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91. 发明授权

US5401488A Substitution of Sn in place of Al in the framework of molecular sieve via treatment with fluoride salts 失效
标题翻译：通过用氟化物盐处理在分子筛的骨架中取代Sn代替Al
公开(公告)号：US5401488A
公开(公告)日：1995-03-28
申请号：US904800
申请日：1992-06-26
申请人： Gary W. Skeels , Diane M. Chapman , Edith M. Flanigen
发明人： Gary W. Skeels , Diane M. Chapman , Edith M. Flanigen
IPC分类号： B01J29/04 , B01J29/89 , C01B39/06 , C01B39/24 , C01B39/26 , C01B39/32 , C01B33/34
CPC分类号： B01J29/046 , B01J29/04 , C01B33/2884 , Y10S423/21 , Y10S423/25 , Y10S423/26 , Y10S423/28
摘要： Molecular sieve compositions are prepared by extracting aluminum and substituting chromium and/or tin for extracted aluminum to give molecular sieve products containing framework chromium and/or tin atoms. The process of preparing the chromium and/or tin-containing molecular sieves involves contacting a starting molecular sieve with a solution or slurry of at least one of a fluoro salt of chromium or a fluoro salt of tin under effective process conditions to provide for aluminum extraction and substitution of chromium and/or tin.
摘要翻译：通过提取铝并用铬和/或锡代替提取的铝制备分子筛组合物，得到含有骨架铬和/或锡原子的分子筛产物。制备含铬和/或锡的分子筛的方法包括在有效的工艺条件下使起始分子筛与铬的氟盐或锡的氟盐中的至少一种的溶液或浆料接触以提供铝提取以及铬和/或锡的取代。

92. 发明授权

US5348924A Zeolite aggregates and catalysts 失效
标题翻译：沸石骨料和催化剂
公开(公告)号：US5348924A
公开(公告)日：1994-09-20
申请号：US23733
申请日：1993-02-23
申请人： Mark J. Potter , Jar-Lin Kao , Virginia R. Cross , Thomas H. Vanderspurt , Edward K. Dienes , Robert E. Riley , Freddie L. Tungate , Arie Bortinger
发明人： Mark J. Potter , Jar-Lin Kao , Virginia R. Cross , Thomas H. Vanderspurt , Edward K. Dienes , Robert E. Riley , Freddie L. Tungate , Arie Bortinger
IPC分类号： B01J29/06 , B01J20/18 , B01J29/068 , B01J29/60 , B01J29/62 , B01J29/89 , B01J29/90 , B01J37/00 , C01B39/00 , C01B39/02 , C01B39/04 , C01B39/10 , C01B39/22 , C01B39/24 , C01B39/26 , C01B39/32 , C01B39/38 , C10G35/095 , B01J29/04
CPC分类号： B01J37/0009 , B01J20/186 , B01J29/60 , B01J29/62 , B01J29/90 , C10G35/095 , B01J2229/36
摘要： A process for producing zeolite aggregates involves providing a formable paste composed of zeolite, a binder composed of an organic/metal oxide containing aluminum, a peptizing agent and water; forming the paste into an aggregate, preferably by extruding into an extrudate; curing the aggregate; hydro-thermally calcining the aggregate; and washing the hydro-thermally calcined aggregate with a washing medium, preferably followed by rinsing with a rinsing medium to remove residual washing medium from the aggregate. The washed and rinsed aggregate may then be permitted to equilibrate or is subjected to a drying procedure. Preferably, the washed and rinsed aggregate is again subjected to curing/hydro-thermal calcining. The resultant aggregates, such as extrudates, have an exterior surface with openings and interstitial spaces between particles of binder and zeolite which communicate by such openings between the exterior surface of the aggregate and micropores of the zeolite; the aggregates also exhibit characteristics of crush strength greater than about 0.9 pounds per millimeter and a loss by attrition of less than about 3.0%. Regenerable catalysts, such as reforming catalysts, based on such aggregate also exhibit a catalyst activity pass through to the zeolite bound in the aggregate of at least 70% of the initial catalyst activity of freshly prepared zeolite, as well as exhibiting more than about 70% of the reforming benzene yield that the reforming catalyst exhibited when similarly tested prior to being exposed to a hydrocarbon stream under specified reforming conditions of the catalyst activity test procedures.
摘要翻译：一种生产沸石聚集体的方法包括提供由沸石组成的可成形糊料，由含铝的有机/金属氧化物，胶溶剂和水组成的粘合剂; 将所述糊料形成为聚集体，优选通过挤出成型为挤出物; 固化骨料; 水热煅烧骨料; 并用洗涤介质洗涤加热热煅烧的聚集体，优选随后用冲洗介质冲洗以从聚集体中除去残余的洗涤介质。然后可以洗涤和漂洗的骨料平衡或进行干燥过程。优选地，洗涤和漂洗的骨料再次进行固化/水热煅烧。所得到的聚集体，例如挤出物，具有在粘合剂和沸石颗粒之间具有开口和间隙的外表面，该孔与沸石的外表面和沸石的微孔之间的这种开口连通; 聚集体还具有大于约0.9磅/毫米的压碎强度的特征，并且损耗小于约3.0％。基于这种骨料的可再生催化剂，如重整催化剂，也表现出催化剂活性通过沸石结合的沸石，其为新制备的沸石的初始催化剂活性的至少70％，并显示大于约70％的重整苯产率，当在催化剂活性测试程序的特定重整条件下暴露于烃流之前，类似地测试重整催化剂显示。

