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91. 发明授权

US4170576A Uses of mixtures of alpha methyl styrene dimers and terpene dimers in perfumery processes and products 失效
标题翻译：在香料工艺和产品中使用α甲基苯乙烯二聚体和萜烯二聚体的混合物
公开(公告)号：US4170576A
公开(公告)日：1979-10-09
申请号：US923183
申请日：1978-07-10
申请人： John B. Hall , Wilhelmus J. Wiegers , Ira D. Hill , Robert M. Novak , Frederick L. Schmitt
发明人： John B. Hall , Wilhelmus J. Wiegers , Ira D. Hill , Robert M. Novak , Frederick L. Schmitt
IPC分类号： A23L27/00 , C07C2/04 , C07C2/42 , C07C13/465 , C11B9/02 , C11B9/00
CPC分类号： C11B9/02 , A23L27/70 , C07C13/465 , C07C2/04 , C07C2/42 , C07C2102/08 , C07C2521/16
摘要： A process is described for providing clear extended compositions of essential oils which comprises a composition of an essential oil and an extender material miscible with said essential oil which does not appreciably alter the aroma of the essential oil insofar as its quality or strength is concerned, the proportion of essential oil in extender material being from about 70% up to about 99%, said extender material being a mixture of (A) a dimerization product of an alpha methyl styrene or a methyl or other C.sub.2 -C.sub.4 lower alkyl homologue thereof or mixture of same, and (B) one or more "dimerization" (or "coupling") products of one or more terpenes which are monocyclic and have two carbon-carbon double bonds or which are bicyclic and have one carbon-carbon double bond or one or more hydrogenated derivatives thereof or mixtures of same.
摘要翻译：描述了一种用于提供精油的清晰延长组合物的方法，其包含精油和与所述精油混溶的增量剂材料的组合物，其不会明显地改变其质量或强度的香精的香味，增量材料中精油的比例为约70％至约99％，所述增量材料是（A）α-甲基苯乙烯或其甲基或其它C 2 -C 4低级烷基同系物的二聚产物或混合物的混合物和（B）一种或多种单环单体并具有两个碳 - 碳双键或双环并具有一个碳 - 碳双键的一个或多个萜烯的“二聚”（或“偶联”）产物或一种或更多的氢化衍生物或其混合物。

92. 发明授权

US4476147A Flavoring of alliaceous-flavored foodstuffs 失效
标题翻译：调味多味食品
公开(公告)号：US4476147A
公开(公告)日：1984-10-09
申请号：US542477
申请日：1983-10-17
申请人： John B. Hall , James M. Sanders , James N. Siano
发明人： John B. Hall , James M. Sanders , James N. Siano
IPC分类号： A24B15/32 , C07C29/40 , C07C33/02 , C07C45/54 , C07C45/67 , C07C45/75 , C07C49/203 , C11D3/50 , A23L1/226
CPC分类号： C11D3/50 , A24B15/32 , C07C29/40 , C07C33/02 , C07C45/54 , C07C45/67 , C07C45/75 , C07C49/203
摘要： A process for augmenting or enhancing the aroma or taste of alliaceous flavors, particularly garlic flavors, by augmenting or enhancing the garlic and green aroma and taste nuances of alliaceous-flavored foodstuffs comprising the step of adding to a alliaceous-flavored foodstuff an aroma or taste augmenting quantity of a mixture of cis and trans isomers of a compound having the structure: ##STR1## wherein the wavy lines indicate both cis and trans juxtaposition of the hydrogen and methallyl moieties about the carbon-carbon double bond.
摘要翻译：通过增加或增强多种风味食品的大蒜和绿色香气和味道的细微差别来增强或增强多种风味香料，特别是蒜味的香气或味道的方法，其包括向三味风味食品中加入香味或味道具有以下结构的化合物的顺式和反式异构体的混合物的增加量：其中波浪线表示氢和甲代烯丙基部分围绕碳 - 碳双键的顺式和反式并置。

