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91. 发明申请

US20100111816A1 INORGANIC PARTICLE-CONTAINING EMULSION AND MANUFACTURING METHOD OF A PARTICLE BY USING THE INORGANIC PARTICLE-CONTAINING EMULSION 审中-公开
标题翻译：无机颗粒包含乳液和使用含有无机颗粒的乳液制备颗粒的方法
公开(公告)号：US20100111816A1
公开(公告)日：2010-05-06
申请号：US12532755
申请日：2008-02-21
申请人： Koji Aga , Hiromichi Kobayashi
发明人： Koji Aga , Hiromichi Kobayashi
IPC分类号： C01B31/14
CPC分类号： C09C3/041 , B01F17/0007 , C01P2006/10 , C01P2006/12 , C04B35/2625 , C04B35/2633 , C04B35/6263 , C04B35/6264 , C04B2235/3206 , C04B2235/3213 , C04B2235/3262 , C09C1/3009 , C09C1/3018 , C09C1/3623 , C09C1/48 , C09C1/56 , C09C3/04
摘要： The invention aims at providing an inorganic particle-containing emulsion which enables further size reduction of particles and can bring about a mono-disperse system and an enhanced yield and a manufacturing method of a particle by the use of the emulsion. This aim can be performed by a water in oil emulsion prepared by mixing an oil phase liquid and an water phase liquid which contains inorganic particles under agitation, in which the water phase liquid contains inorganic particle having a specific gravity of 1.5 to 11 g/cm3 and 0.5 to 5 wt % of agar-agar as calculated by taking the quantity of water contained in the water phase liquid as 100 wt % and the oil phase liquid contains hydrophobic particles as a dispersion stabilizer and in which the water phase liquid is present as the dispersion phase of the water in oil emulsion with the inorganic particles dispersed in the organic particle-containing emulsion; and a manufacturing method of a particle which contains both inorganic particle and agar-agar by the use of the emulsion.
摘要翻译：本发明的目的在于提供一种能够进一步减小颗粒的无机颗粒乳液，并且可以通过使用该乳液产生单分散体系和增加产率以及颗粒的制造方法。该目的可以通过在搅拌下混合油相液体和含有无机粒子的水相液体制备的油包水乳液进行，其中水相液体含有比重为1.5〜11g / cm 3的无机粒子和0.5〜5重量％的琼脂，通过将水相液体中所含的水量取为100重量％计算，油相液体含有疏水性颗粒作为分散稳定剂，其中水相液体以油包水乳液中的分散相与无机颗粒分散在含有机颗粒的乳液中; 以及通过使用乳液来同时含有无机粒子和琼脂的颗粒的制造方法。

92. 发明申请

US20090081304A1 Composite pigment nanoparticles and processes to form organic-inorganic nanoparticle composite particles 审中-公开
标题翻译：复合颜料纳米粒子和形成有机 - 无机纳米颗粒复合颗粒的方法
公开(公告)号：US20090081304A1
公开(公告)日：2009-03-26
申请号：US11903522
申请日：2007-09-21
申请人： Lye Han Valerie Choy , Shivkumar Chiruvolu , Nobuyuki Kambe , Vladimir K. Dioumaev , Hui Du , Shinichi Kuramoto , Hiroto Higuchi
发明人： Lye Han Valerie Choy , Shivkumar Chiruvolu , Nobuyuki Kambe , Vladimir K. Dioumaev , Hui Du , Shinichi Kuramoto , Hiroto Higuchi
IPC分类号： A61K9/14 , C09B67/20 , B02C23/18
CPC分类号： C09B67/0002 , A61K9/143 , B82Y30/00 , C01G23/047 , C01P2004/03 , C01P2004/04 , C01P2004/51 , C01P2004/64 , C01P2004/84 , C09B67/0097 , C09C1/3018 , C09C1/3054 , C09C1/3623 , C09C1/3661
摘要： Milling approaches provide for the efficient formation of composite particles having an inorganic nanoparticle core with an organic coating composition. The nanoparticles can additionally function as a milling media or distinct milling particles can be used and later separated from the product composite particles. In general, the milling is performed in the presence of a dispersing agent that facilitates dispersing of the composite particles in a carrier liquid. The processes described herein can be effectively used in the formation of composite particles comprising organic pigments. Similarly, the composite particles can be formed with other organic compounds, such as organic pharmaceutical compositions.
摘要翻译：研磨方法提供了有机形成具有无机纳米颗粒核心的复合颗粒和有机涂层组合物。纳米颗粒可另外用作研磨介质，或者可以使用不同的研磨颗粒，并且随后从产物复合颗粒中分离。通常，在有助于将复合颗粒分散在载体液体中的分散剂的存在下进行研磨。本文所述的方法可以有效地用于形成包含有机颜料的复合颗粒。类似地，复合颗粒可以与其它有机化合物如有机药物组合物形成。

