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91. 发明授权

US5132478A Alkylaromatic lubricant fluids 失效
标题翻译：烷基芳族润滑剂流体
公开(公告)号：US5132478A
公开(公告)日：1992-07-21
申请号：US629946
申请日：1990-12-19
申请人： Suzzy C. Ho , Margaret M. Wu
发明人： Suzzy C. Ho , Margaret M. Wu
IPC分类号： C10M105/06 , C10M105/16 , C10M105/18 , C10M127/06 , C10M129/10
CPC分类号： C10M105/18 , C10M105/06 , C10M105/16 , C10M127/06 , C10M129/10 , C10M2203/06 , C10M2207/023 , C10M2207/025 , C10M2207/04 , C10M2207/046 , C10M2207/144 , C10M2207/146 , C10M2207/284 , C10M2207/285 , C10M2211/024 , C10M2211/042 , C10M2211/06 , C10M2215/06 , C10M2215/062 , C10M2215/08 , C10M2215/082 , C10M2215/202 , C10M2215/28 , C10M2219/086 , C10M2219/087 , C10M2219/089 , C10M2223/041 , C10M2223/045 , C10N2240/10 , C10N2240/101 , C10N2240/104 , C10N2240/106
摘要： Aromatic compounds are alkylated with C.sub.20 -C.sub.1300 olefinic oligomers using an acidic alkylation catalyst to produce alkylated aromatic products, usually alkylaromatic hydrocarbons. The olefinic oligomers used as alkylating agents are prepared from 1-alkene oligomerization in contact with reduced metal oxide catalyst, preferably reduced chromium oxide on a silica support. The alkylated aromatic hydrocarbons retain the unique features of the alkylating olefinic oligomer and exhibit high viscosity index and low pour point. If the alkylation is carried out under certain combinations of conditions, especially using a Lewis acid catalysts such as aluminum trichloride and at higher temperatures, the alkyl portion of the product will undergo isomerization. The alkylaromatic compositions show improved thermal stability and are useful as lubricant basestocks and additives for improved antiwear properties, antioxidant and other properties.
摘要翻译：使用酸性烷基化催化剂将芳族化合物与C20-C1300烯属低聚物烷基化以产生烷基化芳族产物，通常为烷基芳烃。用作烷基化剂的烯烃低聚物由与还原的金属氧化物催化剂，优选在二氧化硅载体上还原的氧化铬接触的1-烯烃低聚制备。烷基化芳烃保留了烷基化烯属低聚物的独特特征，并表现出高粘度指数和低倾点。如果烷基化在某些条件组合下进行，特别是使用路易斯酸催化剂如三氯化铝，并且在较高的温度下，产物的烷基部分将进行异构化。烷基芳族组合物显示出改善的热稳定性，并且可用作润滑剂基础油料和用于改善抗磨损性能，抗氧化剂和其它性能的添加剂。

92. 发明授权

US5132477A Process for producing alkylaromatic lubricant fluids 失效
标题翻译：生产烷基芳族润滑剂流体的方法
公开(公告)号：US5132477A
公开(公告)日：1992-07-21
申请号：US693161
申请日：1991-04-29
申请人： Suzzy C. Ho , Bruce P. Pelrine , Margaret M. Wu
发明人： Suzzy C. Ho , Bruce P. Pelrine , Margaret M. Wu
IPC分类号： B01J23/26 , B01J27/12 , B01J27/125 , B01J31/02 , C07B61/00 , C07C2/10 , C07C2/66 , C07C11/02 , C07C15/00 , C07C15/02 , C07C15/20 , C08F4/06 , C08F4/22 , C08F10/00 , C10M105/04 , C10M105/06 , C10M127/02 , C10M171/00 , C10N20/02 , C10N20/04 , C10N30/02 , C10N70/00
CPC分类号： C07C15/00 , C07C2/10 , C10M105/06 , C10M171/002 , C07C2521/08 , C07C2523/26 , C10M2203/06 , C10M2205/00 , C10M2205/028 , C10N2220/02 , C10N2240/02 , C10N2240/04 , C10N2240/042 , C10N2240/044 , C10N2240/046
摘要： The thermal and oxidative stability of HVI-PAO olefin oligomers is improved by reaction of the oligomerization mixture containing the olefin oligomer, dimer and isomerized but unoligomerized olefin with an aromatic compound such as toluene, xylene or naphthalene. The reaction is carried out in the presence of an acidic catalyst, which may be heterogeneous solid catalyst such as an acidic clay or a crystalline zeolite such as MCM-22, a homogeneous Friedel-Crafts catalyst such as AlCl.sub.3, BF.sub.3 or their complexes or a supported catalyst such as AlCl.sub.3 on graphite or silica. The reaction improves the yield and thermal stability of the lube range products. The olefinic oligomer mixture which is reacted with the aromatic compound is prepared from 1-alkene oligomerization in contact with a reduced metal oxide, preferably reduced chromium oxide, catalyst on support such as silica.

