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111. 发明专利

DE2200127A1 未知
公开(公告)号：DE2200127A1
公开(公告)日：1973-07-12
申请号：DE2200127
申请日：1972-01-03
申请人： BASF AG
发明人： SCHEFCZIK ERNST DR
IPC分类号： C07C50/24 , C07D221/18 , C07D231/54 , C07D277/60 , C09B1/00 , C09B3/02 , C09B5/02 , C07C49/68

112. 发明专利

CH449159A Verfahren zur Herstellung eines gelb-grün leuchtenden Leuchtstoffes 未知
公开(公告)号：CH449159A
公开(公告)日：1967-12-31
申请号：CH549665
申请日：1965-04-21
申请人： VNII MONOKRISTALLOV STSINTILLY
发明人： BORIS MORDUKHOVICH KRASOVITSKY , VIKTOR KONDRATIEVICH MATVEEV , NADEZHDA FEDOROVNA ZEVCHENKO , LIA MIKHAILOVNA PODGORNAYA
IPC分类号： C09B3/02 , C09K11/06 , C09D5/22 , C09K1/02

113. 发明专利

GB384999A Improvements in and relating to the production of dyestuffs and intermediates of thebenzanthrone series 未知
公开(公告)号：GB384999A
公开(公告)日：1932-12-16
申请号：GB1746731
申请日：1931-06-16
申请人： DAVID CLARENCE RHYS JONES , ROBERT FRASER THOMSON , ICI LTD
IPC分类号： C09B3/02
摘要： Benzanthrone derivatives; dibenzpyrenequinones.--The mixture of alkali soluble products obtainable by condensing o-halogenated benzoic acids or their salts with benzanthrones (for example, according to the process of Specification 358,426) is (i) extracted with an inert organic solvent such as acetic acid, benzene or other liquid in which benzanthrone is readily soluble, (ii) the undissolved portion separated by filtration, (iii) the resulting filtrate diluted with an inert liquid in which benzanthrone is substantially insoluble but which is miscible with the above inert organic solvent, (iv) the precipitated solid separated, and if desired (v) residual dissolved matter recovered. The fractions so separated may be halogenated and also treated with acid condensing agents before or after such halogenation. In examples, (i) the alkali-fusion product of sodium o-chlorbenzoate and benzanthrone is extracted with glacial acetic acid at the boil and on cooling a violet residue separates out which is a blue vat-dye; the filtrates are diluted with water and a light-green precipitate filtered off; this appears to be a benzanthronylbenzoic acid; evaporation of the aqueous filtrates yields a yellow substance; the glacial acetic acid may be replaced by benzene in which case instead of water, petroleum ether or petrol is employed; (2) the light-green precipitate of (1) is brominated in glacial acetic acid; the brominated product is treated with concentrated sulphuric acid to give a dibenzpyrenequinone (dyes yellow to orange); (3) the light-green precipitate of (1) is treated with phosphorus pentoxide in nitrobenzene to give a dibenzpyrenequinone; alternatively boric acid with sulphuric acid may be used as condensing agent; (4) the light-green precipitate of (1) is chlorinated in glacial acetic acid; (5) the yellow residue of (1) is chlorinated in glacial acetic acid; (6) the violet residue of (1) is chlorinated in acetic acid.

114. 发明专利

GB359937A Manufacture of vat dyestuffs 未知
公开(公告)号：GB359937A
公开(公告)日：1931-10-28
申请号：GB2268030
申请日：1930-07-28
申请人： ICI LTD , CECIL SHAW , ROBERT FRASER THOMSON
IPC分类号： C09B3/02
摘要： Benzanthrone dyes.-Grey to black vat dyes are obtained by treating benzanthrone, preferably at moderate temperatures, with a chromic acid oxidizing agent, followed by alkali fusion of the product obtained. In examples, benzanthrone is oxidized with sodium dichromate in sulphuric acid and the product, either with or without previous purification by extraction with toluene, is fused with methylated spirit and caustic potash. The products give direct blue-black or greenish-black shades from the vat.

115. 发明专利

GB328705A Process for the manufacture and production of vat dyestuffs containing sulphur 未知
公开(公告)号：GB328705A
公开(公告)日：1930-05-08
申请号：GB484129
申请日：1929-02-13
申请人： IG FARBENINDUSTRIE AG
IPC分类号： C09B3/02
摘要： 328,705. Johnson, J., Y., (I. G. Farbenindustrie Akt.-Ges.). Feb. 13, 1929. Anthraquinone vat dyes are obtained by the action of alkaline condensing agents on anthraquinonylmercaptobenzanthrones or anthraquinonylmercaptodibenzanthronyls other than those of such compounds in which an anthraquinone residue is attached by means of a mercapto group to the Bz1- and/or 2-positions in a benzanthrone radical. In examples, the following substances are fused with alcoholic potash :-1 -anthraquinonyl-6-mercaptobenzanthrone, 1 -anthraquinonyl- 8-mercaptobenzanthrone, di-a-anthraquinonyl- 6 : 6 -dimercapto-2 : 2'-dibenzanthronyl (prepared by condensing 1 mol. of 6: 6 -dichloro-2 : 2 -dibenzanthronyl with 2 mols. of sodium anthraquinone-1-mercaptide), di-a-anthraquinonyl-6: :6 - dimercapto-Bz1 : Bz1 -dibenzanthronyl and di-aanthraquinonyl - dimercapto - 2 : Bz1 - dibenzanthronyl (prepared by treating 2 : Bz1-dibenzan thronyl with bromine and condensing 1 mol. of the dibromo derivative with 2 mols. of sodium anthraquinone-1-mercaptide). The products dye cotton in greenish-blue to marine-blue shades.

116. 发明专利

DE495366C 未知
公开(公告)号：DE495366C
公开(公告)日：1930-04-05
申请号：DEB0130628
申请日：1927-04-01
申请人： BRITISH DYESTUFFS CORP LTD , JAMES BADDILEY , ARNOLD SHEPHERDSON , SIDNEY THORNLEY
IPC分类号： C09B3/02

117. 发明专利

DE485786C 未知
公开(公告)号：DE485786C
公开(公告)日：1929-11-05
申请号：DEI0027073
申请日：1925-12-19
申请人： IG FARBENINDUSTRIE AG
发明人： HOLZAPFEL DR EDUARD , BRAUNSDORF DR OTTO
IPC分类号： C09B3/02

118. 发明专利

DE458447C 未知
公开(公告)号：DE458447C
公开(公告)日：1928-04-11
申请号：DEC0036980
申请日：1925-07-21
申请人： CASSELLA LEOPOLD & CO GMBH
发明人： KALISCHER DR GEORG , ZERWECK DR WERNER
IPC分类号： C09B3/02

119. 发明专利

DE416028C 未知
公开(公告)号：DE416028C
公开(公告)日：1925-07-06
申请号：DEB0112276
申请日：1924-01-12
申请人： BASF AG
发明人： LUETTRINGHAUS DR ARTHUR , NERESHEIMER DR HEINRICH , EMMER DR HANNS JOSEF
IPC分类号： C09B3/02

120. 发明专利

FR545263A 未知
公开(公告)号：FR545263A
公开(公告)日：1922-10-09
申请号：FR545263D
申请日：1921-12-28
申请人： NAT ANILINE & CHEM CO INC
IPC分类号： C09B3/02

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