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91. 发明专利

JPH03201308A CONDUCTING COMPOUND 失效
公开(公告)号：JPH03201308A
公开(公告)日：1991-09-03
申请号：JP33899789
申请日：1989-12-26
申请人： DAIDO STEEL CO LTD , TOA GOSEI CHEM IND
发明人： TAKAGI SHINOBU , SHIMIZU TAKASUMI , KISHIMOTO YOSHIHISA , URAMOTO YOSHITO
IPC分类号： H01B1/02 , H05K1/09
摘要： PURPOSE:To obtain a conducting compound excellent in printing, conducting and long-stabilized conducting properties, etc., by constituting a conducting compound out of copper particles mixed together with crystal-particle-aggregate copper particles and three-branchlike copper particles, thermosetting resin, fatty acid, metallic salt thereof and amine compound. CONSTITUTION:A conducting compound is constituted of copper particles mixed together with 90-99weight% crystal-particle-aggregated copper particles and 1-10weight% tree-branchlike copper particles, thermosetting resin, fatty acid (salt) of 7-23 carbone molecules, and amine compound. In this case, the copper particles A is such an aggregation of crystal particles that they macroscopicly become particles with their surfaces roughened, while the conducting circuit of obtainable conducting compound is better for soldering than mere crystal particles, and the copper particles are mutually intertwined. Besides, copper particles B, judging from their form, promote the mutual intertwining of the particles and the roughening of the particle surfaces. This enables the obtaining of an excellent conducting compound durable for long use.

92. 发明专利

JPH03176904A CONDUCTIVE PASTE 失效
公开(公告)号：JPH03176904A
公开(公告)日：1991-07-31
申请号：JP31485789
申请日：1989-12-04
申请人： DAIDO STEEL CO LTD
发明人： TAKAGI SHINOBU , SHIMIZU TAKASUMI , NISHINAKAGAWA TAMOTSU
IPC分类号： H01B1/16 , H05K1/09
摘要： PURPOSE:To realize conductive paste having excellent performance and burnable in the atmosphere at a low cost by using predetermined quantities of respective Cu powder, B powder, boric acid or borate powder, glass frit and organic vehicle. CONSTITUTION:Low cost Cu is used to substitute for expensive Ni. A predetermined ratio is provided between respective compositions. Namely, the ratio of B powder against 100 weight part of the total weight of Cu powder and B powder is 3.5-3.9 weight part. The ratio of boric acid or borate against 100 weight part of the total weight of Cu powder and B powder is 2.0-50.0. The ratio of glass frit against 100 weight part of the total weight of Cu powder and B powder is 10-30 weight part. A conductive composition having excellent fluidity, formability, printing property and high conductivity can be manufactured with this paste composed in that method.

93. 发明专利

JPH0367402A CONDUCTING COMPOSITION MATERIAL 失效
公开(公告)号：JPH0367402A
公开(公告)日：1991-03-22
申请号：JP20213289
申请日：1989-08-03
申请人： TOA GOSEI CHEM IND , DAIDO STEEL CO LTD
发明人： KISHIMOTO YOSHIHISA , URAMOTO YOSHITO , TAKAGI SHINOBU , SHIMIZU TAKASUMI
IPC分类号： H01B1/22 , C09D5/24 , H05K1/09
摘要： PURPOSE:To form a pattern on a substrate by printing or the like and improve the conductivity, stability and direct soldering property by using a composite material made of specially processed copper grains, thermosetting resin, specific fatty acid, or metal salt and an amine compound. CONSTITUTION:The grain size of copper grains is set to 0.1-50mum to suppress surface oxidation and allow screen printing, and silver is electrolytically replaced and coated on the surface to have the high conductivity, oxidation resistance and long-term stability. The coating quantity is preferably 0.1-20wt.%. This conducting filler 75-95 pts.wt. is combined in the total solid quantity 100 pts.wt. of resin binder containing thermosetting phenol resin 20-100wt.% in the resin component. Fatty acid (salt) 0.01-10wt.% with the carbon number 7-23 and amine compound 0.1-50 pts.wt. Such as monoethanol amine are added and kneaded to obtain a composite material. The oxidation resistance and soldering property of copper grains are improved.

