/31551 , Y10T428/31605
摘要： An isocyanate-terminated sulfocompound is the reaction product of a polyisocyanate and a sulfopolyol or sulfopolyamine which is the reaction product of one mole of a sulfodicarboxylic acid and about two moles of an aliphatic polyol or polyamine having two or more hydroxyl or amino groups attached to a linear chain and having a molecular weight of up to 2000. The sulfocompound can be reacted with ethylenically-unsaturated alcohols, water, polyamines, or polyols, to give ethylenically-unsaturated sulfocompounds, sulfopolyureas or sulfopolyurethanes.
摘要翻译：异氰酸酯封端的磺基化合物是多异氰酸酯和磺基多元醇或磺胺多胺的反应产物，其是1摩尔磺基二羧酸和约2摩尔脂族多元醇或具有两个或更多个羟基或氨基的多胺的反应产物，线性链并具有高达2000的分子量。磺基化合物可以与烯键式不饱和醇，水，多胺或多元醇反应，得到烯键式不饱和的磺基化合物，磺基聚合物或磺基多氨基甲酸酯。

13. 发明授权

US4746717A Isocyanate-terminated sulfocompounds 失效
标题翻译：异氰酸酯封端的磺基化合物
公开(公告)号：US4746717A
公开(公告)日：1988-05-24
申请号：US9616
申请日：1987-01-22
申请人： Wayne K. Larson
发明人： Wayne K. Larson
IPC分类号： C08G18/46 , C08G18/60 , C08G18/67 , C08G18/81 , C08G63/688 , C08G69/48 , C08L67/06 , C09D167/06 , C08G18/32
CPC分类号： C09D167/06 , C08G18/4676 , C08G18/603 , C08G18/671 , C08G18/673 , C08G18/8108 , C08G18/8175 , C08G63/6884 , C08G69/48 , C08L67/06
摘要： An isocyanate-terminated sulfocompound is the reaction product of a polyisocyanate and a sulfopolyol or sulfopolyamine which is the reaction product of one mole of a sulfodicarboxylic acid and about two moles of an aliphatic polyol or polyamine having two or more hydroxyl or amino groups attached to a linear chain and having a molecular weight of up to 2000. The sulfocompound can be reacted with ethylenically-unsaturated alcohols, water, polyamines, or polyols, to give ethylenically-unsaturated sulfocompounds, sulfopolyureas or sulfopolyurethanes.
摘要翻译：异氰酸酯封端的磺基化合物是多异氰酸酯和磺基多元醇或磺胺多胺的反应产物，其是1摩尔磺基二羧酸和约2摩尔脂族多元醇或具有两个或更多个羟基或氨基的多胺的反应产物，线性链并具有高达2000的分子量。磺基化合物可以与烯键式不饱和醇，水，多胺或多元醇反应，得到烯键式不饱和的磺基化合物，磺基聚合物或磺基多氨基甲酸酯。

14. 发明授权

US4667661A Curable resin coated sheet having reduced tack 失效
公开(公告)号：US4667661A
公开(公告)日：1987-05-26
申请号：US784671
申请日：1985-10-04
申请人： Matthew T. Scholz , Dennis C. Bartizal , Katherine E. Reed , Wayne K. Larson , Dean A. Ersfeld , Timothy C. Sandvig , Richard S. Buckanin
发明人： Matthew T. Scholz , Dennis C. Bartizal , Katherine E. Reed , Wayne K. Larson , Dean A. Ersfeld , Timothy C. Sandvig , Richard S. Buckanin
IPC分类号： A61L15/07 , A61F13/00 , A61L15/12 , A61L15/48 , A61F5/04 , A61F13/04 , B32B17/04
CPC分类号： A61L15/48 , A61L15/125 , Y10S428/913 , Y10T29/49732 , Y10T428/1314 , Y10T428/31551 , Y10T428/31598 , Y10T428/31601 , Y10T442/2311 , Y10T442/2328 , Y10T442/2992
摘要： A curable resin coated sheet useful as an orthopedic bandage which has reduced tack is provided. The resin coated sheet is pre-lubricated with a lubricant which is (a) bonded to the resin, (b) added to the resin or applied to the surface of the coated sheet, or (c) a combination of (a) and (b). The lubricant is present in an amount to reduce the kinetic coefficient of friction of a surface of the coated sheet to less than 1.2.

