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101. 发明授权

US5021092A Method for the preparation of gray-green pigments based on zirconium silicate/vanadium compounds and sodium compound 失效
标题翻译：基于硅酸锆/钒化合物和钠化合物的灰绿色颜料的制备方法
公开(公告)号：US5021092A
公开(公告)日：1991-06-04
申请号：US389761
申请日：1989-08-04
申请人： Dietrich Speer , Akos Kiss , Peter Kleinschmit
发明人： Dietrich Speer , Akos Kiss , Peter Kleinschmit
IPC分类号： C01G31/02 , C09C1/00 , C09C1/28
CPC分类号： C09C1/0012 , C01P2002/70
摘要： The preparation of gray-green unitary pigment bodies based on zirconium silicate-vanadium oxide wherein a mixture of zirconium oxide and silicon oxide in the presence of a vanadium and lithium compound is calcined above 600.degree. C. and wherein the amount of V.sub.2 O.sub.5 is more than 17 percent by weight and the amount of lithium compound added is such that the atom ratio Li/Li+V is from 0.1 to 0.5.
摘要翻译：制备基于硅酸锆 - 氧化钒的灰绿色整体色素体，其中在钒和锂化合物的存在下，氧化锆和氧化硅的混合物在600℃以上煅烧，其中V 2 O 5的量大于 17重量％，添加的锂化合物的量使得Li / Li + V的原子比为0.1〜0.5。

102. 发明授权

US5008223A Grayish-black encapsulated pigments and method of their production 失效
标题翻译：灰黑色胶囊颜料及其制作方法
公开(公告)号：US5008223A
公开(公告)日：1991-04-16
申请号：US487295
申请日：1990-03-02
申请人： Dietrich Speer , Akos Kiss , Peter Kleinschmit , Juergen Hanich
发明人： Dietrich Speer , Akos Kiss , Peter Kleinschmit , Juergen Hanich
IPC分类号： C04B41/85 , C01B33/20 , C09C1/00 , C09C1/30 , C09C1/56 , C09C3/06
CPC分类号： C09C1/0012 , C01P2002/08 , C01P2004/84 , C01P2006/12
摘要： The grayish-black encapsulated pigments contain carbon black particles with specific surface areas of 10 to 1000 m.sup.2 /g (BET) encapsulated in colorless crystals of zirconium silicate. In order to produce the pigments, mixtures of zirconium oxide with a particle size distribution (D50 values) between 7 and 10 .mu.m and a spec. surface between 2 and 4 m.sup.2 /g, silicon oxide, carbon black and mineralizers are heated under reducing conditions to 900.degree. to 1400.degree. C. and calcined for 0.5 to 8 hours and recalcined under oxidizing conditions to remove the non-included carbon black. The encapsulated pigments of the invention are suitable for the pigmented coloration of glazes.
摘要翻译：灰黑色胶囊状颜料含有炭黑颗粒，其表面积为10至1000m2 / g（BET），其包封在无色硅酸锆晶体中。为了制备颜料，氧化锆的混合物的粒度分布（D50值）在7和10μm之间，表面积为2〜4m2 / g，氧化硅，炭黑和矿化剂在还原条件下加热至900〜1400℃，煅烧0.5〜8小时，在氧化条件下重新煅烧，除去未包含的炭黑。本发明的胶囊化颜料适用于釉料着色着色。

103. 发明授权

US4976943A Spherical, hydrophilic silica, method of its preparation and use 失效
标题翻译：球形，亲水性二氧化硅，其制备方法及用途
公开(公告)号：US4976943A
公开(公告)日：1990-12-11
申请号：US351054
申请日：1989-05-12
申请人： Ingo Pauli , Peter Kleinschmit , Rudolf Schwarz
发明人： Ingo Pauli , Peter Kleinschmit , Rudolf Schwarz
IPC分类号： C01B33/16 , C01B33/12 , C01B33/18 , C08K3/34 , C08K3/36
CPC分类号： C01B33/183 , C01B33/12 , C01P2002/02 , C01P2004/32 , C01P2004/51 , C01P2004/61 , C01P2004/62 , C01P2006/12 , C01P2006/90
摘要： A spherical, hydrophilic silica consisting of compact, massive, non-crystalline particles without inner pores with a particle size of 0.5 to 10 .mu.m, preferably 0.5 to 4 .mu.m and especially 1 to 3 .mu.m with a BET surface of
摘要翻译：一种球形的亲水性二氧化硅，其由紧凑的，块状的，非结晶的颗粒组成，没有内孔，粒径为0.5至10μm，优选0.5至4μm，特别是1至3μm，BET表面积<50m2 通过将水蒸气和气态四氯化硅分别加热至300-400℃的温度，以2:1至6.7:1的摩尔比彼此混合来制备/ g，优选1至10m 2 / g。并在600-1200℃的温度下使混合物反应。