93. 发明授权

US4560499A Isosolanone and solanone intermediates and organoleptic uses 失效
标题翻译： Isosolanone和solanone中间体和感官用途
公开(公告)号：US4560499A
公开(公告)日：1985-12-24
申请号：US609349
申请日：1984-06-22
申请人： John B. Hall , James M. Sanders , James N. Siano
发明人： John B. Hall , James M. Sanders , James N. Siano
IPC分类号： A24B15/32 , C07C29/40 , C07C33/02 , C07C45/54 , C07C45/67 , C07C45/75 , C07C49/203 , C11D3/50 , C11B9/00
CPC分类号： C11D3/50 , A24B15/32 , C07C29/40 , C07C33/02 , C07C45/54 , C07C45/67 , C07C45/75 , C07C49/203 , C07C67/03
摘要： Described is a novel genus of compounds defined according to the structure: ##STR1## wherein Z represents hydrogen, MgX and the moiety having the structure: ##STR2## and X represents chloro, bromo or iodo; as well as the novel compounds defined according to the structures: ##STR3## and mixtures of same shown according to the structure: ##STR4## wherein the wavy lines indicate both cis and trans juxtaposition of the hydrogen and methallyl moieties about the carbon-carbon double bond; uses of same as intermediates in a process for producing isosolanone which is a mixture of compounds having the structures: ##STR5## or shown by the single structure: ##STR6## and solanone which is a mixture of compounds having the structures: ##STR7## or shown by the structure: ##STR8## wherein the wavy lines are indicative of a cis or trans juxtaposition of the hydrogen or 2-propenyl moieties about the double bond; and organoleptic uses of the compounds having the structures: ##STR9##
摘要翻译：描述了根据以下结构定义的化合物的新颖属性：其中Z表示氢，MgX和具有以下结构的部分：其中X表示氯，溴或碘; 以及根据以下结构定义的新颖化合物：根据以下结构显示的相同的结构：其中波浪线表示氢和甲代烯丙基部分在碳 - 碳双键上的顺式和反式并置键; 在作为制备具有以下结构的化合物的混合物的方法中使用与中间体的相同的化合物：具有以下结构的化合物：或者由单一结构显示：作为化合物的混合物，其具有以下结构：或由以下结构示出：其中波浪线表示在双键上的氢或2-丙烯基部分的顺式或反式并置; 和具有以下结构的化合物的感官用途：

