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    • 122. 发明授权
    • Method of controlling the pressure of a continuous digester using an
extraction-dilution
    • 使用萃取 - 稀释法控制连续蒸煮器的压力的方法
    • US5824188A
    • 1998-10-20
    • US712977
    • 1996-09-12
    • J. Robert ProughBruno S. MarcocciaRichard O. LaaksoCarl L. Luhrmann
    • J. Robert ProughBruno S. MarcocciaRichard O. LaaksoCarl L. Luhrmann
    • D21C3/02D21C3/22D21C3/24D21C7/00D21C7/12D21C7/14D21C9/02D21C11/00D21C11/04
    • D21C3/224D21C11/0021D21C11/04D21C3/02D21C3/24D21C7/00D21C7/12D21C7/14D21C9/02
    • The sulfide ion concentration and sulfidity of kraft cooking liquor during kraft cooking of cellulose pulp is selectively increased. After treatment in a first treatment zone in which impregnation or kraft cooking takes place using a kraft cooking liquor having a first sulfide ion concentration and sulfidity, black liquor is extracted from the material, liquid is withdrawn from the material and dilution liquid is added to the withdrawn liquid and the withdrawn liquid with dilution liquid is reintroduced. In a second treatment zone after the first zone a second kraft cooking liquor is introduced having a second sulfide ion concentration and sulfidity greater than the first sulfide ion concentration and sulfidity (typically by about 20-50%), including by manipulating controlling the flow rate of extraction and the flow rates of withdrawal of liquid and addition of dilution liquid. The pressure of the continuous digester is controlled in a unique manner that avoids disruptions to the column of pulp continuously moving downwardly in the digester, anywhere in the digester, but particularly avoids non-uniform, unstable material in the countercurrent washing zone. The pressure is controlled by withdrawing liquid from, and introducing liquor into, the digester at at least one additional extraction-dilution loop aside from the main extraction of the digester and the wash dilution liquid introduction mechanism below the wash screens. Pressure can also be maintained (e.g. at about 130-170 psi) by also controlling the amount of wash dilution liquor, and by varying the extraction flow.
    • 纤维素纸浆硫酸盐蒸煮时硫酸盐蒸煮液的硫化物离子浓度和硫化物有选择地增加。 在使用具有第一硫化物离子浓度和硫化物的硫酸盐蒸煮液进行浸渍或硫酸盐蒸煮的第一处理区域中处理之后,从该材料中提取黑液,从该物质中取出液体并将稀释液加入到 取出的液体和用稀释液体排出的液体被重新引入。 在第一区域之后的第二处理区域中,引入第二硫酸盐蒸煮液,其具有大于第一硫化物离子浓度和硫化物浓度的硫化物的第二硫离子浓度和硫化物(通常为约20-50%),包括通过控制流速 的提取液和液体的提取流量以及稀释液的添加量。 以独特的方式控制连续蒸煮器的压力,避免在蒸煮器中的任何地方在蒸煮器中连续向下移动的纸浆柱的中断,但是特别地避免了逆流洗涤区域中不均匀的不稳定的材料。 除了从洗涤屏幕下面的蒸煮器和洗涤稀释液引入机构的主要提取之外,在至少一个额外的提取 - 稀释回路中,从蒸煮器中抽出液体并将其引入到蒸煮器中来控制压力。 还可以通过控制洗涤稀释液的量以及通过改变提取流量来保持压力(例如约130-170psi)。
    • 123. 发明授权
    • Method of papermaking having zero liquid discharge
    • 造纸方法为零液体排放
    • US5762758A
    • 1998-06-09
    • US654248
    • 1996-05-28
    • Roger P. Hoffman
    • Roger P. Hoffman
    • D21B1/32D21C5/02D21C9/02D21C11/00D21F1/66D21F1/70
    • D21C5/02D21B1/32D21C11/0021D21C9/02D21F1/66Y02W30/646Y02W30/648
    • A method of papermaking having zero liquid discharge. A cellulosic pulp composed of recycled materials is initially cleaned to remove contaminants and foreign material, and the clean pulp is then washed to remove dissolved solids and pulping chemicals, and the washed pulp is then utilized in the papermaking process. The contaminants are separated from the liquid residue resulting from the pulp cleaning operation, preferably by floatation clarification, and the effluent from the clarification is evaporated to produce steam or water vapor along with an evaporated residue. The evaporated residue is combined with the suspended solids that were removed from the liquid residue and the combined residue is then subjected to a mechanical dewatering operation to reduce the water content so that the dewatered material can then be either landfilled or incinerated. The condensate from the evaporation can be combined with fresh makeup water and used in the papermaking process. Water recovered from the papermaking process is recycled to the pulp washing operation and water recovered from the pulp washing is recycled to the pulp cleaning and pulping operations, thus resulting in zero liquid discharge from the operation.
