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1. 发明申请

US20050038279A1 Proces for the preparation of 9, 10-dihydro-9-oxa-10-organylphosphaphenanthrene-10-oxide and derivatives of the same substituted on the phenyl groups 失效
标题翻译：制备9,10-二氢-9-氧杂-10-有机基膦菲-10-氧化物的方法及其在苯基上取代的衍生物
公开(公告)号：US20050038279A1
公开(公告)日：2005-02-17
申请号：US10918838
申请日：2004-08-13
申请人： Uwe Dittrich , Berthold Just , Manfred Doring , Michael Ciesielski
发明人： Uwe Dittrich , Berthold Just , Manfred Doring , Michael Ciesielski
IPC分类号： C07F9/02 , C07F9/28 , C07F9/48 , C07F9/50 , C07F9/6571 , C08K5/5313 , C08L23/02 , C08L25/06 , C08L61/04 , C08L63/00 , C08L67/00 , C08L69/00 , C08L77/00
CPC分类号： C07F9/657172 , C07F9/4841 , C08K5/5313
摘要： A process is provided for the preparation of 9,10-dihydro-9-oxa-10-organylphosphaphenanthrene-10-oxide and derivatives of same substituted on the phenyl groups, in which: (a) 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOP) or a derivative of same is reacted in the presence of at least one mono- or polyhydric alcohol with at least one ortho ester with formation of a first intermediate product, (b) the intermediate product from step (a) is optionally reacted with at least one further mono- or polyhydric alcohol with formation of a further intermediate product and (c) the intermediate product from steps (a) or (b) is transformed by addition of catalytic quantities of alkylation agent into 9,10-dihydro-9-oxa-10-organylphosphaphenanthrene-10-oxide or a derivative of same substituted on the phenyl groups.
摘要翻译：提供了制备9,10-二氢-9-氧杂-10-有机基膦菲-10-氧化物及其在苯基上取代的相同衍生物的方法，其中：（a）9,10-二氢-9-氧杂 -10-磷杂菲-10-氧化物（DOP）或其衍生物在至少一种一元醇或多元醇与至少一种原酸酯的存在下反应，形成第一中间产物，（b）中间产物步骤（a）任选地与至少一种另外的一元醇或多元醇反应形成另外的中间产物，和（c）通过加入催化量的烷基化来转化来自步骤（a）或（b）的中间产物试剂转化成9,10-二氢-9-氧杂-10-有机基膦菲-10-氧化物或其在苯基上取代的相同衍生物。

2. 发明申请

US20050038278A1 Process for the preparation of 9, 10-dihydro-9-OXA-10-organyloxyphosphaphenanthrene-10-oxide or -thione and derivatives of the same substituted on the phenyl groups 失效
标题翻译：制备9,10-二氢-9-OXA-10-有机氧基菲啶-10-氧化物或硫代酮的方法及其在苯基上取代的衍生物
公开(公告)号：US20050038278A1
公开(公告)日：2005-02-17
申请号：US10918836
申请日：2004-08-13
申请人： Uwe Dittrich , Berthold Just , Manfred Doring , Michael Ciesielski
发明人： Uwe Dittrich , Berthold Just , Manfred Doring , Michael Ciesielski
IPC分类号： C07F9/6571 , C07F9/02
CPC分类号： C08K5/5313 , C07F9/657181 , C07F9/65719
摘要： A process is provided for the preparation of 9,10-dihydro-9-oxa-10-organyloxyphosphaphenanthrene-10-oxide or -thione and derivatives of same substituted on the phenyl groups, in which: (a) 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOP) or a derivative of same is reacted in the presence of at least one mono- or polyhydric alcohol with at least one ortho ester with formation of a first intermediate product, (b) the intermediate product from step (a) is optionally reacted with at least one further mono- or polyhydric alcohol with formation of a further intermediate product and (c) the intermediate product from steps (a) or (b) is transformed by addition of oxidation agent into 9,10-dihydro-9-oxa-10-organyloxyphosphaphenanthrene-10-oxide or -thione or a derivative of same substituted on the phenyl groups.
摘要翻译：提供了用于制备9,10-二氢-9-氧杂-10-有机氧基菲啶-10-氧化物或硫代酮及其在苯基上取代的相同衍生物的方法，其中：（a）9,10-二氢 - 9-氧杂-10-磷杂菲-10-氧化物（DOP）或其衍生物在至少一种一元醇或多元醇与至少一种原酸酯的存在下反应，形成第一中间产物，（b）来自步骤（a）的中间产物任选地与至少一种另外的一元醇或多元醇反应形成另外的中间产物，和（c）通过加入氧化来转化来自步骤（a）或（b）的中间产物试剂转化成9,10-二氢-9-氧杂-10-有机氧基亚磷酰-10-氧化物或硫代酮或其在苯基上取代的相同衍生物。