94. 发明授权

US4609754A Process for the production of isosolanone and solanone, intermediates useful in said process and organoleptic uses of said intermediates 失效
标题翻译：用于生产异溶胶酮和溶胶酮的方法，可用于所述方法的中间体和所述中间体的感官用途
公开(公告)号：US4609754A
公开(公告)日：1986-09-02
申请号：US609348
申请日：1984-06-22
申请人： John B. Hall , James M. Sanders , James N. Siano
发明人： John B. Hall , James M. Sanders , James N. Siano
IPC分类号： A24B15/32 , C07C29/40 , C07C33/02 , C07C45/54 , C07C45/67 , C07C45/75 , C07C49/203 , C11D3/50 , C07C69/72
CPC分类号： C11D3/50 , A24B15/32 , C07C29/40 , C07C33/02 , C07C45/54 , C07C45/67 , C07C45/676 , C07C45/75 , C07C49/203 , C07C67/03 , C07C69/72
摘要： Described is a novel genus of compounds defined according to the structure: ##STR1## wherein Z represents hydrogen, MgX and the moiety having the structure: ##STR2## and X represents chlor, bromo, or iodo; as well as 5-isopropyl-8-methyl-5,8-nonadien-2-one; uses of same as intermediates in a process for producing isosolanone and solanone; and organoleptic uses of 5-isopropyl-8-methyl-5,8-nonadien-2-one and 2,6-dimethyl-5-methylene-1-hepten-4-ol.The novel process of our invention involved the steps of:(i) formation of the compound having the structure: ##STR3## by means of reacting 3-methyl-2-methylenebutanal with the compound having the structure: ##STR4## (ii) acid hydrolysis of the resulting compound in order to form 2,6-dimethyl-5-methylene-1-heptene-4-ol;(iii) reaction of 2,6-dimethyl-5-methylene-1-hepten-4-ol with methyl aceto acetate in order to form 2,6-dimethyl-5-methylene-1-hepten-4-yl aceto acetate or, directly, 5-isopropyl-8-methyl-5,8-nonadiene-2-one;(iv) reacting 2,6-dimethyl-5-methylene-1-hepten-4-yl aceto acetate in the presence of an appropriate catalyst to form the 5-isopropyl-8-methyl-5,8-nonadiene-2-one; and(v) isomerizing the 5-isopropyl-8-methyl-5,8-nonadien-2-one in order to form a mixture of solanone and the isosolanone or 5-isopropyl-8-methyl-5,8-nonadiene-2-one.
摘要翻译：描述了根据以下结构定义的化合物的新颖属性：其中Z表示氢，MgX和具有以下结构的部分：＆lt; IMAGE＆gt; X表示氯，溴或碘; 以及5-异丙基-8-甲基-5,8-壬二烯-2-酮; 在制备异山芋酮和solanone的方法中使用与中间体相同的物质; 和5-异丙基-8-甲基-5,8-壬二烯-2-酮和2,6-二甲基-5-亚甲基-1-庚烯-4-醇的感官用途。本发明的新方法涉及以下步骤：（i）通过使3-甲基-2-亚甲基丁醛与具有以下结构的化合物反应形成具有以下结构的化合物：（ⅱ）酸水解所得化合物以形成2,6-二甲基-5-亚甲基-1-庚烯-4-醇; （iii）2,6-二甲基-5-亚甲基-1-庚烯-4-醇与乙酰乙酸甲酯的反应，以形成2,6-二甲基-5-亚甲基-1-庚烯-4-基乙酸乙酯或直接得到5-异丙基-8-甲基-5,8-壬二烯-2-酮; （iv）使2,6-二甲基-5-亚甲基-1-庚烯-4-基乙酸乙酯在合适的催化剂存在下反应，形成5-异丙基-8-甲基-5,8-壬二烯-2-酮 ; 和（v）异构化5-异丙基-8-甲基-5,8-壬二烯-2-酮，以形成Solone和二异丙基酮或5-异丙基-8-甲基-5,8-壬二烯-2-酮的混合物 -一。

95. 发明授权

US4433695A Process for the production of isosolanone and solanone, intermediates useful in said process and organoleptic uses of said intermediates 失效
标题翻译：用于生产异溶胶酮和溶胶酮的方法，可用于所述方法的中间体和所述中间体的感官用途
公开(公告)号：US4433695A
公开(公告)日：1984-02-28
申请号：US380542
申请日：1982-05-20
申请人： John B. Hall , James M. Sanders , James N. Siano
发明人： John B. Hall , James M. Sanders , James N. Siano
IPC分类号： A24B15/32 , C07C29/40 , C07C33/02 , C07C45/54 , C07C45/67 , C07C45/75 , C07C49/203 , C11D3/50 , A24B3/12
CPC分类号： C11D3/50 , A24B15/32 , C07C29/40 , C07C33/02 , C07C45/54 , C07C45/67 , C07C45/676 , C07C45/75 , C07C49/203 , C07C67/03
摘要： A process for augmenting or enhancing the aroma or taste of a smoking tobacco or smoking tobacco article comprising the step of adding to a smoking tobacco or smoking tobacco article component, an aroma or taste augmenting or enhancing quantity of a mixture of cis and trans isomers of a compound having the structure: ##STR1## wherein the wavy lines represent cis or trans juxtaposition of the hydrogen and 2-methyl-1-propenyl moieties around the carbon-carbon double bond.
摘要翻译：一种用于增强或增强吸烟烟草或吸烟烟草制品的香气或味道的方法，其包括向吸烟烟草或烟草制品组分添加香味或味道增加或增加量的顺式和反式异构体混合物的步骤具有以下结构的化合物：其中波浪线代表碳 - 碳双键周围的氢和2-甲基-1-丙烯基部分的顺式或反式并置。