15. 发明授权

US4558149A Sulfonate-containing photopolymer systems 失效
标题翻译：含磺酸盐的光聚合物体系
公开(公告)号：US4558149A
公开(公告)日：1985-12-10
申请号：US562459
申请日：1983-12-16
申请人： Wayne K. Larson
发明人： Wayne K. Larson
IPC分类号： C08F2/00 , C08F2/48 , C08F290/00 , C08F299/00 , C08F299/06 , C08G18/00 , C08G18/46 , C08G18/60 , C08G18/67 , C08G18/68 , C08G18/81 , C08G63/00 , C08G63/66 , C08G63/68 , C08G63/685 , C08G63/688 , C08G69/48 , C08L67/06 , C09D167/06 , C07C143/525
CPC分类号： C09D167/06 , C08G18/4676 , C08G18/603 , C08G18/671 , C08G18/673 , C08G18/8108 , C08G18/8175 , C08G63/6884 , C08G69/48 , C08L67/06 , Y10T428/31551 , Y10T428/31565
摘要： A low molecular weight, film-forming, polymerizable, ethylenically-unsaturated compound is water- and organic solvent-soluble (i.e., soluble in both water and organic solvents) but is readily converted on exposure to actinic radiation to a polymer that is solvent-insoluble (i.e., not soluble in water, organic solvents, or mixtures of water and organic solvents) and, in certain examples, is hydrophobic. The compound comprises the ethylenically-unsaturated derivative (i.e., an ester or an amide) of a sulfopolyol or sulfopolyamine having an ethylenic unsaturated functionality of 2 to 18 and an equivalent weight per ethylenic unsaturated functionality of less than 2500.
摘要翻译：低分子量，成膜，可聚合的烯属不饱和化合物是水溶性和有机溶剂可溶的（即，可溶于水和有机溶剂），但是容易地在曝露于光化辐射下转化为溶剂型聚合物，不溶于水（即不溶于水，有机溶剂或水和有机溶剂的混合物），在某些实例中是疏水性的。该化合物包含具有2至18的烯属不饱和官能度和小于2500的每个烯属不饱和官能团的当量的磺基多元醇或磺胺多胺的烯键式不饱和衍生物（即酯或酰胺）。

16. 发明授权

US4052368A Water-dispellable hot melt polyester adhesives 失效
标题翻译：水不溶性热熔胶聚酯胶粘剂
公开(公告)号：US4052368A
公开(公告)日：1977-10-04
申请号：US697968
申请日：1976-06-21
申请人： Wayne K. Larson
发明人： Wayne K. Larson
IPC分类号： C08G63/00 , C08G63/16 , C08G63/688 , C08L67/00 , C08L67/02 , C09J7/00 , C09J7/02 , C09J167/00 , C08G63/68
CPC分类号： C09J7/0207 , C08G63/688 , C09J167/00 , C09J7/00 , Y10T428/3179
摘要： Water-dispellable, optionally pressure-sensitive hot melt resins having superior heat-aging properties are made by reacting (1) diols, of which at least 90% are polycaprolactonediol and/or monoalkylene diols, with (2) dicarboxylic acids, of which up to 95% are aliphatic, 5-25% are aromatic and have a magnesium or alkali metal sulfonate group attached to the ring, and the balance are non-sulfonated aromatic. These resins, which find use as hot melt adhesives for book binding and other purposes, can be readily dissolved or dispersed in a paper beater during a repulping operation. The product can be wound upon itself and supplied in roll form, optionally reinforced by a fibrous membrane.