93. 发明申请

US20070199479A1 RUTILE-BASED PIGMENT AND A METHOD FOR THE PRODUCTION THEREOF 失效
标题翻译：基于颜色的颜料及其生产方法
公开(公告)号：US20070199479A1
公开(公告)日：2007-08-30
申请号：US11676804
申请日：2007-02-20
申请人： Rainer Heubach
发明人： Rainer Heubach
IPC分类号： C09C1/36
CPC分类号： C09C1/0084 , B02C17/16 , B02C17/20 , B02C17/22 , C01P2002/30 , C01P2002/52 , C01P2004/51 , C01P2004/53 , C01P2004/62 , C01P2004/80 , C01P2006/80 , C09C1/0096 , C09C1/34 , C09C1/36 , C09C1/3623 , C09C3/041
摘要： The invention relates to a fine-particle, bright and high-coating rutile-based pigment that is devoid of any metal or reactive metal compounds relevant to mill abrasion detectable by application technology but whose grain-size in terms of particle diameters ranges from 50 to 1000 μm, for mono-, bi-, tri- or oliho-modal size distribution and a primary maximum ranges from 230 to 400 μm, wherein optionally for a bi- or poly-modal frequency distribution, a secondary maximum is less than 25% of the primary maximum between 400 and 1000 μm. The method for producing said pigment consists in treating an organic mixed-phase rutile structured oxide pigment by high-speed grinding in suspension in a ball grinding mill provided with a mechanically and chemically resistant coating until said grain-size and a substantially isometric rounded particle shape are attained. According to the invention, means for viscosity adjustment and surface conditioning of the pigment are also provided. The inventive pigment differs from prior art by improved brightness, low whiteness or low lightness, relatively high hue saturation and by extremely high covering power which is not obtainable in said class of products up to now and exhibits a low photoactivity with respect to known fine-particle rutiles. In practice no abrasivity, neither interaction of possible grinding residues with an application matrix is observed.
摘要翻译：本发明涉及一种微粒，光亮和高涂层的金红石型颜料，其没有任何金属或反应性金属化合物，其与通过应用技术可检测到的研磨磨损相关，但是其粒径在粒径范围为50至 1000μm，用于单，双，三或模式尺寸分布，初级最大值范围为230-400μm，其中任选地对于双模或多模态频率分布，二次最大值小于25％最大的最大值在400到1000之间。制备所述颜料的方法在于通过在具有机械和化学防腐涂层的球磨机中悬浮高速研磨来处理有机混合相金红石结构氧化物颜料，直到所述晶粒尺寸和基本上等长的圆形颗粒形状达到了。根据本发明，还提供了用于颜料的粘度调节和表面调节的方法。本发明的颜料与现有技术不同，通过改进的亮度，低白度或低亮度，相对高的色相饱和度以及迄今为止在所述类别的产品中不可获得的非常高的覆盖功率，并且相对于已知的细小颜料显示出低的光活性，颗粒金红石。在实践中没有磨蚀性，也没有观察到可能研磨残留物与应用基质的相互作用。