96. 发明授权

US4535192A Tertiary pentamethylindanol derivatives and organoleptic uses thereof 失效
公开(公告)号：US4535192A
公开(公告)日：1985-08-13
申请号：US671330
申请日：1984-11-14
申请人： John B. Hall , Takao Yoshida
发明人： John B. Hall , Takao Yoshida
IPC分类号： A24B15/34 , C07C35/23 , C07C35/32 , C11B9/00 , C11D3/50
CPC分类号： C11D3/50 , A24B15/345 , C07C35/23 , C07C35/32 , C11B9/0049
摘要： Described are tertiary pentamethylindanol derivatives defined according to the structure: ##STR1## wherein the dashed line represents a carbon-carbon single bond or a carbon-carbon double bond and uses thereof in augmenting or enhancing the aroma or taste of consumable materials selected from the group consisting of perfume compositions, colognes, perfumed articles, foodstuffs, smoking tobaccos and smoking tobacco compositions.

97. 发明授权

US4131557A Soap composition 失效
标题翻译：肥皂组成
公开(公告)号：US4131557A
公开(公告)日：1978-12-26
申请号：US847210
申请日：1977-10-31
申请人： John B. Hall , Wilhelmus J. Wiegers
发明人： John B. Hall , Wilhelmus J. Wiegers
IPC分类号： C07C37/14 , C07C39/17 , C11B9/00 , C11D9/44
CPC分类号： C07C37/14 , C11B9/0046 , C07C2102/42
摘要： Described is a soap composition containing as a key ingredient, a mixture of compounds having a sandalwood aroma produced according to a process which comprises:(1) Reacting catechol with camphene in the presence of a Friedel Crafts Catalyst to form a first alkylation product; and then(2) Treating said first alkylation product with hydrogen in the presence of a hydrogenation catalyst, thus forming, initially, diol intermediates and then, on continuing the hydrogenation, the mixture useful in the perfume compositions of our invention.
摘要翻译：描述了含有作为关键成分的皂组合物，根据以下方法制备的具有檀香香气的化合物的混合物，其包含：

98. 发明授权

US4115406A 2-Alkyl-4-phenyl-dihydropyrans and processes for augmenting the organoleptic properties of foodstuffs and tobacco using one or more of said pyrans 失效
标题翻译： 2-烷基-4-苯基 - 二氢吡喃，以及使用一种或多种所述吡喃葡萄糖增强食品和烟草的感官特性的方法
公开(公告)号：US4115406A
公开(公告)日：1978-09-19
申请号：US847094
申请日：1977-10-31
申请人： Joaquin Francisco Vinals , Jacob Kiwala , Denis E. Hruza, Sr. , John B. Hall , Manfred Hugo Vock
发明人： Joaquin Francisco Vinals , Jacob Kiwala , Denis E. Hruza, Sr. , John B. Hall , Manfred Hugo Vock
IPC分类号： A24B15/40 , C07D309/18 , C11B9/00 , C07D309/04
CPC分类号： A24B15/403 , C07D309/18 , C11B9/008
摘要： Described is the novel compound group, 2-alkyl-4-phenyl-dihydropyrans having the generic structure: ##STR1## where one of the dashed lines is a carbon-carbon double bond and the other of the dashed lines is a carbon-carbon single bond, R.sup.1 is one of C.sub.1 -C.sub.3 alkyl, and R is one of C.sub.2 -C.sub.4 alkyl, a process for producing same; a process comprising adding to tobacco an amount sufficient to augment the flavor or aroma of such tobacco of one or more of said pyran compounds; flavor formulations for use in conjunction with tobacco products containing one or more of such pyrans; a process comprising adding to foodstuffs, foodstuff flavorings, chewing gums, chewing gum flavorings, toothpaste and toothpaste flavorings one or more of said pyran compounds in a quantity sufficient to augment or enhance neroli-like and grape-like flavors, and flavoring compositions containing said pyran compounds.
摘要翻译：描述了具有以下通用结构的新化合物基团2-烷基-4-苯基 - 二氢吡喃：其中虚线之一是碳 - 碳双键，另一条虚线是碳 - 碳单键键，R1是C1-C3烷基之一，R是C 2 -C 4烷基之一，其生产方法; 一种方法，其包括向烟草中加入足以增加一种或多种所述吡喃化合物的烟草的风味或香气的量; 与含有一种或多种这种吡喃的烟草制品一起使用的风味制剂; 包括向食品，食品调味剂，口香糖，口香糖调味剂，牙膏和牙膏调味剂中添加足以增加或增强橙花状和葡萄状调味剂的一种或多种所述吡喃化合物的方法，以及含有所述吡喃化合物。

