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    • 102. 发明授权
    • Toner processes
    • 墨粉处理
    • US5902710A
    • 1999-05-11
    • US132949
    • 1998-08-12
    • Beng S. OngRaj D. Patel
    • Beng S. OngRaj D. Patel
    • G03G9/097B82B1/00G03G9/08G03G9/087
    • G03G9/0804
    • A process for the preparation of toner comprising(i) preparing, or providing an aqueous colorant dispersion, which dispersion is comprised of a colorant and an ionic surfactant in water;(ii) blending said colorant dispersion with a latex emulsion comprised of resin particles, a nonionic surfactant, and an ionic surfactant of opposite charge polarity to that of the ionic surfactant in said colorant dispersion;(iii) heating the resulting mixture below about the glass transition temperature (Tg) of the latex resin to form toner sized aggregates;(iv) heating the resulting aggregate suspension of (iii) above about the Tg of the latex resin; and(v) retaining the temperature in the range of from about 30.degree. C. to about 95.degree. C., and subsequently, adding an aqueous solution of boric acid, or an aqueous solution of a metal salt; adjusting the pH of the resulting reaction mixture to from about 9 to about 12 by the addition of a base, followed by the addition of a salicylic acid or catechol; and optionally(vi) isolating, washing and drying the toner obtained.
    • 一种制备调色剂的方法,包括(i)制备或提供水性着色剂分散体,该分散体由着色剂和离子表面活性剂在水中组成; (ii)将所述着色剂分散体与由所述着色剂分散体中的离子表面活性剂相反的极性的树脂颗粒,非离子表面活性剂和离子表面活性剂组成的胶乳乳液混合; (iii)将所得混合物加热至胶乳树脂的玻璃化转变温度(Tg)以下以形成调色剂尺寸的聚集体; (iv)在胶乳树脂的Tg附近加热(iii)所得的聚集体悬浮液; 和(v)将温度保持在约30℃至约95℃的范围内,随后加入硼酸水溶液或金属盐水溶液; 通过加入碱将所得反应混合物的pH调节至约9至约12,然后加入水杨酸或儿茶酚; 和(vi)分离,洗涤和干燥获得的调色剂。