104. 发明授权

US4697009A N-silylpropyl-N'-acyl-ureas and process for their production 失效
标题翻译： N-甲硅烷基丙基-N'-酰基脲及其生产方法
公开(公告)号：US4697009A
公开(公告)日：1987-09-29
申请号：US875867
申请日：1986-06-18
申请人： Ulrich Deschler , Peter Kleinschmit , Rudolf Michel
发明人： Ulrich Deschler , Peter Kleinschmit , Rudolf Michel
IPC分类号： C08G18/00 , C07F7/18 , C08G18/80 , C07F7/10
CPC分类号： C07F7/182
摘要： The invention is directed to N-silylpropyl-N'-acyl ureas and their production from an alkali cyanate, a 3-halopropylsilane and in a given case, a cyclic acidamide. By heating the compounds of the invention the blocked isocyanate function can be set free.
摘要翻译：本发明涉及N-甲硅烷基丙基-N'-酰基脲，它们由碱式氰酸酯，3-卤代丙基硅烷的产生，在给定情况下是环状酰胺。通过加热本发明的化合物，可以使封闭的异氰酸酯官能团自由。

105. 发明授权

US4668648A Magnesium-silicate bound zeolite granulates of the type of zeolite A, process for their production and use 失效
标题翻译：沸石A类型的硅酸镁结合沸石颗粒，其生产和使用过程
公开(公告)号：US4668648A
公开(公告)日：1987-05-26
申请号：US827926
申请日：1986-02-10
申请人： Hans Strack , Peter Kleinschmit
发明人： Hans Strack , Peter Kleinschmit
IPC分类号： A24D3/16 , B01J20/18 , C01B39/14 , B01J29/06
CPC分类号： B01J20/183 , A24D3/166
摘要： Magnesium-silicate bound zeolite granulates of type A are disclosed wherein the zeolite component does not contain magnesium exclusively, or contains no magnesium at all, as the cation. The granulates are produced by placing powdered zeolite A in a mixer, adding sodium silicate solution, mixing until zeolite granulates with a grain size of at least 0.1 mm are obtained, optionally after-rolling these zeolite granulates, optionally initially drying the moist zeolite granulates at temperatures of 20 to 39 degrees C., during which the carbon dioxide content of the drying air is adjusted to less than 200 ppm, then optionally drying in a second drying step at temperatures of 40-120 degrees C. and optionally in a third drying stage at 121-200 degrees C. under otherwise identical conditions, and then optionally activating the granulates thus obtained at temperatures of 600 degrees C. maximum. The granulates thus obtained are treated with an aqueous magnesium salt solution, washed, then optionally treated with aqueous metal salt solution, washed, dried at 40-200 degrees C., preferably 100 to 120 degrees C., and then optionally calcined at 300 to 650 degrees C.
摘要翻译：公开了A型的硅酸镁结合的沸石颗粒，其中沸石组分不含镁，或完全不含有镁作为阳离子。颗粒是通过将粉末状沸石A置于混合器中，加入硅酸钠溶液，混合直到得到粒度至少为0.1mm的沸石颗粒，任选地后轧这些沸石颗粒，任选地首先将湿沸石颗粒干燥温度为20至39摄氏度，在此期间将干燥空气的二氧化碳含量调节至小于200ppm，然后任选地在第二干燥步骤中在40-120℃的温度和任选地在第三次干燥在121-200℃的条件下，在相同的条件下，然后任选地在600摄氏度的温度下活化由此获得的颗粒最大值。将如此得到的颗粒用镁盐水溶液处理，洗涤，然后任选用金属盐水溶液处理，洗涤，在40-200℃，优选100-120℃下干燥，然后任选在300℃煅烧至 650摄氏度

106. 发明授权

US4608236A Process for the production of a seed mixture for faujasite synthesis 失效
标题翻译：用于生产八面沸石合成种子混合物的方法
公开(公告)号：US4608236A
公开(公告)日：1986-08-26
申请号：US593164
申请日：1984-03-26
申请人： Hans Strack , Peter Kleinschmit
发明人： Hans Strack , Peter Kleinschmit
IPC分类号： C01B33/26 , B01J29/00 , C01B33/36 , C01B39/20
CPC分类号： C01B39/20 , Y10S423/21
摘要： A seed mixture is produced by reacting an amorphous, synthetic sodium aluminum silicate with an Na.sub.2 O-supplying compound in an aqueous system at temperatures of 10.degree. to 35.degree. C. (room temperature). The seed mixture exhibits a composition of Na.sub.2 O:Al.sub.2 O.sub.3 :SiO.sub.2 :H.sub.2 O=(12.+-.3):1:(15.+-.3):(240.+-.60). This seed mixture can be used in the synthesis of zeolite Y and/or zeolite X.
摘要翻译：通过使无定形合成的硅酸铝钠与供水化合物NaO在10至35℃（室温）的水溶液体系中反应制备种子混合物。种子混合物显示组成为Na 2 O：Al 2 O 3 :SiO 2 :H 2 O =（12 +/- 3）：1：（15 +/- 3）：（240 +/- 60）。该种子混合物可用于合成沸石Y和/或沸石X.