93. 发明授权

US5242675A Zeolite L 失效
标题翻译：沸石L
公开(公告)号：US5242675A
公开(公告)日：1993-09-07
申请号：US825408
申请日：1992-01-24
申请人： Johannes P. Verduijn
发明人： Johannes P. Verduijn
IPC分类号： B01J29/60 , C01B39/32 , C07C5/22 , C07C5/41 , C07C15/00 , C10G35/095
CPC分类号： C10G35/095 , B01J29/60 , C01B33/2884 , C01B39/32 , C07C5/226 , C07C5/417 , B01J2229/26 , B01J2229/42 , C07C2529/62 , Y10S423/28
摘要： Zeolite L with flat basal planes, and reduced crystallite size is prepared in a synthesis modified by the addition of small amounts of additional metal such as magnesium, calcium, barium, cobalt, zinc, chromium, manganese or nickel. The addition of these metals also suppresses unwanted zeolite W formation even when the synthesis would otherwise form this zeolite.
摘要翻译：通过加入少量附加金属如镁，钙，钡，钴，锌，铬，锰或镍改性的合成中制备具有平坦基面的沸石L和还原的微晶尺寸。这些金属的添加也抑制不希望的沸石W形成，即使合成否则将形成该沸石。

94. 发明授权

US5051387A Zeolite L preparation 失效
标题翻译：沸石L制备
公开(公告)号：US5051387A
公开(公告)日：1991-09-24
申请号：US440150
申请日：1989-11-22
申请人： Wicher T. Koetsier , Johannes P. Verduijn
发明人： Wicher T. Koetsier , Johannes P. Verduijn
IPC分类号： B01J29/00 , B01J29/52 , B01J29/60 , B01J29/61 , B01J29/62 , C01B39/06 , C01B39/32 , C07B61/00 , C07C1/00 , C07C5/22 , C07C5/32 , C07C5/393 , C07C5/41 , C07C15/00 , C07C67/00
CPC分类号： C01B39/32 , B01J29/60 , C07C5/226 , C07C5/415 , C07C2529/62
摘要： Zeolite L with cylindrical morphology and having excellent properties as a catalyst base may be prepared with high crystallinity and reduced contamination even in large scale syntheses were fluctuation in gel compositions may occur by employing a gel composition having the following molar ratios of components:2.64-2.67 M.sub.2/n O:Al.sub.2 O.sub.3 :8.8-9.7 SiO.sub.2 :145-160 H.sub.2 Owhere M is a cation of valence n, especially potassium. The ratio M.sub.2/n O:SiO.sub.2 is preferably at least 0.275.
摘要翻译：具有圆柱形态并具有优异性能的催化剂基团的沸石L可以以高结晶度和甚至在大规模合成中降低的污染物制备，因此通过使用具有以下摩尔比的组分的凝胶组合物可能发生凝胶组合物的波动：2.64-2.67 M2 / nO：Al2O3：8.8-9.7SiO2：145-160H2O，其中M是价数n，特别是钾的阳离子。比率M2 / nO：SiO2优选为至少0.275。

