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101. 发明授权

US06958608B2 Nuclear magnetic resonance equipment 失效
标题翻译：核磁共振设备
公开(公告)号：US06958608B2
公开(公告)日：2005-10-25
申请号：US10852254
申请日：2004-05-25
申请人： Kazumasa Takagi , Kazuo Saitoh , Hisaaki Ochi , Hiroshi Morita , Masae Kiryu , Michiya Okada
发明人： Kazumasa Takagi , Kazuo Saitoh , Hisaaki Ochi , Hiroshi Morita , Masae Kiryu , Michiya Okada
IPC分类号： G01R33/32 , G01R33/34 , G01R33/343 , G01V3/00
CPC分类号： G01R33/34053 , G01R33/34007 , G01R33/34023 , G01R33/34092 , G01R33/3456
摘要： The invention provides nuclear magnetic resonance equipment realizing improved sensitivity of a probe for receiving a free induction decay (FID) signal in nuclear magnetic resonance (NMR) spectroscopy in a high frequency band of 600 MHz or higher. By manufacturing a solenoid coil of a higher filling factor by using a superconductor of extremely low resistance to high frequency current, sensitivity is increased. A superconducting thin film made of magnesium diboride (MgB2) formed on a donut plate-type substrate is disposed so that the film surface becomes parallel with the uniform magnetic field. The object is realized by a probe made by a solenoid coil formed by connecting a plurality of coil parts by capacitive coupling via a normal metal lead.
摘要翻译：本发明提供了在600MHz或更高的高频带内实现核磁共振（NMR）光谱中接收自由感应衰减（FID）信号的探头的灵敏度提高的核磁共振设备。通过使用对高频电流具有极低电阻的超导体制造具有较高填充系数的电磁线圈，灵敏度增加。设置形成在环状基板上的由二硼化镁（MgB 2 N 2）构成的超导薄膜，使得膜表面与均匀的磁场平行。该目的通过由螺线管线圈制成的探针实现，该螺线管通过通过电容耦合经由正常金属引线连接多个线圈部分而形成。

102. 发明申请

US20050231202A1 Probe for NMR apparatus using magnesium diboride 失效
公开(公告)号：US20050231202A1
公开(公告)日：2005-10-20
申请号：US11139548
申请日：2005-05-31
申请人： Hiroshi Morita , Michiya Okada , Katsuzou Aihara
发明人： Hiroshi Morita , Michiya Okada , Katsuzou Aihara
IPC分类号： H01F6/00 , G01R33/34 , G01V3/00 , H01F6/06
CPC分类号： G01R33/34053 , G01R33/34023 , G01R33/34069 , G01R33/34092 , H01F6/06
摘要： To provide a probe coil for an NMR apparatus which can transmit and receive high frequency radio waves with improved Q-factor and S/N ratio. As a measure, the probe coil for an NMR apparatus is provided as of a solenoid type formed of magnesium diboride superconductor. As another measure, the probe coil for an NMR apparatus has a plurality of coils using magnesium diboride superconductors connected in series. As further another measure, there is used a magnesium diboride superconductor mixed with metal. As still further another measure, the probe coil for an NMR apparatus is formed by using a single metal selected from gold, silver, copper, aluminum, iron, platinum, palladium, nickel, stainless steel, chromium, magnesium, tantalum, niobium, titanium, zinc, beryllium, tungsten, or cobalt, or an alloy including a plurality thereof.

103. 发明授权

US06937019B2 Supersensitive nuclear magnetic resonance micro imaging apparatus 失效
标题翻译：超敏核磁共振微成像装置
公开(公告)号：US06937019B2
公开(公告)日：2005-08-30
申请号：US10656185
申请日：2003-09-08
申请人： Michiya Okada , Tsuyoshi Wakuda , Shigeru Kakugawa , Hiroshi Morita , Katsuzou Aihara
发明人： Michiya Okada , Tsuyoshi Wakuda , Shigeru Kakugawa , Hiroshi Morita , Katsuzou Aihara
IPC分类号： G01R33/465 , G01R33/30 , G01R33/34 , G01R33/3815 , G01R33/48 , G01R33/56 , G01V3/00
CPC分类号： G01R33/3815 , G01R33/465 , G01R33/5604
摘要： A supersensitive nuclear magnetic resonance imaging apparatus includes superconducting magnet, a gradient magnetic field coil, a high frequency emitting coil, and a receiving coil, wherein a biosample, including at least one of cells, organic tissues, and laboratory small animals, is inserted in a sample chamber of generally 1 to 30 mm in diameter. The superconducting magnet is formed of laterally divided split magnets, and the direction of the magnetic field generated by the magnet is generally horizontal. The receiving coil is in the form of a solenoid coil, and the biosample is inserted from a direction orthogonal to the direction of the magnetic field in a generally vertical direction. The spatial resolution in imaging of the biosample is not more than one-tenth of a cell that forms the biosample.
摘要翻译：超灵敏核磁共振成像装置包括超导磁体，梯度磁场线圈，高频发射线圈和接收线圈，其中将包括细胞，有机组织和实验室小动物中的至少一个的生物样本插入通常为1至30mm的样品室。超导磁体由横向分开的分割磁体形成，并且由磁体产生的磁场的方向大致水平。接收线圈是螺线管线圈的形式，并且生物样本沿着与大致垂直方向的磁场方向正交的方向插入。生物样品成像中的空间分辨率不超过形成生物样品的细胞的十分之一。