107. 发明授权

US4514231A Natural oxidic or silicate filler modified on the surface, a process for its production 失效
标题翻译：表面改性的天然氧化物或硅酸盐填料，其生产工艺
公开(公告)号：US4514231A
公开(公告)日：1985-04-30
申请号：US602768
申请日：1984-04-23
申请人： Dieter Kerner , Peter Kleinschmit , Alan Parkhouse , Siegfried Wolff
发明人： Dieter Kerner , Peter Kleinschmit , Alan Parkhouse , Siegfried Wolff
IPC分类号： C08L7/00 , C08K9/00 , C08K9/04 , C08K9/06 , C08L21/00 , C08L23/00 , C08L33/00 , C08L33/02 , C08L101/00 , C09C1/42 , C09C3/00 , C09C3/12
CPC分类号： C09C3/12 , C08K9/06 , C09C1/42 , C01P2004/84
摘要： The invention is directed to the modification of natural oxidic or silicate fillers with water insoluble sulfur containing organosilicon compounds. For this purpose, the fillers are converted into an aqueous suspension and treated with the organosilicon compounds, in a given case in the presence of an emulsifier.
摘要翻译：本发明涉及用水不溶性含硫有机硅化合物改性天然氧化物或硅酸盐填料。为此，将填料转化为水性悬浮液，并在有机硅化合物的情况下在乳化剂存在下进行处理。

108. 发明授权

US4408064A Bis-(silylethyl)-oligosulphides and process for their production 失效
标题翻译：双（甲硅烷基乙基） - 二硫化物及其生产方法
公开(公告)号：US4408064A
公开(公告)日：1983-10-04
申请号：US106862
申请日：1979-12-26
申请人： Rudolf Schwarz , Peter Kleinschmit , Christa Liedtke , Siegfried Wolff
发明人： Rudolf Schwarz , Peter Kleinschmit , Christa Liedtke , Siegfried Wolff
IPC分类号： C08L7/00 , C07F7/08 , C07F7/12 , C07F7/18 , C08G75/02 , C08G75/14 , C08K5/5425 , C08K5/548 , C08L21/00 , C08L23/00 , C08L33/00 , C08L33/02 , C08L101/00
CPC分类号： C08K5/548 , C07F7/12 , C07F7/182 , C08G75/02 , C08G75/14
摘要： Novel bis-(silylethyl)-oligosulphides are obtained by reacting a vinyl silane of the formula (CH.sub.2 .dbd.CH).sub.m -SiR.sub.n.sup.1 R.sub.4-(m+n) in which R represents chlorine, bromine, iodine, C.sub.1 -C.sub.3 -alkoxy, 2-methoxyethoxy, 2-ethoxyethoxy or hydroxy, R.sup.1 represents C.sub.1 -C.sub.3 -alkyl, phenyl or C.sub.5 -C.sub.7 -cycloalkyl, n is 0, 1 or 2, m is 1 or 2 and m+n is 1, 2 or 3 with sulphur as well as in a given case hydrogen sulphide in molar ratios of vinyl silane to sulphur of from 1:2.5 to 1:10 and vinyl silane to hydrogen sulphide of from 1:0 to 1:5 at temperatures between about 100.degree. and 200.degree. C. under pressure of from 1 to 25 bars (total pressure at the reaction temperature) and in the presence of sulphidation catalysts known per se, in a given case followed by hydrolysis or partial hydrolysis of the reaction products. The bis-(silylethyl)-oligosulphides are used as reinforcing additives (adhesive agents) in crosslinkable rubber mixtures containing silicate fillers and in a given case carbon black as well as in a given case sulphur and other customary constituents.
摘要翻译：通过使式（CH2 = CH）m-SiRn1R4-（m + n）的乙烯基硅烷（其中R表示氯，溴，碘，C1-C3-烷氧基，2-甲基苯基）甲氧基乙氧基，2-乙氧基乙氧基或羟基，R1代表C1-C3-烷基，苯基或C5-C7-环烷基，n是0,1或2，m是1或2，m + n是1,2或3，以及在给定情况下，在约100至200℃的温度下，乙烯基硅烷与硫的摩尔比为1:2.5至1:10的硫化氢和乙烯基硅烷至硫化氢的摩尔比为1:0至1:5 在1至25巴的压力（在反应温度下的总压力）和本身已知的硫化催化剂的存在下，在给定的情况下随后水解或部分水解反应产物。双（甲硅烷基乙基） - 二硫化物用作含有硅酸盐填料的交联性橡胶混合物中的增强添加剂（粘合剂），在给定情况下用于炭黑以及在给定情况下硫和其它常规组分。