93. 发明授权

US5055626A Novel lubricants 失效
标题翻译：新型润滑剂
公开(公告)号：US5055626A
公开(公告)日：1991-10-08
申请号：US471454
申请日：1990-01-29
申请人： Suzzy C. Ho , Margaret M. Wu
发明人： Suzzy C. Ho , Margaret M. Wu
IPC分类号： C07C2/48 , C10G50/02 , C10M105/06
CPC分类号： C10M105/06 , C07C2/48 , C10G50/02 , C07C2521/08 , C07C2523/26 , C07C2523/28 , C07C2523/30 , C10M2203/06
摘要： Alkylaromatic lubricant products are produced by the reaction of a long chain alkyne such as octyne, decyne or dodecyne over a reduced Group VIB metal oxide catalyst, preferably reduced chromium on silica. The products, which are predominantly n-alkyl substituted, possess excellent thermal and oxidative stability and may be used as lubricant base stocks and viscosity improvers.
摘要翻译：烷基芳族润滑剂产物通过长链炔烃如辛炔，癸炔或十二炔与还原的VIB族金属氧化物催化剂反应制备，优选在二氧化硅上还原的铬。主要为正烷基取代的产品具有优异的热和氧化稳定性，可用作润滑剂基础油和粘度改进剂。

94. 发明授权

US4990711A Synthetic polyolefin lubricant blends having high viscosity indices 失效
标题翻译：具有高粘度指数的合成聚烯烃润滑剂共混物
公开(公告)号：US4990711A
公开(公告)日：1991-02-05
申请号：US210436
申请日：1988-06-23
申请人： Catherine S. H. Chen , Margaret M. Wu
发明人： Catherine S. H. Chen , Margaret M. Wu
IPC分类号： C10G71/00 , C10G50/02 , C10M169/04 , C10N20/00 , C10N20/02 , C10N20/04 , C10N30/02 , C10N60/02 , C10N70/00
CPC分类号： C10M169/041 , C10G2400/10 , C10M2203/0206 , C10M2205/024 , C10M2205/0245 , C10M2205/026 , C10M2205/0265 , C10M2205/028 , C10N2220/02
摘要： Compositions and methods of preparation for a lubricant mixture having enhanced viscosity index comprising:(a) a low viscosity C.sub.20 -C.sub.60 lubricant range liquid comprising substantially linear hydrocarbons prepared by shape selective catalysis of lower olefin with medium pore acid zeolite catalyst to provide substantially linear liquid olefinic intermediates or C.sub.20.sup.+ hydrogenated lubricants, said lubricant range liquid having a kinematic viscosity of about 2-10 cS at 100.degree. C.; and(b) at least one poly(alpha-olefin) having viscosity greater than 20 cS and viscosity index improvement properties.
摘要翻译：制备具有增强的粘度指数的润滑剂混合物的组合物和方法包括：（a）低粘度C20-C60润滑剂范围液体，其包含基本上直链的烃，其通过下式烯烃与中孔酸沸石催化剂的形状选择性催化制备，以提供基本上线性的液体烯烃中间体或C20 +氢化润滑剂，所述润滑剂范围液体在100℃下的运动粘度为约2-10cS。和（b）至少一种粘度大于20cS的聚（α-烯烃）和粘度指数改进性能。