99. 发明授权

US4104203A Perfume compositions containing catechol-camphene reaction products 失效
标题翻译：含有儿茶酚camp烯反应产物的香料组合物
公开(公告)号：US4104203A
公开(公告)日：1978-08-01
申请号：US846960
申请日：1977-10-31
申请人： John B. Hall , Wilhelmus Johannen Wiegers
发明人： John B. Hall , Wilhelmus Johannen Wiegers
IPC分类号： C07C37/14 , C07C39/17 , C11B9/00
CPC分类号： C07C37/14 , C11B9/0046 , C07C2102/42
摘要： Described is a novel perfume material and cologne containing as a key ingredient a mixture of compounds having a sandalwood aroma prepared by a process which comprises:(1) Reacting catechol with camphene in the presence of a Friedel Crafts Catalyst to form a first alkylation product; and then(2) Treating said first alkylation product with hydrogen in the presence of a hydrogenation catalyst, thus forming, initially, diol intermediates and then, on continuing the hydrogenation, the mixture useful in the perfume compositions of our invention.
摘要翻译：描述了一种新颖的香水材料和古龙水，其包含通过以下方法制备的具有檀香香气的化合物的混合物的混合物，该方法包括：

100. 发明授权

US4070491A 2-Alkyl-4-phenyl-dihydropyrans and processes for augmenting the organoleptic properties of foodstuffs and tobacco using one or more of said pyrans 失效
标题翻译： 2-烷基-4-苯基 - 二氢吡喃，以及使用一种或多种所述吡喃葡萄糖增强食品和烟草的感官特性的方法
公开(公告)号：US4070491A
公开(公告)日：1978-01-24
申请号：US780641
申请日：1977-03-23
申请人： Joaquin Francisco Vinals , Jacob Kiwala , Denis E. Hruza, Sr. , John B. Hall , Manfred Hugo Vock
发明人： Joaquin Francisco Vinals , Jacob Kiwala , Denis E. Hruza, Sr. , John B. Hall , Manfred Hugo Vock
IPC分类号： A23G4/00 , A23G4/06 , A23L27/20 , A24B15/40 , C07D309/18 , A23L1/235
CPC分类号： A23G4/06 , A23L27/2052 , A24B15/403 , C07D309/18
摘要： Described is the novel compound group, 2-alkyl-4-phenyl-dihydropyrans having the generic structure: ##STR1## where one of the dashed lines is a carbon-carbon double bond, R.sup.1 is one of C.sub.1 -C.sub.3 alkyl, and R is one of C.sub.2 -C.sub.4 alkyl, a process for producing same; a process comprising adding to tobacco an amount sufficient to augment the flavor or aroma of such tobacco of one or more of said pyran compounds; flavor formulations for use in conjunction with tobacco products containing one or more of such pyrans; a process comprising adding to foodstuffs, foodstuff flavorings, chewing gums, chewing gum flavorings, toothpaste and toothpaste flavorings one or more of said pyran compounds in a quantity sufficient to augment or enhance neroli-like and grape-like flavors, and flavoring compositions containing said pyran compounds.
摘要翻译：描述了具有以下一般结构的新化合物基团2-烷基-4-苯基 - 二氢吡喃：其中一条虚线为碳 - 碳双键，R1为C1-C3烷基之一，R为 C 2 -C 4烷基之一，其制备方法; 一种方法，其包括向烟草中加入足以增加一种或多种所述吡喃化合物的烟草的风味或香气的量; 与含有一种或多种这种吡喃的烟草制品一起使用的风味制剂; 包括向食品，食品调味剂，口香糖，口香糖调味剂，牙膏和牙膏调味剂中添加足以增加或增强橙花状和葡萄状调味剂的一种或多种所述吡喃化合物的方法，以及含有所述吡喃化合物。

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