17. 发明授权

US5929160A Method for reducing water uptake in silyl terminated sulfopoly(ester-urethanes) 失效
标题翻译：减少甲硅烷基封端的磺基聚合物（酯 - 氨基甲酸酯）吸水率的方法
公开(公告)号：US5929160A
公开(公告)日：1999-07-27
申请号：US937487
申请日：1997-09-25
申请人： Larry R. Krepski , Steven M. Heilmann , Daniel E. Mickus , Wayne K. Larson
发明人： Larry R. Krepski , Steven M. Heilmann , Daniel E. Mickus , Wayne K. Larson
IPC分类号： C08L75/06 , C08G18/08 , C08G18/10 , C08G18/46 , C08G18/71 , C08G18/83 , C08J3/00 , C08K3/20 , C08L75/00 , C08L83/00
CPC分类号： C08G18/4676 , C08G18/0828 , C08G18/10
摘要： A method of decreasing the water uptake in a sulfopoly(ester-urethane) by preparing said sulfopoly(ester-urethane) from a chain extended sulfopolyester polyol which itself has been prepared in a two-step method, said sulfopoly(ester-urethane) comprising in its backbone at least one non-terminal arylene or alkylene group comprising a pendant sulfonic acid group or salt thereof, said sulfonic acid group or salt thereof having the formula ##STR1## wherein R is a trivalent aliphatic or aromatic group and M is a cation, said sulfonic acid group or salt thereof being bonded directly through said aliphatic or aromatic group to ester groups, the polymer of said sulfo(polyester-urethane) being terminated by at least one hydrolyzable silyl group,said two-step method for preparing said chain extended sulfopolyester polyol comprising the steps of:a) reacting a sulfopolycarboxylic acid or ester with a polyol to produce a sulfopolyester polyol,b) chain extending said sulfopolyester polyol by an esterification reaction with a lower aliphatic lactone to produce a chain extended sulfopolyester polyol, andsaid chain extended sulfopolyester polyol then, (1) in one embodiment, being reacted with a stoichiometric excess of a polyisocyanate and at least one of a polyol, polyamine, and polythiol to produce an isocyanate-terminated sulfo(polyester-urethane), which is then reacted with a nucleophilic, hydrolyzable silane or (2) in a second embodiment, being reacted with a polyisocyanate and a stoichiometric excess of at least one of a polyol, polyamine, and polythiol to produce a hydroxyl-, amino-, or mercapto-terminated sulfo(polyester-urethane) which is then reacted with an electrophilic hydrolyzable silane to produce said sulfopoly(ester-urethane), which when dried has decreased water uptake.
摘要翻译：所述磺基聚（酯 - 氨基甲酸酯）包括通过由两步法制备的扩链磺基聚酯多元醇制备所述锍聚（酯 - 氨基甲酸酯）来降低锍聚（酯 - 氨基甲酸酯）中的吸水率的方法，在其主链中至少有一个非末端亚芳基或含有磺酸侧基的亚烷基或其盐，所述磺酸基或其盐具有下式：其中R是三价脂族或芳族基，M是阳离子，所述磺酸所述磺基（聚酯 - 氨基甲酸酯）的聚合物被至少一个可水解的甲硅烷基封端，所述制备所述链延长磺基聚酯多元醇的两步法包括以下步骤：a）使磺基多羧酸或酯与多元醇反应以产生磺基聚酯多元醇，b）通过酯化链延伸所述磺基聚酯多元醇与低级脂肪族内酯反应以产生扩链磺基聚酯多元醇，并且所述链延长磺基聚酯多元醇然后，（1）在一个实施方案中，与化学计量过量的多异氰酸酯和多元醇，多胺和多异硫氰酸酯以产生异氰酸酯封端的磺基（聚酯 - 氨基甲酸酯），然后与亲核的可水解的硅烷反应，或（2）在第二个实施方案中与多异氰酸酯和化学计量过量的多元醇，多胺和多硫醇，以产生羟基，氨基或巯基封端的磺基（聚酯 - 氨基甲酸酯），然后与亲电的可水解硅烷反应产生所述磺化聚（酯 - 氨基甲酸酯），当干燥时，其吸水量降低。