104. 发明申请

US20050174202A1 Superconducting wire material and method for preparation thereof, and superconducting magnet using the same 审中-公开
标题翻译：超导线材及其制备方法以及使用其的超导磁体
公开(公告)号：US20050174202A1
公开(公告)日：2005-08-11
申请号：US10480839
申请日：2002-06-11
申请人： Kazuhide Tanaka , Michiya Okada , Hiroshi Morita , Yasuo Suzuki
发明人： Kazuhide Tanaka , Michiya Okada , Hiroshi Morita , Yasuo Suzuki
IPC分类号： H01F6/00 , H01B12/10 , H01B13/00 , H01F6/06 , H01L39/14 , H01L39/24 , H01H75/00
CPC分类号： H01F6/06 , H01L39/141 , H01L39/2487
摘要： An object of the present invention is to provide: a superconducting wire with a boron-containing superconductor charged or included therein, the superconducting wire further being able to have a practical critical current density; a method for manufacturing the superconducting wire, and; a superconducting magnet using the superconducting wire. The present invention is characterized in that: in a superconducting wire which has a boron-containing superconductor charged or included therein, a metal-sheathing material made of either a single metal selected from a group consisting of gold, silver, aluminum, copper, iron, platinum, palladium, nickel, stainless steel, chromium, magnesium, tantalum, niobium, titanium, tin, beryllium, tungsten, and cobalt, or an alloy consisting of a plurality of metals selected from this group, is disposed on the outer surface of the foregoing superconducting wire, the density of the superconducting wire after it has been finally processed is 80% or more of its theoretical density, and the critical temperature of the superconducting wire is 30K or more.
摘要翻译：本发明的目的是提供：具有充电或包含在其中的含硼超导体的超导线，所述超导线还能够具有实用的临界电流密度; 一种制造超导线材的方法，使用超导线的超导磁体。本发明的特征在于：在具有充电或包含其中的含硼超导体的超导线中，由金，银，铝，铜，铁等构成的一种金属制成的金属包覆材料，铂，钯，镍，不锈钢，铬，镁，钽，铌，钛，锡，铍，钨和钴，或由选自该组的多种金属组成的合金设置在上述超导线材，其最终加工后的超导线材的密度为理论密度的80％以上，超导线材的临界温度为30K以上。

105. 发明申请

US20050122114A1 Nuclear magnetic resonance spectrometer for liquid-solution 有权
公开(公告)号：US20050122114A1
公开(公告)日：2005-06-09
申请号：US11033630
申请日：2005-01-13
申请人： Michiya Okada , Tsuyoshi Wakuda , Shigeru Kakugawa , Hiroshi Morita , Katsuzo Aihara
发明人： Michiya Okada , Tsuyoshi Wakuda , Shigeru Kakugawa , Hiroshi Morita , Katsuzo Aihara
IPC分类号： G01R33/34 , G01N24/08 , G01R33/3815 , G01R33/465 , H01F5/00 , H01F7/20 , G01V3/00
CPC分类号： G01R33/34046 , G01R33/34053 , G01R33/34092 , G01R33/3806 , G01R33/3815 , G01R33/465
摘要： In a nuclear magnetic resonance spectrometer, the shape of a detection coil is changed from a conventional cage type to a solenoid type of higher sensitivity. Accordingly, differing from the conventional superconductive magnet of multilayer air core solenoids, a superconductive magnet is right and left divided to split magnets for generating 11 T, preferably, 14.1 T in the horizontal direction, and the magnetic field uniformity is set to 0.001 ppm or less and the temporal stability is set to 0.001 ppm or less.

