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    • 91. 发明授权
    • Shielded tip access tube for a reactor probe
    • 用于反应器探针的屏蔽提示通道
    • US3846080A
    • 1974-11-05
    • US22075372
    • 1972-01-26
    • TEXACO INC
    • MACLEAN JJONES H
    • B01J8/24B01J8/26G01K1/08B01J9/20B01J11/04
    • B01J8/1809B01J8/26B01J2208/0007B01J2208/00539B01J2208/00548B01J2208/00584B01J2208/0061G01K1/08
    • 1. IN A REGENERATOR FOR A FLUIDIZED CATALYST WHEREIN THE PARTICULATED CATALYST MATERIAL IS CIRCULATED WITHIN A REGENERATION COMPARTMENT HAVING VERTICAL WALLS, IN A TURBULENT FLOW BY A CARRIER GAS TO FORM A FLUIDIZED BED, AND WHEREIN THE CONDITION OF SAID FLUIDIZED BED IS REGULATED TO MAINTAIN PREDETERMINED OPERATING CONDITIONS THEREIN, THE IMPROVEMENT FOR CONTINUOUSLY MONITORING THE PRESSURE WITHIN SAID FLUIDIZED BED COMPRISING, A CONDUIT EXTENDING INTO SAID REGENERATOR COMPARTMENT AND HAVING AN OPEN END DISPOSED IN SAID FLUIDIZED CATALYST BED, THE OTHER END OF SAID CONDUIT COMMUNICATED WITH A SOURCE OF A PURGE GAS, A PRESSURE SENSING ELEMENT CONNECTED TO SAID CONDUIT, AND IN COMMUNICATION WITH SAID REGENERATION COMPARTMENT, A SHEILD DISPOSED ABOUT SAID CONDUIT OPEN END DEFINING A CHAMBER IN COMMUNICATION WITH SAID FLUIDIZED BED WHEREBY TO RECEIVE THE FLUIDIZED CATALYST AS WELL AS PURGE GAS AT THE CONDUIT OPEN END, SAID SHEILD INCLUDING A CYLINDRICAL ELEMENT HAVING A PERFORATED WALL SPACED FROM SAID CONDUIT OPEN, END, THEREBY DEFINING AN ANNULUS ABOUT THE CONDUIT, AND A SUBSTANTIALLY FLAT PERFORATED FACE PLATE AT THE END OF SAID CYLINDRICAL SHEILD ELEMENT TO DEFINE A PARTIAL CLOSURE TO THE LATTER ADJACENT TO SAID CONDUIT OPEN END, SAID FACE PLATE BEING DISPOSED IN A PLANE SUBSTANTIALLY PARALLEL TO THE VERTICAL WALLS OF SAID REGENERATION COMPARTMENT.

      D R A W I N G
    • 92. 发明授权
    • Device for testing vertical tubes in a chemical reactor
    • 用于在化学反应器中测试垂直管的装置
    • US09500631B2
    • 2016-11-22
    • US14277845
    • 2014-05-15
    • Extundo Incorporated
    • Clifford L. JohnsDaniel D. Sympson
    • B08B9/093G01N33/00B01J8/00B01J8/06B01J19/00G01L19/08
    • G01N33/0004B01J8/001B01J8/008B01J8/06B01J19/0073B01J2208/0007B01J2208/00539B01J2208/00584B01J2208/00654B01J2208/00769B01J2208/00805B01J2219/002B01J2219/00213B01J2219/0024G01L19/083G01L19/086
    • Method for calibrating a device for measuring back pressure in open-ended chemical reactor tubes, comprising the steps of: providing a device for measuring back pressure in open-ended chemical reactor tubes, including a frame member and a plurality of injector tubes mounted on the frame member with a spacing between the injector tubes; providing a test stand, comprising a frame member; a base supporting said frame member; and a plurality of calibration tubes mounted on the frame member, each of said calibration tubes having an open top and a dosed bottom, with a precision orifice in the dosed bottom to simulate the chemical reactor tubes to be tested; inserting the plurality of injector tubes into the respective calibration tubes; sealing between the injector tubes and the calibration tubes; sending gas through the injector tubes and taking a back pressure reading for each of the injector tubes; and generating correction factors for each injector tube to correct for variations in the back pressure readings.
    • 用于校准用于测量开放式化学反应器管中的背压的装置的方法,包括以下步骤:提供用于测量开放式化学反应器管中的背压的装置,包括框架构件和安装在所述壳体上的多个注射器管 框架构件,其在注射器管之间具有间隔; 提供测试台,包括框架构件; 支撑所述框架构件的基座; 以及安装在所述框架构件上的多个校准管,每个所述校准管具有敞开的顶部和定量的底部,在所述定量的底部具有精确的孔,以模拟待测试的化学反应器管; 将多个注射器管插入相应的校准管中; 注射器管和校准管之间的密封; 通过注射管输送气体并对每个注射器管采取背压读数; 并产生每个注射管的校正因子,以校正背压读数的变化。
    • 93. 发明申请
    • METHOD FOR MAXIMIZING THE REACTION VOLUME IN A SLURRY PHASE REACTOR
    • 用于最大化浆液相反应器中的反应体积的方法
    • US20160012207A1
    • 2016-01-14
    • US14758315
    • 2014-01-22
    • ENI S.p. A.