3. 发明申请

US20050020739A1 Derivatives of 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide 审中-公开
标题翻译： 9,10-二氢-9-氧杂-10-磷杂菲-10-氧化物的衍生物
公开(公告)号：US20050020739A1
公开(公告)日：2005-01-27
申请号：US10890035
申请日：2004-07-13
申请人： Uwe Dittrich , Berthold Just , Manfred Doring , Michael Ciesielski
发明人： Uwe Dittrich , Berthold Just , Manfred Doring , Michael Ciesielski
IPC分类号： C07F9/6571 , C08K5/5313 , C08K5/49 , C07F9/02
CPC分类号： C08K5/5313 , C07F9/657172
摘要： Novel derivatives of 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide, processes for their preparation and the use of the derivatives for flame protection of natural products and plastics are disclosed.
摘要翻译：公开了9,10-二氢-9-氧杂-10-磷杂菲-10-氧化物的新衍生物，其制备方法及其衍生物用于天然产物和塑料的火焰保护。

4. 发明授权

US08058329B2 Nitrous bridged derivatives of 6H-dibenz[c,e][1,2]-oxaphosphorine-6-oxides, process for the preparation and use thereof 失效
标题翻译： 6H-二苯并[c，e] [1,2] - 氧磷磷-6-氧化物的亚硝基桥连衍生物，其制备方法及用途
公开(公告)号：US08058329B2
公开(公告)日：2011-11-15
申请号：US10598012
申请日：2005-11-03
申请人： Berthold Just , Uwe Dittrich , Holger Keller , Manfred Doering , Uwe Storzer , Michael Ciesielski
发明人： Berthold Just , Uwe Dittrich , Holger Keller , Manfred Doering , Uwe Storzer , Michael Ciesielski
IPC分类号： C04B24/26 , C08K3/00 , C04B28/04 , C07D251/00 , C07F9/02
CPC分类号： C08G59/34 , C07D251/34 , C07F9/657172 , C09K21/12
摘要： Nitrous bridged derivatives of 6H-dibenz[c,e][1,2]-oxaphosphorine-6-oxides, process for the preparation and use thereof.The invention refers to nitrous bridged derivatives of 6H-dibenz[c,e][1,2]-oxaphosphorine-6-oxides, a process for the preparation thereof and their use as flameproofing agents for polymers such as polyesters, polyamides, polycarbonates, polystyrenes, polyethylene, polypropylene, phenolic and epoxy resins. The derivatives have the Formulae I or II:
摘要翻译： 6H-二苯并[c，e] [1,2] - 氧磷磷-6-氧化物的亚硝基桥联衍生物，其制备和使用方法。本发明涉及6H-二苯并[c，e] [1,2] - 氧磷磷-6-氧化物的亚硝基桥联衍生物，其制备方法及其作为聚合物如聚酯，聚酰胺，聚碳酸酯等的防火剂的用途，聚苯乙烯，聚乙烯，聚丙烯，酚醛树脂和环氧树脂。衍生物具有式I或II：