95. 发明授权

US4926004A Regeneration of reduced supported chromium oxide catalyst for alpha-olefin oligomerization 失效
标题翻译：用于α-烯烃低聚的还原的负载型铬氧化物催化剂的再生
公开(公告)号：US4926004A
公开(公告)日：1990-05-15
申请号：US282362
申请日：1988-12-09
申请人： Bruce P. Pelrine , Margaret M. Wu
发明人： Bruce P. Pelrine , Margaret M. Wu
IPC分类号： B01J23/92 , B01J38/12 , C07C2/10
CPC分类号： B01J38/12 , B01J23/92 , C07C2/10 , C07C2521/08 , C07C2523/26 , Y02P20/584
摘要： A process for producing liquid oligomers useful as lubricants from alpha-olefins feedstock, such as 1-decene. The olefins are oligomerized over a supported and reduced metal oxide catalyst from Group VIB of the Periodic Table to produce the oligomers. The chromium-on-silica oligomerization catalysts can be regenerated to allow repeated recycling of the catalyst with reduced losses in yield of the lubricant. The regeneration process is particularly useful to regenerate catalyst deactivated during the course of oligomerization at high temperatures to produce low viscosity HVI-PAO lubricant. The regeneration process is carried out by (i) purging the deactivated catalyst with inert gas to strip unreacted olefin and lubricant product; (ii) contacting the purged catalyst with a stream of oxidizing gas at an elevated temperature to oxidize the carbonaceous deposits; and (iii) cooling the catalyst and contacting it with a stream of reducing gas to reduce the metal component to a lower valence state.
摘要翻译：用于生产由α-烯烃原料如1-癸烯用作润滑剂的液体低聚物的方法。烯烃在元素周期表VIB的负载和还原的金属氧化物催化剂上低聚，以产生低聚物。可以再生铬 - 二氧化硅低聚催化剂，以允许反复循环使用催化剂，同时减少润滑剂的产率损失。再生过程特别有用于在低温反应过程中在高温下再生催化剂失活以产生低粘度HVI-PAO润滑剂。再生过程是通过（i）用惰性气体净化去活化的催化剂以除去未反应的烯烃和润滑剂产物; （ii）在高温下使被吹扫的催化剂与氧化气体流接触以氧化碳质沉积物; 和（iii）冷却催化剂并将其与还原气体流接触以将金属组分降低至更低的化合价态。

96. 发明授权

US4827064A High viscosity index synthetic lubricant compositions 失效
标题翻译：高粘度指数合成润滑剂组合物
公开(公告)号：US4827064A
公开(公告)日：1989-05-02
申请号：US210435
申请日：1988-06-23
申请人： Margaret M. Wu
发明人： Margaret M. Wu
IPC分类号： C10G50/02 , C10M143/08 , C07C2/08 , C07C9/22
CPC分类号： C10G50/02 , C10M143/08 , C10M2205/00 , C10M2205/028 , C10N2220/02
摘要： Novel lubricant compositions comprising polyalphaolefins are disclosed having high viscosity indices with low pour point. The compositions are characterized by a uniform molecular structure with low branch ratios. The invention describes a liquid lubricant composition comprising C.sub.30 -C.sub.1300 hydrocarbons, said composition having a branch ratio of less than 0.19, weight average molecular weight between 300 and 45,000 number average molecular weight between 300 and 18,000, molecular weight distribution between 1 an 5 and pour point below -15.degree. C. 1-decene trimer comprising 9-methyl, 11-octylheneicosane and 11-octyldocosane is disclosed.
摘要翻译：公开了包含聚α-烯烃的新型润滑剂组合物，具有低倾点的高粘度指数。组合物的特征在于具有低分支比的均匀分子结构。本发明描述了一种包含C30-C1300烃的液体润滑剂组合物，所述组合物的分支比小于0.19，重均分子量在300和45,000之间，数均分子量在300和18,000之间，分子量分布在1和5之间，低于-15℃。公开了包含9-甲基，11-辛基二十二烷和11-辛基二十二烷的1-癸烯三聚体。