94. 发明授权

US07238231B1 Process for manufacturing zirconia-treated titanium dioxide pigments 有权
标题翻译：氧化锆处理的二氧化钛颜料的制造方法
公开(公告)号：US07238231B1
公开(公告)日：2007-07-03
申请号：US11600643
申请日：2006-11-16
申请人： Daniel H. Craig , Jeffrey D. Elliott , Harmon E. Ray
发明人： Daniel H. Craig , Jeffrey D. Elliott , Harmon E. Ray
IPC分类号： C09C3/06 , C09C1/36 , C01G23/047 , C01G23/07 , B05D7/00
CPC分类号： C09C1/3661 , C01G23/07 , C01P2004/84 , C09C1/3623 , C09C1/363 , C09C1/3692
摘要： An improved process is described for manufacturing zirconia-treated titanium dioxide pigments, wherein the zirconia treatment is accomplished in the process of fluidizing a titanium dioxide filter or press cake and then drying the same, through the addition to the filter or press cake of one or more alkaline water-soluble zirconium reagents selected from ammonium zirconyl carbonate, the water-soluble ammonium zirconyl carboxylates and mixtures of these. Aqueous solutions of such zirconium reagents, in addition to being effective for imparting a zirconia surface treatment to the titanium dioxide materials, also prove to be effective fluidizing agents for forming high solids dispersions of the zirconia-treated titanium dioxide pigment materials which can be spray dried without substantial dilution and excessive energy requirements.
摘要翻译：描述了用于制造氧化锆处理的二氧化钛颜料的改进方法，其中氧化锆处理在使二氧化钛过滤器或压滤饼流化并随后将其干燥的过程中通过添加到过滤器或压滤饼选自碳酸锆铵，水溶性锆酸锆酸酯及其混合物的更碱性的水溶性锆试剂。这种锆试剂的水溶液除了有效地对二氧化钛材料进行氧化锆表面处理外，还被证明是有效的流化剂，用于形成可被喷雾干燥的氧化锆处理的二氧化钛颜料的高固体分散体没有显着的稀释和过多的能量需求。

95. 发明申请

US20060045841A1 Process for making titanium dioxide and resulting product 审中-公开
标题翻译：制备二氧化钛和所得产品的方法
公开(公告)号：US20060045841A1
公开(公告)日：2006-03-02
申请号：US10928387
申请日：2004-08-30
申请人： Daniel Craig , Jeffrey Elliott , George Perakis , Harmon Ray
发明人： Daniel Craig , Jeffrey Elliott , George Perakis , Harmon Ray
IPC分类号： C09C1/36
CPC分类号： C08J3/20 , C08J3/226 , C08J2423/00 , C09C1/3623 , C09C1/363 , C09C1/3692
摘要： A process is disclosed for making titanium dioxide pigment particularly suited for dispersion in thermoplastics, in which the titanium dioxide pigment is recoverable from a slurry through the use of conventional vacuum-type and/or pressure-type filtration systems without the deposition of additional inorganic oxides and in the absence of added flocculating agents, and further in which the thus-recovered, washed and filtered pigment can be dried by spray drying, without the dilution required in the production of such pigments according to a prior art process likewise omitting the deposition of additional inorganic oxides to those formed in a vapor phase oxidation step providing the agglomerated titanium dioxide starting material and omitting any use of added flocculating agents.
摘要翻译：公开了一种制备二氧化钛颜料特别适于分散在热塑性塑料中的方法，其中通过使用常规的真空型和/或压力型过滤系统可从浆料中回收二氧化钛颜料，而不沉积另外的无机氧化物并且在没有添加的絮凝剂的情况下，并且其中如此回收的洗涤和过滤的颜料可以通过喷雾干燥而干燥，而不需要根据现有技术方法生产这种颜料所需的稀释，同样省略了提供在气相氧化步骤中形成的无机氧化物，提供附聚的二氧化钛原料，并省略任何使用的添加的絮凝剂。