95. 发明公开

KR1020080031261A 배향성 제올라이트 물질 및 그에 대한 생성 방법 无效
标题翻译：面向沸石的材料及其制造方法
公开(公告)号：KR1020080031261A
公开(公告)日：2008-04-08
申请号：KR1020087000425
申请日：2006-07-28
申请人： 유니버시태트 베른
发明人： 칼자페리,기온 , 사발라,루이스,아란사수 , 리,후안룽 , 후버,스테판
IPC分类号： C01B39/32 , B32B9/00 , H01L31/0216 , H01L31/0232
CPC分类号： H01L51/447 , Y02E10/542 , Y02E10/549 , Y10T156/1092 , Y10T428/24322
摘要： An oriented zeolite material comprises a plurality of zeolite crystals (2) arranged on a substrate (4), each one of said crystals having a proximal face (6) adjacent to said substrate and a distal face (8) opposed therefrom and substantially parallel to said proximal face. Each one of said crystals has a plurality of straight through uniform channels (10) extending between the proximal face and the distal face and having a channel axis parallel to and a channel width transverse to a longitudinal crystal axis A. Each channel has a proximal channel end (12) located at the proximal face and a distal channel end (14) located at the distal face, and each crystal is attached to the substrate by means of a linking layer (16) that substantially occludes the proximal channel ends.
摘要翻译：定向沸石材料包括布置在基底（4）上的多个沸石晶体（2），所述晶体中的每一个具有邻近所述基底的近端面（6）和与其相对的远侧面（8），并且基本上平行于说近端面。所述晶体中的每一个具有在近端面和远端面之间延伸的多个直通的均匀通道（10），并且具有平行于纵向晶轴A的通道轴线和通道宽度。每个通道具有近端通道位于近端面处的端部（12）和位于远端面处的远端通道端部（14），并且每个晶体通过基本上封闭近端通道端部的连接层（16）附接到基板。

96. 发明授权

KR100512573B1 제올라이트 엘 제조방법 失效
标题翻译： ZEOLITE L的制备
公开(公告)号：KR100512573B1
公开(公告)日：2005-09-06
申请号：KR1020007013005
申请日：1998-05-20
申请人： 셰브런 유.에스.에이.인크.
发明人： 스티븐,제이.밀러
IPC分类号： C01B39/32
摘要： 오직 제올라이트 L을 제조하기에 충분한 수분만을 포함한 반응혼합물로부터 결정성 알루미노실리케이트 제올라이트 L을 제조하는 방법이 개시되어 있다. 본 구현예에 있어서, 반응혼합물은 자가지지(self-supporting)적이며, 원하는 형태로 성형될 수 있다. 본 발명의 방법은 결정화조건하에 외부로부터 첨가된 액상이 존재하지 않는 조건하에서 반응혼합물이 가열되고, 이로인하여 결정물을 건조시키기 이전에 결정화 생성물로부터 과량의 유체를 제거할 필요가 없는 특징이 있다.

97. 发明授权

KR100157638B1 제올라이트 L 失效
标题翻译：沸石-L
公开(公告)号：KR100157638B1
公开(公告)日：1998-12-15
申请号：KR1019920701008
申请日：1990-10-30
申请人： 엑손 리써치 앤드 엔지니어링 컴파니
发明人： 요하네스페트루스베르두이즌
IPC分类号： B01J29/60 , C01B39/32
CPC分类号： C10G35/095 , B01J29/60 , B01J29/62 , C01B39/32 , C07C5/387 , C07C5/41 , C07C2529/62 , Y02P20/52 , C07C15/04
摘要： 촉매가 하키퍽 또는 동전 모양의 매우 편평한 원통체인 L형 칼륨 제올라이트는 K
2 O/SiO
2 및 SiO
2 /Al
2 O
3 의 비를 조절하고 제올라이트가 결정화되는 혼합물에 소량의 2가양이온, 예를들면 마그네슘 또는 바륨을 포함시키므로써 제조할 수 있다. 생성된 제올라이트는 짧은 채널 길이를 가지며, 방향족화 촉매에 대한 기재로서 특히 유용하다.