5. 发明申请

US20100280215A1 NITROUS BRIDGED DERIVATIVES OF 6H-DIBENZ[C,E][1,2]-OXAPHOSPHORINE-6-OXIDES, PROCESS FOR THE PREPARATION AND USE THEREOF 审中-公开
标题翻译： 6H-DIBENZ [C，E] [1,2] - 氧化萘-6-氧化物的硝基桥联衍生物，其制备和使用方法
公开(公告)号：US20100280215A1
公开(公告)日：2010-11-04
申请号：US12836716
申请日：2010-07-15
申请人： Berthold Just , Uwe Dittrich , Holger Keller , Manfred Doering , Uwe Storzer , Michael Ciesielski
发明人： Berthold Just , Uwe Dittrich , Holger Keller , Manfred Doering , Uwe Storzer , Michael Ciesielski
IPC分类号： C08G69/02
CPC分类号： C08G59/34 , C07D251/34 , C07F9/657172 , C09K21/12
摘要： The invention refers to nitrous bridged derivatives of 6H-dibenz[c,e][1,2]-oxaphosphorine-6-oxides, a process for the preparation thereof and their use as flameproofing agents for polymers such as polyesters, polyamides, polycarbonates, polystyrenes, polyethylene, polypropylene, phenolic and epoxy resins. The derivatives have the Formulae I or II:
摘要翻译：本发明涉及6H-二苯并[c，e] [1,2] - 氧磷磷-6-氧化物的亚硝基桥联衍生物，其制备方法及其作为聚合物如聚酯，聚酰胺，聚碳酸酯等的防火剂的用途，聚苯乙烯，聚乙烯，聚丙烯，酚醛树脂和环氧树脂。衍生物具有式I或II：

6. 发明申请

US20080167405A1 Nitrous Bridged Derivatives of 6H-Dibenz[C,E][1,2]-Oxaphosphorine-6-Oxides, Process For the Preparation and Use Thereof 失效
标题翻译： 6H-二苯并[C，E] [1,2] - 次磷酸-6-氧化物的亚麻桥接衍生物，其制备方法及用途
公开(公告)号：US20080167405A1
公开(公告)日：2008-07-10
申请号：US10598012
申请日：2005-11-03
申请人： Berthold Just , Uwe Dittrich , Holger Keller , Manfred Doering , Uwe Storzer , Michael Ciesielski
发明人： Berthold Just , Uwe Dittrich , Holger Keller , Manfred Doering , Uwe Storzer , Michael Ciesielski
IPC分类号： C07D251/32 , C08K5/34 , C07F9/547
CPC分类号： C08G59/34 , C07D251/34 , C07F9/657172 , C09K21/12
摘要： Nitrous bridged derivatives of 6H-dibenz[c,e][1,2]-oxaphosphorine-6-oxides, process for the preparation and use thereof.The invention refers to nitrous bridged derivatives of 6H-dibenz[c,e][1,2]-oxaphosphorine-6-oxides, a process for the preparation thereof and their use as flameproofing agents for polymers such as polyesters, polyamides, polycarbonates, polystyrenes, polyethylene, polypropylene, phenolic and epoxy resins. The derivatives have the Formulae I or II:
摘要翻译： 6H-二苯并[c，e] [1,2] - 氧磷磷-6-氧化物的亚硝基桥联衍生物，其制备和使用方法。本发明涉及6H-二苯并[c，e] [1,2] - 氧磷磷-6-氧化物的亚硝基桥联衍生物，其制备方法及其作为聚合物如聚酯，聚酰胺，聚碳酸酯等的防火剂的用途，聚苯乙烯，聚乙烯，聚丙烯，酚醛树脂和环氧树脂。衍生物具有式I或II：