18. 发明授权

US5756633A Silyl terminated sulfopoly(ester-urethane) compositions 失效
标题翻译：甲硅烷基封端的磺基（酯 - 氨基甲酸酯）组合物
公开(公告)号：US5756633A
公开(公告)日：1998-05-26
申请号：US609193
申请日：1996-03-01
申请人： Wayne K. Larson
发明人： Wayne K. Larson
IPC分类号： C08G18/08 , C08G18/10 , C08G18/46 , C08G18/71 , C08G18/83 , C08G18/61
CPC分类号： C08G18/832 , C08G18/0828 , C08G18/10 , C08G18/4676 , C08G18/718 , Y10T428/31551 , Y10T428/31565 , Y10T428/31591 , Y10T428/31601 , Y10T428/31605
摘要： Water-dispersible sulfopoly(ester-urethane) compositions which comprise, in their backbone, at least one arylene or alkylene sulfonic acid group or a salt thereof, the polymer being terminated by at least one hydrolyzable silyl group. The compositions of the invention preferably have a sulfonate equivalent weight of about 500 to about 12,000 g/equivalent and a number average molecular weight less than 50,000. Compositions of the invention have utility as durable treatments such as low surface energy coatings that exhibit release towards adhesive materials, grease, and oils.
摘要翻译：在其主链中包含至少一个亚芳基或亚烷基磺酸基团或其盐的水分散性磺基聚（酯 - 氨基甲酸酯）组合物，所述聚合物被至少一个可水解甲硅烷基封端。本发明的组合物优选具有约500至约12,000g /当量的磺酸盐当量重量和小于50,000的数均分子量。本发明的组合物可用作耐久处理，例如表现出对粘合剂材料，油脂和油的释放的低表面能涂料。

19. 发明授权

US4738992A Hydrophilic polyurethane/polyurea sponge 失效
标题翻译：亲水性聚氨酯/聚脲海绵
公开(公告)号：US4738992A
公开(公告)日：1988-04-19
申请号：US875453
申请日：1986-06-17
申请人： Wayne K. Larson , Steven T. Hedrick
发明人： Wayne K. Larson , Steven T. Hedrick
IPC分类号： C08G18/08 , C08G18/14
CPC分类号： C08G18/0828 , C08G2101/0008 , C08G2101/0083 , Y10T428/249958 , Y10T442/652
摘要： A water-absorbing sponge comprises at least one of a pendent sulfo-group containing polyurea and polyurethane, the polymer containing at least one sulfonate equivalent per 20,000 molecular weight units.
摘要翻译：吸水海绵包含至少一种含侧基磺基的聚脲和聚氨酯，所述聚合物每20,000个分子量单元含有至少一个磺酸盐当量。

20. 发明授权

US4638017A Hydrophilic polyurethane/polyurea sponge 失效
标题翻译：亲水性聚氨酯/聚脲海绵
公开(公告)号：US4638017A
公开(公告)日：1987-01-20
申请号：US806758
申请日：1985-12-09
申请人： Wayne K. Larson , Steven T. Hedrick
发明人： Wayne K. Larson , Steven T. Hedrick
IPC分类号： C08G18/65 , C08G18/08 , C08G18/30 , C08G18/32 , C08G18/77 , C08J9/04 , C08G18/14
CPC分类号： C08G18/0828 , C08G2101/0008 , C08G2101/0083
摘要： A water-absorbing sponge comprises at least one of a sulfo- group containing polyurea and polyurethane, the polymer containing at least one sulfonate equivalent per 20,000 molecular weight units.
摘要翻译：吸水海绵包括含有磺基的聚脲和聚氨酯中的至少一种，所述聚合物每20,000个分子量单元含有至少一个磺酸盐当量。

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