98. 发明公开

KR1019920703202A 제올라이트 L 失效
标题翻译：沸石L
公开(公告)号：KR1019920703202A
公开(公告)日：1992-12-17
申请号：KR1019920701008
申请日：1990-10-30
申请人： 엑손 리써치 앤드 엔지니어링 컴파니
发明人： 요하네스페트루스베르두이즌
IPC分类号： B01J29/60 , C01B39/32

99. 发明申请

WO2008052603A1 METHOD FOR THE PREPARATION OF MICRO-POROUS CRYSTALS AND CONJUGATES THEREOF 审中-公开
标题翻译：微孔晶体的制备及其结合方法
公开(公告)号：WO2008052603A1
公开(公告)日：2008-05-08
申请号：PCT/EP2007/005811
申请日：2007-06-29
申请人： ROCHE DIAGNOSTICS GMBH , F. HOFFMANN-LA ROCHE AG , UNIVERSITÄT BERN , POPOVIC, Zoran , TSOTSALAS, Manuel, Matthias , BUSBY, Michael , DE COLA, Luisa , CALZAFERRI, Gion , JOSEL, Hans-Peter
发明人： POPOVIC, Zoran , TSOTSALAS, Manuel, Matthias , BUSBY, Michael , DE COLA, Luisa , CALZAFERRI, Gion , JOSEL, Hans-Peter
IPC分类号： C01B39/32 , C09K11/06 , G01N21/64 , G01N23/223 , G01N24/08 , G01N29/02
CPC分类号： G01N33/533 , G01N33/582
摘要： A conjugate comprising a dye-labeled microporous crystal, a stop-cock moiety, and covalently bound thereto an affinity binding agent is disclosed. The dye-labeled microporous crystal is a zeolite crystal, such as a zeolite L crystal, having a large number of channels in its interior into which the dye is loaded. The stop-cock moiety can be functionalized with an amino group to which a carboxyester group can be attached. The affinity binding agent allows for the binding to a biological moiety. The conjugate of the moiety can be used in in-vivo and/or in-vitro imaging applications.
摘要翻译：公开了包含染料标记的微孔结晶，停止旋塞部分并与其共价结合的亲和力结合剂的缀合物。染料标记的微孔结晶是沸石晶体，例如沸石L晶体，其内部具有大量通道，染料加载到其中。停止旋塞部分可以与可以连接羧基酯基团的氨基官能化。亲和力结合剂允许结合生物部分。该部分的缀合物可用于体内和/或体外成像应用。

100. 发明申请

WO02036490A1 DYE LOADED ZEOLITE MATERIAL 审中-公开
标题翻译： DYE加载沸石材料
公开(公告)号：WO02036490A1
公开(公告)日：2002-05-10
申请号：PCT/CH2001/000647
申请日：2001-11-05
IPC分类号： B01J39/14 , C09K11/06 , G01Q30/20 , H01L51/30 , C01B39/42 , B01J29/04 , C01B39/00 , C01B39/32
CPC分类号： C09K11/06 , B01J20/3204 , B01J39/14 , B82Y15/00 , H01L51/005 , H01L51/0064 , H01L51/0069 , H01L51/0071 , H01L51/008 , H01L51/447 , Y02E10/549
摘要： The present invention provides a dye loaded zeolite material comprising: a) at least one zeolite crystal having straight through uniform channels each having a channel axis parallel to, and a channel width transverse to, a c-axis of crystal unit cells; b) closure molecules having an elongated shape and consisting of a head moiety and a tail moiety, the tail moiety having a longitudinal extension of more than a dimension of the crystal unit cells along the c-axis and the head moiety having a lateral extension that is larger than said channel width and will prevent said head moiety from penetrating into a channel; c) a channel being terminated, in generally plug-like manner, at least at one end thereof located at a surface of the zeolite crystal by a closure molecule hose tail moiety penetrates into said chanel and whose head moiety substantially occludes said channel end while projecting over said surface; and d) an essentially linear arrangement of luminescent dye molecules enclosed within a terminated channel adjacent to at least one closure molecule and exhibiting properties related to supramolecular organization.
摘要翻译：本发明提供一种负载染料的沸石材料，包括：a）至少一种具有直通均匀通道的沸石晶体，每个通道均具有平行于晶体单元晶胞的c轴的沟道轴线和沟道宽度; b）具有细长形状并由头部部分和尾部部分组成的封闭分子，所述尾部部分具有比c轴更多的晶体单位细胞尺寸的纵向延伸，并且头部部分具有侧向延伸，大于所述通道宽度，并且将防止所述头部部分穿透通道; c）通常通过塞子状方式终止位于沸石晶体的表面的通道，封闭分子软管尾部穿透到所述香烟中，并且其头部基本上封闭所述通道端，同时突出在所述表面上; 以及d）包封在与至少一个封闭分子相邻的封端通道中并且显示与超分子组织相关的性质的发光染料分子的基本线性排列。

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