7. 发明授权

US07317120B2 Process for the preparation of 9,10-dihydro-9-oxa-10-organylphosphaphenanthrene-10-oxide and derivatives of the same substituted on the phenyl groups 失效
标题翻译：制备9,10-二氢-9-氧杂-10-有机基膦菲-10-氧化物的方法及其在苯基上取代的衍生物
公开(公告)号：US07317120B2
公开(公告)日：2008-01-08
申请号：US10918838
申请日：2004-08-13
申请人： Uwe Dittrich , Berthold Just , Manfred Döring , Michael Ciesielski
发明人： Uwe Dittrich , Berthold Just , Manfred Döring , Michael Ciesielski
IPC分类号： C07F9/02
CPC分类号： C07F9/657172 , C07F9/4841 , C08K5/5313
摘要： A process is provided for the preparation of 9,10-dihydro-9-oxa-10-organylphosphaphenanthrene-10-oxide and derivatives of same substituted on the phenyl groups, in which: (a) 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOP) or a derivative of same is reacted in the presence of at least one mono- or polyhydric alcohol with at least one ortho ester with formation of a first intermediate product, (b) the intermediate product from step (a) is optionally reacted with at least one further mono- or polyhydric alcohol with formation of a further intermediate product and (c) the intermediate product from steps (a) or (b) is transformed by addition of catalytic quantities of alkylation agent into 9,10-dihydro-9-oxa-10-organylphosphaphenanthrene-10-oxide or a derivative of same substituted on the phenyl groups.
摘要翻译：提供了制备9,10-二氢-9-氧杂-10-有机基膦菲-10-氧化物及其在苯基上取代的相同衍生物的方法，其中：（a）9,10-二氢-9-氧杂 -10-磷杂菲-10-氧化物（DOP）或其衍生物在至少一种一元醇或多元醇与至少一种原酸酯的存在下反应，形成第一中间产物，（b）中间产物步骤（a）任选地与至少一种另外的一元醇或多元醇反应形成另外的中间产物，和（c）通过加入催化量的烷基化来转化来自步骤（a）或（b）的中间产物试剂转化成9,10-二氢-9-氧杂-10-有机基膦菲-10-氧化物或其在苯基上取代的相同衍生物。

8. 发明授权

US07317119B2 Process for the preparation of 9, 10-dihydro-9-OXA-10-organyloxyphosphaphenanthrene-10-oxide or -thione and derivatives of the same substituted on the phenyl groups 失效
标题翻译：制备9,10-二氢-9-OXA-10-有机氧基菲啶-10-氧化物或硫代酮的方法及其在苯基上取代的衍生物
公开(公告)号：US07317119B2
公开(公告)日：2008-01-08
申请号：US10918836
申请日：2004-08-13
申请人： Uwe Dittrich , Berthold Just , Manfred Döring , Michael Ciesielski
发明人： Uwe Dittrich , Berthold Just , Manfred Döring , Michael Ciesielski
IPC分类号： C07F9/02
CPC分类号： C08K5/5313 , C07F9/657181 , C07F9/65719
摘要： A process is provided for the preparation of 9,10-dihydro-9-oxa-10-organyloxyphosphaphenanthrene-10-oxide or -thione and derivatives of same substituted on the phenyl groups, in which: (a) 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOP) or a derivative of same is reacted in the presence of at least one mono- or polyhydric alcohol with at least one ortho ester with formation of a first intermediate product, (b) the intermediate product from step (a) is optionally reacted with at least one further mono- or polyhydric alcohol with formation of a further intermediate product and (c) the intermediate product from steps (a) or (b) is transformed by addition of oxidation agent into 9,10-dihydro-9-oxa-10-organyloxyphosphaphenanthrene-10-oxide or -thione or a derivative of same substituted on the phenyl groups.
摘要翻译：提供了用于制备9,10-二氢-9-氧杂-10-有机氧基菲啶-10-氧化物或硫代酮及其在苯基上取代的相同衍生物的方法，其中：（a）9,10-二氢 - 9-氧杂-10-磷杂菲-10-氧化物（DOP）或其衍生物在至少一种一元醇或多元醇与至少一种原酸酯的存在下反应，形成第一中间产物，（b）来自步骤（a）的中间产物任选地与至少一种另外的一元醇或多元醇反应形成另外的中间产物，和（c）通过加入氧化来转化来自步骤（a）或（b）的中间产物试剂转化成9,10-二氢-9-氧杂-10-有机氧基亚磷酰-10-氧化物或硫代酮或其在苯基上取代的相同衍生物。