96. 发明申请

US20060042512A1 Surface-treated pigments 审中-公开
标题翻译：表面处理颜料
公开(公告)号：US20060042512A1
公开(公告)日：2006-03-02
申请号：US10928439
申请日：2004-08-30
申请人： Daniel Craig
发明人： Daniel Craig
IPC分类号： C09C1/36
CPC分类号： C09C1/3623 , C01P2004/62 , C09C1/3661 , C09C1/3669 , C09C1/3692 , C09C3/006 , C09C3/063 , C09C3/08 , Y10T428/2991
摘要： Inorganic pigments, having deposited on the pigment surface at least one hydroxy group-functionalized saturated fatty acid, possess improved processibility and dispersibility in thermoplastic materials, and impart improved properties to thermoplastic compositions containing said surface-treated pigments.
摘要翻译：在颜料表面上沉积至少一种羟基官能化的饱和脂肪酸的无机颜料具有改进的热塑性材料的加工性和分散性，并赋予包含所述表面处理颜料的热塑性组合物改善的性能。

97. 发明申请

US20050228112A1 Titanium dioxide pigment and method for producing the same and resin composition using the same 有权
标题翻译：二氧化钛颜料及其制造方法及使用其的树脂组合物
公开(公告)号：US20050228112A1
公开(公告)日：2005-10-13
申请号：US10523589
申请日：2003-08-06
申请人： Hideo Takahashi , Toshihiko Akamatsu , Kazuhiro Tominaga , Taku Katou , Yoshio Nagai , Yoshitaka Muraki , Yukako Ota
发明人： Hideo Takahashi , Toshihiko Akamatsu , Kazuhiro Tominaga , Taku Katou , Yoshio Nagai , Yoshitaka Muraki , Yukako Ota
IPC分类号： C01G23/053 , C08K3/22 , C09C1/36 , C09D7/12
CPC分类号： C09C1/3623 , C01G23/0532 , C01P2004/62 , C01P2006/60 , C01P2006/62 , C08K3/22 , C08K9/02 , C08K9/04 , C08K2003/2241 , C09C1/3607 , C09C1/3661 , C09D7/61 , C09D7/62 , C09D7/68
摘要： The titanium dioxide pigment of the present invention contains an anatase type crystal in an amount of 98-100% and has an average particle diameter of 0.2-0.4 μm and a whiteness of 95-97 in terms of L value of linseed oil. The titanium dioxide pigment of the present invention has characteristics peculiar to anatase type, for example, optical characteristics such as bluish color tone and physical characteristics such as low hardness, and furthermore has high opacity which is not possessed by conventional anatase type titanium oxide pigments.
摘要翻译：本发明的二氧化钛颜料含有98-100％的锐钛矿型结晶，平均粒径为0.2-0.4μm，白度为95-97，以亚麻子油的L值计。本发明的二氧化钛颜料具有锐钛矿型特有的特性，例如蓝色调的光学特性和低硬度等物理特性，而且还具有高透明度，这是常规锐钛矿型氧化钛颜料所不具有的。

98. 发明申请

US20030236317A1 Titanium oxide dispersion composition, and method and container for preserving the same 失效
标题翻译：氧化钛分散体组合物及其保存方法和容器
公开(公告)号：US20030236317A1
公开(公告)日：2003-12-25
申请号：US10456746
申请日：2003-06-09
申请人： SUMITOMO CHEMICAL COMPANY, LIMITED
发明人： Yoshiaki Sakatani , Kensen Okusako , Hironobu Koike
IPC分类号： C01G023/02
CPC分类号： C09C1/3669 , B01J21/063 , B01J35/0013 , B01J35/004 , B65D81/30 , C01G23/0532 , C01P2002/84 , C09C1/3623 , Y10T428/13 , Y10T428/1352
摘要： A titanium oxide dispersion composition is provides, the composition comprising a solvent and a titanium oxide with an average secondary particle diameter of 100 nm or smaller, the dispersion composition having a maximum intensity within the range of from 435 nm to 700 nm of a primary differential spectrum of a transmittance spectrum, wherein the transmittance spectrum is measured using an ultraviolet-visible spectrophotometer after adjusting a solid content of the dispersion composition to be about 2% by weight. The composition provides a film having a high hydrophilicity under the irradiation of a visible light.
摘要翻译：提供二氧化钛分散体组合物，所述组合物包含平均二次粒径为100nm以下的溶剂和氧化钛，所述分散组合物的初级微分子的最大强度在435nm〜700nm的范围内透射光谱的光谱，其中在将分散组合物的固体含量调节至约2重量％之后，使用紫外 - 可见分光光度计测量透射光谱。该组合物在可见光的照射下提供具有高亲水性的膜。