109. 发明授权

US4387081A Process for the production of hydrogen cyanide 失效
标题翻译：生产氰化氢的方法
公开(公告)号：US4387081A
公开(公告)日：1983-06-07
申请号：US304049
申请日：1981-09-21
申请人： Carl Voigt , Peter Kleinschmit , Gerd Schreyer , Gerhard Sperka
发明人： Carl Voigt , Peter Kleinschmit , Gerd Schreyer , Gerhard Sperka
IPC分类号： B01J23/00 , C01C3/02
CPC分类号： C01C3/0233
摘要： In order to be independent of the situation in regard to methane and natural gas and at the same time to obtain a heating gas there is employed in the hydrocyanic acid-methane-ammonia process (the BMA process) in place of methane an alkanol or alkanediol having 2-4 carbon atoms, preferably ethyl alcohol, and this is reacted with ammonia in a C:N ratio of 0.8:1 to 2:1. Optionally additional hydrogen can be present.
摘要翻译：为了独立于甲烷和天然气的情况，同时获得加热气体，采用氢氰酸 - 甲烷 - 氨法（BMA法）代替烷烃或链烷二醇具有2-4个碳原子，优选乙醇，并且其与C：N比为0.8:1至2:1的氨反应。可选地，可以存在另外的氢。

110. 发明授权

US4384132A Bis-(silylethyl)-oligosulphides and process for their production 失效
标题翻译：双（甲硅烷基乙基） - 二硫化物及其生产方法
公开(公告)号：US4384132A
公开(公告)日：1983-05-17
申请号：US282949
申请日：1981-07-13
申请人： Rudolf Schwarz , Peter Kleinschmit , Christa Liedtke , Siegfried Wolff
发明人： Rudolf Schwarz , Peter Kleinschmit , Christa Liedtke , Siegfried Wolff
IPC分类号： C08L7/00 , C07F7/08 , C07F7/12 , C07F7/18 , C08G75/02 , C08G75/14 , C08K5/5425 , C08K5/548 , C08L21/00 , C08L23/00 , C08L33/00 , C08L33/02 , C08L101/00
CPC分类号： C08K5/548 , C07F7/12 , C07F7/182 , C08G75/02 , C08G75/14
摘要： Novel bis-(silylethyl)-oligosulphides are obtained by reacting a vinyl silane of the formula (CH.sub.2 .dbd.CH).sub.m -- SiR.sub.n.sup.1 R.sub.4 -(m+n) in which R represents chlorine, bromine, iodine, C.sub.1 -C.sub.3 -alkoxy, 2-methoxyethoxy, 2-ethoxyethoxy or hydroxy, R.sup.1 represents C.sub.1 -C.sub.3 -alkyl, phenyl or C.sub.5 -C.sub.7 -cycloalkyl, n is 0, 1 or 2, m is 1 or 2 and m+n is 1, 2 or 3 with sulphur as well as in a given case hydrogen sulphide in molar ratios of vinyl silane to sulphur of from 1:2.5 to 1:10 and vinyl silane to hydrogen sulphide of from 1:0 to 1:5 at temperatures between about 100.degree. and 200.degree. C. under pressure of from 1 to 25 bars (total pressure at the reaction temperature) and in the presence of sulphidation catalysts known per se, in a given case followed by hydrolysis or partial hydrolysis of the reaction products. The bis-(silylethyl)-oligosulphides are used as reinforcing additives (adhesive agents) in crosslinkable rubber mixtures containing silicate fillers and in a given case carbon black as well as in a given case sulphur and other customary constituents.
摘要翻译：通过使式（CH2 = CH）m -SiRn1R4 - （m + n）的乙烯基硅烷（其中R表示氯，溴，碘，C1-C3-烷氧基，2-甲基苯基）甲氧基乙氧基，2-乙氧基乙氧基或羟基，R1代表C1-C3-烷基，苯基或C5-C7-环烷基，n是0,1或2，m是1或2，m + n是1,2或3，以及在给定情况下，在约100至200℃的温度下，乙烯基硅烷与硫的摩尔比为1:2.5至1:10的硫化氢和乙烯基硅烷至硫化氢的摩尔比为1:0至1:5 在1至25巴的压力（在反应温度下的总压力）和本身已知的硫化催化剂的存在下，在给定的情况下随后水解或部分水解反应产物。双（甲硅烷基乙基） - 二硫化物用作含有硅酸盐填料的交联性橡胶混合物中的增强添加剂（粘合剂），在给定情况下用于炭黑以及在给定情况下硫和其它常规组分。

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