94. 发明专利

JPH029713A PRODUCTION OF BORON PHOSPHIDE 失效
公开(公告)号：JPH029713A
公开(公告)日：1990-01-12
申请号：JP15894288
申请日：1988-06-27
申请人： DAIDO STEEL CO LTD
发明人： SHIMIZU TAKASUMI , TAKAGI SHINOBU , MATSUYAMA MAKOTO
IPC分类号： C01B35/04
摘要： PURPOSE:To easily product boron phosphide by reacting red phosphorus with boron at a high temp. under high pressure to prepare the compd. having a substantially equimolar amt. thereof. CONSTITUTION:The mixture of red phosphorus and boron in the substantially equimolar amt. is reacted at a high temp. under high pressure. The preferable condition for reacting the mixture is 500-1500 deg.C the reaction temp. and 1000-3000kg f/cm the reaction pressure. As the apparatus, a hot isostatic pressing apparatus or hot pressing apparatus is suitable. By the method above- mentioned, the red phosphorus is molten by heating at a high temp. and suppressed to escape at a high pressure, and the boron is dissolved in such red phosphorus to react in the substantially equimolar amt. At the time, by using fine powder as raw material, the fine powdered boron phosphide can be formed, or by molding both raw materials with a binder and thereafter by reacting, a sintered compact having a fixed shape can be obtd.

95. 发明专利

JPH0198674A CONDUCTIVE COMPOSITION 失效
公开(公告)号：JPH0198674A
公开(公告)日：1989-04-17
申请号：JP25571987
申请日：1987-10-09
申请人： DAIDO STEEL CO LTD
发明人： SHIMIZU TAKASUMI , TAKAGI SHINOBU , NISHINAKAGAWA TAMOTSU
IPC分类号： C09D11/00 , C09D11/02 , C09D11/033 , C09D11/52 , H01B1/00 , H01B1/22 , H05K1/09
摘要： PURPOSE:To make it possible to form a conductive composition useful as a conductive ink or a conductive paste having good printability and conductivity of a conductive film, by mixing a specified metallic powder mixture, a binder and a solvent together as principal components. CONSTITUTION:This conductive composition mainly consists of a metallic powder, a binder and a solvent. Said metallic powder is a mixture of a spherical powder and a flaky powder at a weight ratio of 9:1-5:5. It is desirable that said spherical powder has a diameter

96. 发明专利

JPS6447801A PRODUCTION OF FINE METAL POWDER 失效
公开(公告)号：JPS6447801A
公开(公告)日：1989-02-22
申请号：JP20229287
申请日：1987-08-13
申请人： DAIDO STEEL CO LTD
发明人： TAKAGI SHINOBU
IPC分类号： B22F9/22 , B22F9/26
摘要： PURPOSE:To produce a metal powder having high purity and crystallinity by dissolving and dispersing fine metal oxide powder into an org. solvent of a specific b. p. and holding this liquid suspension in a hydrogen atmosphere for a prescribed period of time at the temp. below the b. p. of the solvent. CONSTITUTION:The fine powder of the metal oxide or metal hydroxide of copper, silver, platinum, etc., is dissolved and dispersed in the org. solvent having >=100 deg.C b. p. Ethylene glycol or glycerol or the deriv. thereof is preferably used for the org. solvent. This liquid suspension of the org. solvent is held in the hydrogen atmosphere for the prescribed period of time at the temp. below the b. p. thereof. The fine metal powder of a polyhedral shape having good crystallinity is thus obtd. by the relatively simple operation. This fine metal powder is less surface-oxidized and is hardly oxidized at ordinary temp.