99. 发明授权

US5824146A Method for making a photodurable aqueous titanium dioxide pigment slurry using a high level of aluminum co-oxidant 失效
标题翻译：使用高水平的铝助氧化物制造可光化水溶性二氧化钛颜料浆料的方法
公开(公告)号：US5824146A
公开(公告)日：1998-10-20
申请号：US888083
申请日：1997-07-03
申请人： Michael Warren Ott
发明人： Michael Warren Ott
IPC分类号： C09D17/00 , C09C1/36
CPC分类号： C09C1/3623 , C09C1/3607 , C01P2004/50 , C01P2004/60 , C01P2004/82 , C01P2006/22 , C01P2006/60 , C01P2006/80
摘要： This invention relates to a new method for making a photodurable, aqueous titanium dioxide (TiO.sub.2) pigment slurry. This method involves reacting titanium tetrachloride, aluminum chloride and an oxygen-containing gas in the presence of a nucleant in the vapor phase to produce TiO.sub.2 pigment. A sufficient amount of aluminum chloride is added to provide at least 2 wt. % alumina in the TiO.sub.2 pigment. The TiO.sub.2 pigment is separated from the reaction gases; and mixed with sufficient water to produce a TiO.sub.2 slurry comprising at least 78 wt. % TiO.sub.2 solids. The slurry may be used in coating formulations such as paints.
摘要翻译：本发明涉及制备可光化的水性二氧化钛（TiO 2）颜料浆料的新方法。该方法包括在蒸气相中的成核剂存在下使四氯化钛，氯化铝和含氧气体反应，生成TiO 2颜料。加入足够量的氯化铝以提供至少2重量％％二氧化钛颜料中的氧化铝。 TiO 2颜料与反应气体分离; 并与足够的水混合以产生包含至少78wt。％TiO2固体。浆料可以用于涂料配方如油漆中。

100. 发明授权

US5733365A Process for preparing an improved low-dusting, free-flowing pigment 失效
公开(公告)号：US5733365A
公开(公告)日：1998-03-31
申请号：US801656
申请日：1997-02-18
申请人： John E. Halko , Phillip M. Story , James W. Kauffman , Kelly A. Green
发明人： John E. Halko , Phillip M. Story , James W. Kauffman , Kelly A. Green
IPC分类号： C08K9/04 , C09C1/36 , C09C3/04 , C09C3/08 , C09D7/12
CPC分类号： C09C1/3661 , C08K9/04 , C09C1/3623 , C09C1/3669 , C09C3/08 , C09D7/1225 , C01P2004/51 , C01P2004/61 , C01P2004/80 , C01P2006/11 , C01P2006/20 , C01P2006/40 , C01P2006/80 , C01P2006/82 , C01P2006/90 , C08K3/22
摘要： A process for preparing a low-dusting, free-flowing pigment which has not been subjected to any micronizing treatment comprising the steps of providing an inorganic pigment material; providing a source of water; forming a fine, well dispersed slurry of the pigment and water; milling the slurry; depositing a treating agent having the formula ROOCCHSO.sub.3 MCH.sub.2 COOR' wherein R and R' are monovalent alkyl radicals having from about 2 to about 20 carbon atoms, and M is a metallic monovalent cation on the slurried milled pigment; and drying the pigment material having a treating agent deposited thereon. The invention also provides the free-flowing pigments produced by this process.

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