106. 发明申请

US20050122112A1 NMR analyzer 失效
标题翻译： NMR分析仪
公开(公告)号：US20050122112A1
公开(公告)日：2005-06-09
申请号：US11025915
申请日：2005-01-03
申请人： Katsuzou Aihara , Michiya Okada , Shigeru Kakugawa , Hiroshi Morita , Tsuyoshi Wakuda
发明人： Katsuzou Aihara , Michiya Okada , Shigeru Kakugawa , Hiroshi Morita , Tsuyoshi Wakuda
IPC分类号： G01R33/32 , G01R33/345 , G01R33/3815 , G01R33/3875 , G01V3/00
CPC分类号： G01R33/34046 , G01R33/34053 , G01R33/3806 , G01R33/3815 , G01R33/44 , G01R33/4808
摘要： A first room-temperature space is formed penetrating through a cryostat along a center axis of a split-type multi-layer cylindrical superconducting coil system which has a ratio of the maximum empirical magnetic field to the central magnetic filed of not larger than 1.3 and is horizontally arranged such that the center axis of the coil is in the horizontal direction, a room-temperature shim coil system is arranged in said first room-temperature space to improve the homogeneity of the magnetic field, a second room-temperature space is formed penetrating through the cryostat and passing through the center of said split gap in the vertical direction, and a sample to be measured and an NMR probe having a solenoid-type probe coil are inserted in said second room-temperature space. Further, the NMR analyzer has a new function constituted by a system for irradiating and detecting the electromagnetic waves having wavelengths of shorter than 0.1 mm.
摘要翻译：第一室温空间形成为沿分离型多层圆柱形超导线圈系统的中心轴穿过低温恒温器，该分离型多层圆柱形超导线圈系统的最大经验磁场与中心磁场的比值不大于1.3，水平排列为使得线圈的中心轴线处于水平方向，在所述第一室温空间内布置室温垫片线圈系统，以改善磁场的均匀性，形成第二室温空间通过低温恒温器并沿着垂直方向穿过所述分割间隙的中心，并且将待测量样品和具有螺线管型探针线圈的NMR探针插入所述第二室温空间中。此外，NMR分析仪具有由用于照射和检测波长小于0.1mm的电磁波的系统构成的新功能。

107. 发明授权

US06859036B2 NMR analyzer 失效
标题翻译： NMR分析仪
公开(公告)号：US06859036B2
公开(公告)日：2005-02-22
申请号：US10315215
申请日：2002-12-10
申请人： Katsuzou Aihara , Michiya Okada , Shigeru Kakugawa , Hiroshi Morita , Tsuyoshi Wakuda
发明人： Katsuzou Aihara , Michiya Okada , Shigeru Kakugawa , Hiroshi Morita , Tsuyoshi Wakuda
IPC分类号： G01R33/32 , G01R33/345 , G01R33/3815 , G01R33/3875 , G01V3/00
CPC分类号： G01R33/34046 , G01R33/34053 , G01R33/3806 , G01R33/3815 , G01R33/44 , G01R33/4808
摘要： A first room-temperature space is formed penetrating through a cryostat along a center axis of a split-type multi-layer cylindrical superconducting coil system which has a ratio of the maximum empirical magnetic field to the central magnetic field of not larger than 1.3 and is horizontally arranged such that the center axis of the coil is in the horizontal direction, a room-temperature shim coil system is arranged in said first room-temperature space to improve the homogeneity of the magnetic field, a second room-temperature space is formed penetrating through the cryostat and passing through the center of said split gap in the vertical direction, and a sample to be measured and an NMR probe having a solenoid-type probe coil are inserted in said second room-temperature space. Further, the NMR analyzer has a new function constituted by a system for irradiating and detecting the electromagnetic waves having wavelengths of shorter than 0.1 mm.
摘要翻译：第一室温空间形成为沿着分离式多层圆柱形超导线圈系统的中心轴穿过低温恒温器，其具有最大经验磁场与中心磁场的比例不大于1.3，并且是水平排列为使得线圈的中心轴线处于水平方向，在所述第一室温空间内布置室温垫片线圈系统，以改善磁场的均匀性，形成第二室温空间通过低温恒温器并沿着垂直方向穿过所述分割间隙的中心，并且将待测量样品和具有螺线管型探针线圈的NMR探针插入所述第二室温空间中。此外，NMR分析仪具有由用于照射和检测波长小于0.1mm的电磁波的系统构成的新功能。