97. 发明专利

JP2012129217A Pulverulent body to be pressure-molded for powder magnetic core and method for producing powder magnetic core 审中-公开
标题翻译：用于粉末磁芯的压力成型体和用于生产粉末磁芯的方法
公开(公告)号：JP2012129217A
公开(公告)日：2012-07-05
申请号：JP2010272564
申请日：2010-12-07
申请人： Daido Steel Co Ltd , 大同特殊鋼株式会社
发明人： TAKAGI SHINOBU , TAKEMOTO SATOSHI
IPC分类号： H01F1/20 , B22F1/00 , B22F1/02 , B22F3/00 , B22F3/24 , H01F41/02
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a powder magnetic core which reduces iron loss, and to provide a pulverulent body to be pressure-molded for the powder magnetic core.SOLUTION: The pulverulent body is composed of a mixed power of a coagulation prevention powder (3) and a pure Fe powder (2) made of pure Fe. The coagulation prevention powder that is composed of at least one from among MgO, TiOand AlOis provided on a part of the pure Fe powder surface. Further, a binder (5) is provided on the whole pure Fe powder surface so as to cover it. The manufacturing method comprises: a step of obtaining the pure Fe powder with an atomizing method; an intermediate mixing step of mixing the pure Fe powder with the coagulation prevention powder to obtain an intermediate powder composed of an intermediate powder that is the pure Fe powder of having the coagulation prevention powder provided at a part of the pure Fe powder surface; a heat-treatment step of heat-treating the intermediate powder to remove a distortion accumulated inside of the pure Fe powder; a mixing step of mixing the intermediate powder with the binder to obtain a mixture containing the binder and an Fe powder composed of the pure Fe powder having the binder provided so as to cover the whole pure Fe powder surface; and a molding step of pressure-molding the mixture.
摘要翻译：解决的问题：提供一种制造减少铁损的粉末磁芯的方法，并提供用于粉末磁芯的压模的粉状体。解决方案：粉末体由防凝粉（3）和纯Fe制成的纯Fe粉（2）的混合动力组成。由MgO，TiO 2 和Al 2

98. 发明专利

JP2009019228A Metal separator material for polymer electrolyte fuel cell 审中-公开
标题翻译：用于聚合物电解质燃料电池的金属分离器材料
公开(公告)号：JP2009019228A
公开(公告)日：2009-01-29
申请号：JP2007181476
申请日：2007-07-10
申请人： Daido Steel Co Ltd , 大同特殊鋼株式会社
发明人： FUTO MASAYOSHI , TAKAGI SHINOBU , HISADA TAKEO
IPC分类号： C22C38/00 , C22C38/60 , H01M8/02 , H01M8/10
CPC分类号： Y02E60/521
摘要： PROBLEM TO BE SOLVED: To make it possible to use austenitic stainless steel as a metal separator material for polymer electrolyte fuel cell by increasing the electric conductivity of the austenitic stainless steel while maintaining its excellent sulfuric acid corrosion resistance. SOLUTION: The austenitic stainless steel, which has a composition consisting of, by mass, 0.02 to 0.4% C, 0.03 to 2% Ti, 0.01 to 0.7% S, ≤2% Si, ≤2% Mn, 2 to 30% Ni, 12 to 30% Cr, ≤0.05% P, ≤0.03% O, ≤0.05% N and the balance Fe with inevitable impurities and satisfying inequalities 0.3≤4×C/Ti≤1.0 and 0.2≤1.5×S/Ti≤1.0 (wherein each atomic symbol represents its content in mass%), is used as the metal separator material. COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：为了使奥氏体不锈钢作为固体高分子型燃料电池的金属隔板材料可以通过提高奥氏体不锈钢的导电率同时保持其优异的耐硫酸腐蚀性而成为可能。解决方案：奥氏体不锈钢，其组成以质量计为0.02〜0.4％，0.03〜2％Ti，0.01〜0.7％S，≤2％Si，≤2％Mn，2〜 30％Ni，12〜30％Cr，≤0.05％P，≤0.03％O，≤0.05％N，余量为Fe和不可避免的杂质，满足不等式0.3≤4×C /Ti≤1.0和0.2≤1.5×S / Ti≤1.0（其中，各原子符号表示其质量％）作为金属隔板材料。版权所有（C）2009，JPO＆INPIT