    • Alberto Maria Antonio MALANDRINOVincenzo PICCOLO
    • G06F19/00G01B21/02G01B21/00
    • B01J8/22B01J8/1809B01J2208/00584B01J2219/002B01J2219/00209B01J2219/00243B01J2219/0025H01L21/67276
    • Method for maximizing the reaction volume in a slurry phase reactor by determining the ratio (f) between the height of the foams (Hf) and the height of the reactor (HR) through an algorithm defining the gas hold-up in three zones, a first lower zone in which a bubble regime is established, a second intermediate zone where there can be the presence of foams, a third zone situated in the upper hemispherical part in which the multiphase mixture is accelerated until it reaches outlet conditions, the average gas hold-up being given by the weighted average of each of the three gas hold-ups of the three zones, characterized in that it uses nuclear densimeters positioned inside the reactor at different heights and comprises: measuring, for each nuclear densimeter used, gas density values, relating to different gas and/or slurry velocities, which correspond through said algorithm to calculated gas hold-up values, revealing, with a calculated gas hold-up of less than 40%, the absence of foams at least up to the height at which the densimeter is positioned, whose density measured corresponds to said gas hold-up, with a calculated gas hold-up higher than 70%, the presence of foams starting at least from the height of the reactor in which the densimeter is positioned, whose density measured corresponds to said gas hold-up, finally, determining through said algorithm, the ratio f and the extension in height of the possible presence of foams, calculating the consequent height Hf.
    • 通过确定三个区域中的气体滞留的算法,通过确定泡沫(Hf)的高度与反应器的高度(HR)之间的比率(f)来最大化淤浆相反应器中的反应体积的方法, 建立气泡状态的第一下部区域,可能存在泡沫的第二中间区域,位于上半球部分中的第三区域,多相混合物加速到其中,直到达到出口条件,平均气体保持 由三个区域的三个气体滞留量中的每一个的加权平均值给出,其特征在于,其使用位于反应器内部的不同高度的核密度计,并且包括:对于使用的每个核密度计,测量气体密度值 ,涉及不同的气体和/或浆料速度,其通过所述算法对应于计算的气体滞留值,显示在计算的气体滞留小于40%时,在 至少直到密度计位于的高度,其测量的密度对应于所述气体滞留,计算的气体滞留高于70%,泡沫的存在至少从反应器的高度开始,其中 密度计定位,其密度测量对应于所述气体滞留,最后,通过所述算法确定比率f和可能存在泡沫的高度的延伸,计算随之而来的高度Hf。
    • 96. 发明授权
    • Method and system for determining catalyst activity
    • 测定催化剂活性的方法和系统
    • US07904271B2
    • 2011-03-08
    • US12281572
    • 2007-03-06
    • Daniel SirauxAlain Brusselle
    • Daniel SirauxAlain Brusselle
    • G01N9/00A61L2/00C08F2/00G01F1/00C08F4/00
    • B01J19/1856B01J8/0015B01J8/20B01J19/1837B01J19/1862B01J19/2435B01J2208/00584B01J2208/00752B01J2219/00173Y10S526/919
    • The present invention relates to a method for determining activity of a catalyst in a polymerization process, said polymerization process comprising the steps of feeding a catalyst and a diluent into a storage vessel, to form a concentrated settled catalyst, feeding said concentrated settled catalyst into a mixing vessel equipped with mixing means and feeding hydrocarbon diluent into said mixing vessel, to form a diluted catalyst slurry, feeding said diluted catalyst slurry into a polymerization reactor via a volumetric pump, and feeding at least one monomer into said polymerization reactor to form a polymer. The method is characterized in that density of the diluted catalyst slurry is measured between an outlet of the mixing vessel and the volumetric pump, the amount of catalyst fed into the polymerization reactor is determined based on the measured density of the diluted catalyst slurry, and the amount of catalyst fed into the polymerization reactor is compared to the amount of the polymer formed to determine the activity of the catalyst. The invention also relates to a system suitable for carrying out the method.
    • 本发明涉及一种在聚合过程中测定催化剂活性的方法,所述聚合方法包括以下步骤:将催化剂和稀释剂进料到储存容器中,以形成浓缩的沉降催化剂,将所述浓缩沉淀催化剂加入到 配备有混合装置的混合容器和将烃稀释剂进料到所述混合容器中以形成稀释的催化剂浆料,通过容积泵将所述稀释的催化剂浆料进料到聚合反应器中,并将至少一种单体进料到所述聚合反应器中以形成聚合物 。 该方法的特征在于,在混合容器的出口和容积泵之间测量稀释的催化剂浆料的密度,基于测量的稀释的催化剂浆料的密度来确定进料到聚合反应器中的催化剂的量, 将进料到聚合反应器中的催化剂的量与形成的聚合物的量进行比较以确定催化剂的活性。 本发明还涉及一种适于实施该方法的系统。