108. 发明授权

US06768306B2 Probe for NMR apparatus using magnesium diboride 失效
标题翻译：使用二硼化镁的NMR仪器的探头
公开(公告)号：US06768306B2
公开(公告)日：2004-07-27
申请号：US10315115
申请日：2002-12-10
申请人： Hiroshi Morita , Michiya Okada , Katsuzou Aihara
发明人： Hiroshi Morita , Michiya Okada , Katsuzou Aihara
IPC分类号： G01V300
CPC分类号： G01R33/34053 , G01R33/34023 , G01R33/34069 , G01R33/34092 , H01F6/06
摘要： To provide a probe coil for an NMR apparatus which can transmit and receive high frequency radio waves with improved Q-factor and S/N ratio. As a measure, the probe coil for an NMR apparatus is provided as of a solenoid type formed of magnesium diboride superconductor. As another measure, the probe coil for an NMR apparatus has a plurality of coils using magnesium diboride superconductors connected in series. As further another measure, there is used a magnesium diboride superconductor mixed with metal. As still further another measure, the probe coil for an NMR apparatus is formed by using a single metal selected from gold, silver, copper, aluminum, iron, platinum, palladium, nickel, stainless steel, chromium, magnesium, tantalum, niobium, titanium, zinc, beryllium, tungsten, or cobalt, or an alloy including a plurality thereof.
摘要翻译：提供一种能够以改善的Q因子和S / N比发送和接收高频无线电波的NMR装置的探针线圈。作为测量，用于NMR装置的探针线圈以由二硼化镁超导体形成的螺线管形式提供。作为另一个措施，用于NMR装置的探针线圈具有使用串联连接的二硼化硼超导体的多个线圈。作为另一个措施，使用与金属混合的二硼化镁超导体。作为另一种措施，NMR装置的探针线圈通过使用选自金，银，铜，铝，铁，铂，钯，镍，不锈钢，铬，镁，钽，铌，钛的单一金属形成，锌，铍，钨或钴，或包含多个的合金。

109. 发明授权

US6103669A Superconducting wire and method of producing the same 失效
标题翻译：超导线及其制造方法
公开(公告)号：US6103669A
公开(公告)日：2000-08-15
申请号：US448137
申请日：1995-05-23
申请人： Akira Okayama , Michiya Okada , Tadaoki Morimoto , Toshimi Matsumoto , Yoshimi Yanai , Hiroshi Satoh , Toshiya Doi , Kazuhide Tanaka , Takahiko Kato
发明人： Akira Okayama , Michiya Okada , Tadaoki Morimoto , Toshimi Matsumoto , Yoshimi Yanai , Hiroshi Satoh , Toshiya Doi , Kazuhide Tanaka , Takahiko Kato
IPC分类号： H01B12/04 , H01B13/00 , H01L39/14 , H01L39/24
CPC分类号： H01L39/143 , H01L39/248 , Y10T29/49014
摘要： This invention provides an oxide-type superconducting flat wire having a critical current density of at least 1,000 A/cm.sup.2, which comprises a Y--Ba--Cu oxide layer having a superconducting property and a silver layer surrounding the oxide layer and has so flat a cross section vertical to the longitudinal direction of the wire that the upper and lower lines between the oxide layer and the silver layers appearing on the cross section having a zone over they are parallel to each other, the thickness of the oxide layer being cold rolled in the range of 0.35 to 0.75 based on the whole thickness of the wire, the whole thickness being 0.2 mm or less, and the metal layer being deformable to follow the shrink deformation of the oxide layer when heat treated to be sintered, but rigid when used. This flat wire is produced by filling a silver-made tube with a Y--Ba--Cu oxide powder having a superconducting property, drawing the tube into a rod wire having a round cross section, then cold rolling the rod wire in the flat wire so that (t.sub.i -t)/t.sub.i .times.100 is equal to or greater than 90%, wherein t.sub.i is the whole thickness of the cross section of the rod wire before the cold rolling and t is the whole thickness of the cold-rolled flat wire, and then heat treating the flat wire to sinter the superconducting oxide.
摘要翻译：本发明提供了具有至少1000A / cm 2的临界电流密度的氧化物型超导扁线，其包括具有超导特性的Y-Ba-Cu氧化物层和围绕氧化物层的银层，并且具有如此平坦的横截面垂直于导线的纵向方向，在它们之间具有区域的横截面上出现的氧化物层和银层之间的上下线之间彼此平行，氧化层的厚度被冷轧基于整个线材的0.35至0.75的范围，整个厚度为0.2mm或更小，并且当热处理烧结时，金属层可变形以跟随氧化物层的收缩变形，但是当使用时是刚性的。该扁线通过用具有超导特性的Y-Ba-Cu氧化物粉末填充银制管而制成，将管拉成具有圆形横截面的棒丝，然后将扁丝中的棒丝冷轧（ti-t）/ tix100等于或大于90％，其中ti是冷轧前棒丝的横截面的整个厚度，t是冷轧扁丝的整个厚度，然后对扁线进行热处理以烧结超导氧化物。

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