99. 发明专利

JP2007323988A Metal separator for fuel cell, manufacturing method of the same, and fuel cell 审中-公开
标题翻译：用于燃料电池的金属分离器，其制造方法和燃料电池
公开(公告)号：JP2007323988A
公开(公告)日：2007-12-13
申请号：JP2006153563
申请日：2006-06-01
申请人： Daido Steel Co Ltd , 大同特殊鋼株式会社
发明人： TAKAGI SHINOBU , FUTO MASAYOSHI , HISADA TAKEO
IPC分类号： H01M8/02 , H01M8/10
CPC分类号： Y02P70/56
摘要： PROBLEM TO BE SOLVED: To provide a metal separator for a fuel cell having sufficient corrosion resistance although a noble metal film is thin, and easy to manufacture. SOLUTION: In this separator for a fuel cell, a metal material plate material constituting it has a plate-like base material of a metal material where a passive film is formed on a surface thereof in the atmosphere, and a noble metal coating layer covering the surface of the base material and containing a diffused metal constituent from the base material. When noble metal concentration is analyzed in the depth direction from the surface layer side of the noble metal coating layer by an Auger electron spectral analysis method, a main part of the noble metal coating layer where the noble metal concentration C N is set constant in the range of 85-99.8 mass% in the depth direction is discerned from a noble metal concentration transition part thereof where the noble metal concentration C N is gradually reduced from the noble metal concentration C A of the main part toward bulk noble metal concentration C B of the base material as shown on the right of the figure. In the main part, the content of the diffused metal constituent C F is 0.2-15 mass%, and the thickness t1 is not smaller than 1 nm and not larger than 100 nm, and larger than the thickness t2 of the noble metal concentration transition part. COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：为了提供一种具有足够的耐腐蚀性的燃料电池用金属隔板，尽管贵金属薄膜薄，易于制造。解决方案：在燃料电池用隔板中，构成它的金属材料板材具有金属材料的板状基材，其中在大气中的表面上形成钝化膜，贵金属涂层覆盖基材的表面并且从基材包含扩散的金属成分的层。当通过俄歇电子光谱分析方法从贵金属涂层的表面层侧的深度方向分析贵金属浓度时，贵金属涂层的贵金属浓度C 从贵金属浓度C N 从贵金属浓度逐渐降低的贵金属浓度转变部分可以看出，深度方向上的SB>在85-99.8质量％的范围内被设定为恒定主要部分朝向基体材料的本体贵金属浓度C B 的C A ，如图所示。在主要部分中，扩散金属成分C F 的含量为0.2〜15质量％，厚度t1不小于1nm且不大于100nm，并且厚度大于厚度 t2的贵金属浓度转变部分。版权所有（C）2008，JPO＆INPIT

100. 发明专利

JP2005142074A Corrosion-resistant conductive member 有权
标题翻译：耐腐蚀导电构件
公开(公告)号：JP2005142074A
公开(公告)日：2005-06-02
申请号：JP2003378533
申请日：2003-11-07
申请人： Daido Steel Co Ltd , 大同特殊鋼株式会社
发明人： HISADA TAKEO , KANEDA YASUSHI , TAKAGI SHINOBU , FUSE NAOKI
IPC分类号： C25D3/48 , H01M8/02
CPC分类号： C25D3/48 , H01M8/0206 , H01M8/021 , H01M8/0228 , Y10T428/12889 , Y10T428/12979
摘要： PROBLEM TO BE SOLVED: To always guarantee high corrosion resistance even in the case of an ultrathin Au layer, for a corrosion-resistant conductive member with a stainless steel sheet equipped with an Au-plating layer of a thickness of 100 nm or less, to be used as a separator for a fuel cell. SOLUTION: A maximum value (v) of energy detection intensity of Au is to reach at least 98% against the total element energy detection intensity (100%) in the Au thin layer from the surface up to an interface between the Au layer and base metals (a face equivalent to a position where a sinking Au curve crosses a rising curve of the most predominant ingredient out of the base metals, when a graph is made of energy intensities obtained in an Auger analysis of the corrosion-resistant conductive member). COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：要解决的问题：即使在超薄Au层的情况下，一直保证高耐腐蚀性，对于具有厚度为100nm的Au镀层的不锈钢板的耐腐蚀导电构件，或较少，被用作燃料电池的分离器。
解决方案：Au的能量检测强度的最大值（v）相对于Au薄层从表面直到Au之间的界面的总元素能量检测强度（100％）达到至少98％层和贱金属（相当于下沉的Au曲线穿过基本金属中最主要成分的上升曲线的位置的面，当图表由在耐腐蚀导电的俄歇分析中获得的能量强度会员）。版权所有（C）2005，JPO＆NCIPI

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