97. 发明授权

US4580000A Selective sorption of n-alkylbenzene from a mixture containing n-alkyl and sec-alkyl benzenes 失效
标题翻译：从含有正烷基和仲烷基苯的混合物中选择性吸附正烷基苯
公开(公告)号：US4580000A
公开(公告)日：1986-04-01
申请号：US687393
申请日：1984-12-28
申请人： Margaret M. Wu
发明人： Margaret M. Wu
IPC分类号： C07C2/66 , C07C7/13 , C07C15/085 , C07C7/12 , B01J8/44
CPC分类号： C07C15/085 , C07C2/66 , C07C7/13 , C07C2529/70
摘要： There is provided a method for the selective sorption of n-alkylbenzene, such as n-propylbenzene, from an alkylbenzene mixture, such as a mixture of n-propylbenzene and isopropylbenzene, with an oxide impregnated ZSM-5 sorbent. This method may be particularly useful in the purification of cumene product streams.
摘要翻译：提供了一种从烷基苯混合物（如正丙基苯和异丙基苯的混合物）与氧化物浸渍的ZSM-5吸附剂选择性吸附正烷基苯（如正丙基苯）的方法。该方法在异丙苯产物流的纯化中可能特别有用。

98. 发明授权

US4471150A Catalysts for light olefin production 失效
标题翻译：用于轻烯烃生产的催化剂
公开(公告)号：US4471150A
公开(公告)日：1984-09-11
申请号：US521639
申请日：1983-08-10
申请人： Margaret M. Wu
发明人： Margaret M. Wu
IPC分类号： B01J29/50 , B01J29/70 , B01J29/74 , B01J29/78 , C07C1/20 , C07C1/00
CPC分类号： B01J29/78 , B01J29/50 , B01J29/70 , B01J29/74 , C07C1/20 , B01J2229/20 , B01J2229/26 , B01J2229/42 , C07C2521/10 , C07C2523/34 , C07C2523/42 , C07C2529/50 , C07C2529/54 , C07C2529/70 , C07C2529/74 , Y02P20/52 , Y02P30/42
摘要： Modified zeolite catalyst compositions comprising a crystalline aluminosilicate zeolite having pore windows formed by 8-membered rings of oxygen atoms, e.g. ZSM-34, in combination with a magnesium oxide, manganese oxide or magnesium oxide/platinum oxide catalyst modifier. Such modified zeolite catalysts are especially useful for converting methanol and/or methyl ester to an olefin-containing hydrocarbon product enriched in ethylene and propylene with enhanced catalyst lifetime.
摘要翻译：改进的沸石催化剂组合物，其包含具有由8-元环氧原子形成的孔窗的结晶铝硅酸盐沸石，例如。 ZSM-34与氧化镁，氧化锰或氧化镁/氧化铂催化剂改性剂组合。这种改性沸石催化剂特别可用于将甲醇和/或甲酯转化为富含乙烯和丙烯的含烯烃的烃产物，并具有增强的催化剂寿命。

99. 发明授权

US4374297A Selective oxidation of ethyl toluene or methyl styrene isomer mixtures to enrich meta-isomer content 失效
标题翻译：乙基甲苯或甲基苯乙烯异构体混合物的选择性氧化以富集间 - 异构体含量
公开(公告)号：US4374297A
公开(公告)日：1983-02-15
申请号：US336102
申请日：1981-12-30
申请人： John M. Klosek , Margaret M. Wu
发明人： John M. Klosek , Margaret M. Wu
IPC分类号： C07C7/148 , C07C7/00
CPC分类号： C07C7/14816
摘要： The meta isomer content of ethyl toluene or methyl styrene isomer mixtures containing predominately meta isomer and para isomer is increased by subjecting the mixture to oxidation with an oxygen containing gas, e.g. air in the presence of a zeolite modified with a transition metal oxidation catalyst, e.g. Co or Cu ZSM-5. The para isomer is selectively oxidized and the meta isomer is easily separated from the product to give isomer mixtures containing greater than 90 percent meta from mixtures containing 60-65 percent meta and not separable by conventional means.
摘要翻译：含有主要间位异构体和对位异构体的乙基甲苯或甲基苯乙烯异构体混合物的间位异构体含量通过使含氧气体氧化，例如，在用过渡金属氧化催化剂改性的沸石的存在下， Co或Cu ZSM-5。对位异构体被选择性氧化，并且间位异构体容易从产物中分离出来，得到含有大于90％的含有60-65

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