    • 一种具有零液体排放的造纸方法。 首先清洁由回收材料组成的纤维素纸浆以除去污染物和异物,然后清洁干净的纸浆以除去溶解的固体和制浆化学品,然后将洗涤过的纸浆用于造纸过程。 污染物与纸浆清洁操作中产生的液体残留物分离,优选通过浮选澄清分离,并且来自澄清的流出物被蒸发以产生蒸汽或水蒸汽以及蒸发的残余物。 将蒸发的残余物与从液体残余物中除去的悬浮固体组合,然后对合并的残余物进行机械脱水操作以减少水分含量,以便然后将脱水的材料进行填埋或焚化。 来自蒸发的冷凝物可以与新鲜的补充水结合,并用于造纸过程。 从造纸工艺回收的水被循环到纸浆洗涤操作中,从纸浆清洗回收的水被循环到纸浆清洁和制浆操作中,从而导致操作中的液体零排放。
    • 129. 发明授权
    • Apparatus for treatment of chips with heated black liquor
    • 用加热黑液处理碎片的装置
    • US5346591A
    • 1994-09-13
    • US52756
    • 1993-04-27
    • Kaj Henricson
    • Kaj Henricson
    • D21C1/00D21C3/02D21C3/24D21C11/00D21C7/14
    • D21C3/24D21C1/00D21C11/0021
    • An apparatus provide for the production of low kappa number (e.g. below 20) kraft paper pulp, and a low viscosity black liquor which is easily transported to a recovery or disposal stage. Comminuted cellulosic fibrous material is steamed, passed to a treatment vessel, land then introduced into the top of a continuous digester. Black liquor is withdrawn from the digester and heated about 20-40 degrees C above cooking temperature (e.g. about 170 degrees C), and then introduced into contact with the material in the treatment vessel. After the material is treated with the black liquor, it is withdrawn from the treatment vessel, and passed to the recovery or disposal stage. White liquor may be introduced into the treatment vessel after black liquor withdrawal, after passing in heat exchange relationship with liquid recirculated from an impregnation vessel to a high pressure feeder. Alkali may be added to the black liquor withdrawn from the digester, prior to heating, and after heating it may be passed to a reaction vessel.
    • 一种用于生产低卡伯值(例如低于20)的牛皮纸浆和低粘度黑液的装置,其易于运输至回收或处理阶段。 蒸发的纤维素纤维材料被蒸制,通入处理容器,然后将土地引入连续蒸煮器的顶部。 将黑液从蒸煮器中取出并在烹调温度(例如约170℃)下加热约20-40℃,然后与处理容器中的材料接触。 用黑液处理材料后,将其从处理容器中取出,并送至回收或处理阶段。 在黑液取出后,与从浸渍容器再循环到高压进料器的液体经过热交换关系后,白液可以被引入处理容器中。 可以在加热之前将碱加入到从蒸煮器中取出的黑液中,并且在加热之后可以将其转移到反应容器中。
    • 130. 发明授权
    • Treatment of chips with high temperature black liquor to reduce black
liquor viscosity
    • 用高温黑液处理烟雾以降低黑色液体粘度
    • US5213662A
    • 1993-05-25
    • US744506
    • 1991-08-14
    • Kaj Henricson
    • Kaj Henricson
    • D21C1/00D21C3/02D21C3/24D21C11/00
    • D21C3/24D21C1/00D21C11/0021
    • A method and apparatus provide for the production of low kappa number (e.g. below 20) kraft paper pulp, and a low viscosity black liquor which is easily transported to a recovery or disposal stage. Comminuted cellulosic fibrous material is steamed, passed to a treatment vessel, and then introduced into the top of a continuous digester. Black liquor is withdrawn from the digester and heated about 20-40 degrees C. above cooking temperature (e.g. about 170 degrees C.), and then introduced into contact with the material in the treatment vessel. After the material is treated with the black liquor, it is withdrawn from the treatment vessel, and passed to the recovery or disposal stage. White liquor may be introduced into the treatment vessel after black liquor withdrawal, after passing in heat exchange relationship with liquid recirculated from an impregnation vessel to a high pressure feeder. Alkali may be added to the black liquor withdrawn from the digester, prior to heating, and after heating it may be passed to a reaction vessel.
    • 一种制备低卡伯值(例如低于20)牛皮纸浆的方法和装置,以及容易运输至回收或处理阶段的低粘度黑液。 蒸发的纤维素纤维材料被蒸去,通过处理容器,然后引入连续蒸煮器的顶部。 将黑液从蒸煮器中取出并在烹调温度(例如约170℃)以上加热约20-40℃,然后与处理容器中的材料接触。 用黑液处理材料后,将其从处理容器中取出,并送至回收或处理阶段。 在黑液取出后,与从浸渍容器再循环到高压进料器的液体经过热交换关系后,白液可以被引入处理容器中。 可以在加热之前将碱加入到从蒸煮器中取出的黑液中,并且在加热之后可以将其转移到反应容器中。