9. 发明授权

US07951878B2 Halogen-free flameproof epoxy resin formulations 失效
标题翻译：无卤素防火环氧树脂配方
公开(公告)号：US07951878B2
公开(公告)日：2011-05-31
申请号：US11916435
申请日：2006-12-12
申请人： Berthold Just , Holger Keller , Manfred Doering , Uwe Storzer , Sebastian Seibold
发明人： Berthold Just , Holger Keller , Manfred Doering , Uwe Storzer , Sebastian Seibold
IPC分类号： C08G59/40 , C08G59/00 , C08G79/06 , C08G79/00
CPC分类号： C08G59/4007 , C08G59/3254 , H05K1/0326 , H05K2201/012
摘要： The invention relates to a method for preparing halogen-free flameproof epoxy resins, in which a halogen-free epoxy resin is reacted with a polyfunctional aldehyde or ketone and a phosphinic acid derivative, wherein the phosphinic acid derivative contains at least one P—H-active structural unit of the formula ═PH(O) and is used in an amount equivalent to the polyfunctionality of the aldehyde or ketone, to a halogen-free flameproof epoxy resin obtainable by this method, to the use of the epoxy resin as a base material for the manufacture of printed circuit boards and printed circuits and to intermediates used to prepare the epoxy resins.
摘要翻译：本发明涉及一种制备无卤素防火环氧树脂的方法，其中无卤环氧树脂与多官能醛或酮和次膦酸衍生物反应，其中次膦酸衍生物含有至少一个P-H- 使用式=PH（O）的活性结构单元，并且以与醛或酮的多官能度相当的量使用该方法获得的无卤素防火环氧树脂，以环氧树脂为基础用于制造印刷电路板和印刷电路的材料以及用于制备环氧树脂的中间体。

10. 发明申请

US20060223921A1 Prepolymers containing phosphororganic compounds and uses thereof 审中-公开
标题翻译：含有有机磷化合物的预聚物及其用途
公开(公告)号：US20060223921A1
公开(公告)日：2006-10-05
申请号：US11398039
申请日：2006-04-05
申请人： Monika Bauer , Berthold Just
发明人： Monika Bauer , Berthold Just
IPC分类号： C08K5/50
CPC分类号： C08G59/1488 , C08G8/10 , C08G59/4021 , C08G59/50 , C08G63/692 , C08G63/91 , C08K5/5313 , C08L63/00 , C08L67/00
摘要： The present invention relates to prepolymers produced by reacting resins with phosphororganic compounds obtained from phosphinic acid derivatives, and their use for producing flame resistant polymers, in particular duromers, and the polymers produced therewith. In particular, the present invention relates to a prepolymer for flame resistant polymers, particularly duromers, which is obtained by reacting at least one phosphinic acid derivative of formula I (R1O)(R2)P(O)—R3, wherein R1 and R2 independently of one another represent an optionally substituted alkyl, aryl, arylalkyl, alkylaryl or alkylarylalkyl group with 1 to 20 carbon atoms, R3 represents hydrogen or an optionally substituted alkyl, aryl, arylalkyl, alkylaryl or alkylarylalkyl group with 1 to 20 carbon atoms, with at least one resin preferably selected from the group consisting of an epoxy resin, cyanate resin, an unsaturated polyester, vinyl ester, phenol resin and a bismaleimide.
摘要翻译：本发明涉及通过使树脂与从次膦酸衍生物获得的磷有机化合物反应制备的预聚物及其制备阻燃聚合物，特别是丁二烯的用途，以及由其制备的聚合物。特别地，本发明涉及通过使至少一种式I的次膦酸衍生物<？in-line-formula description =“In-Line Formulas”end =“...”得到的阻燃聚合物，特别是丁二酸甘油酯的预聚物，（R 1 O）（R 2）P（O）-R 3，<β在线公式描述其中R 1和R 2彼此独立地表示任选取代的烷基，芳基，芳基烷基，烷基芳基或烷基芳基，具有1至20个碳原子的烷基芳基烷基，R 3表示氢或任选取代的具有1至20个碳原子的烷基，芳基，芳基烷基，烷基芳基或烷基芳基烷基，以及至少一种优选选自由环氧树脂，氰酸酯树脂，不饱和聚酯，乙烯基酯，酚醛树脂和双马来酰亚胺组成的组。

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