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1. 发明授权

US08398894B2 Catalyst for preparing carbon nanotubes by controlling its apparent density 有权
标题翻译：通过控制其表观密度来制备碳纳米管的催化剂
公开(公告)号：US08398894B2
公开(公告)日：2013-03-19
申请号：US12642084
申请日：2009-12-18
申请人： Namsun Choi , Hyun-Kyung Sung , Dong Hwan Kim , Sang-Hyo Ryu , Wan Sung Lee , Youngchan Jang
发明人： Namsun Choi , Hyun-Kyung Sung , Dong Hwan Kim , Sang-Hyo Ryu , Wan Sung Lee , Youngchan Jang
IPC分类号： H01B1/00
CPC分类号： H01B1/24 , B01J21/185 , B01J23/78 , B01J35/0026 , B01J37/009 , B01J37/03 , B82Y30/00 , B82Y40/00 , C01B32/15
摘要： The present invention relates to a catalyst for preparing a carbon nanotube having desired apparent density by controlling the adding amount of co-precipitating agent in the process of preparing a catalyst in order to obtain a catalyst having a minimized particle size. More specifically, this invention relates to a catalyst for preparing carbon nanotube having desired apparent density based upon the reverse-correlation between the amount of co-precipitating agent added in the process of preparing catalyst and the apparent density of catalyst. The carbon nanotube prepared by the catalyst having low apparent density shows excellent electrical conductivity and highly uniformed dispersion in the polymer/carbon nanotube composite.
摘要翻译：本发明涉及通过在制备催化剂的过程中控制共沉淀剂的添加量以获得具有最小粒度的催化剂来制备具有所需表观密度的碳纳米管的催化剂。更具体地，本发明涉及一种制备具有所需表观密度的碳纳米管的催化剂，其基于在制备催化剂的方法中加入的共沉淀剂的量与催化剂的表观密度之间的反相关性。通过具有低表观密度的催化剂制备的碳纳米管在聚合物/碳纳米管复合材料中显示出优异的导电性和高度均匀的分散体。

2. 发明授权

US08137591B2 Catalyst for preparing carbon nanotube comprising multi-component support materials containing amorphous silicon particles and the bulk scale preparation of carbon nanotube using the same 有权
标题翻译：用于制备包含含有非晶硅颗粒的多组分载体材料的碳纳米管的催化剂和使用其的碳纳米管的本体规模制备
公开(公告)号：US08137591B2
公开(公告)日：2012-03-20
申请号：US12568884
申请日：2009-09-29
申请人： Dong Hwan Kim , Sang-Hyo Ryu , Wan Sung Lee , Namsun Choi , Hyun-Kyung Sung , Youngchan Jang
发明人： Dong Hwan Kim , Sang-Hyo Ryu , Wan Sung Lee , Namsun Choi , Hyun-Kyung Sung , Youngchan Jang
IPC分类号： H01B1/04
CPC分类号： B01J23/78 , B01J21/185 , B01J23/002 , B01J2523/00 , B82Y30/00 , B82Y40/00 , C01B32/162 , C08J5/005 , Y10T428/2982 , B01J2523/22 , B01J2523/31 , B01J2523/41 , B01J2523/842
摘要： The present invention relates to a catalyst composition for preparing carbon nanotube containing multi-component support materials of amorphous Si, Mg and Al as well as a bulk scale preparation process for preparing carbon nanotube using said catalyst composition. More specifically, this invention relates to a process for preparing carbon nanotube using the catalyst composition comprising a transition metal catalyst and support materials of amorphous Si, Mg and Al.
摘要翻译：本发明涉及一种用于制备含有非晶Si，Mg和Al的多组分载体材料的碳纳米管的催化剂组合物以及使用所述催化剂组合物制备碳纳米管的散装规模制备方法。更具体地，本发明涉及使用包含过渡金属催化剂和非晶Si，Mg和Al的载体材料的催化剂组合物制备碳纳米管的方法。

3. 发明申请

US20120040186A1 Process For Preparing Catalyst Composition For The Synthesis Of Carbon Nanotube With High Yields Using The Spray Pyrolysis Method 有权
标题翻译：使用喷雾热解法制备高产率碳纳米管制备催化剂组合物的方法
公开(公告)号：US20120040186A1
公开(公告)日：2012-02-16
申请号：US13105663
申请日：2011-05-11
申请人： Sang-Hyo Ryu , Hyun-Kyung Sung , Namsun Choi , Wan Sung Lee , Dong Hwan Kim , Youngchan Jang
发明人： Sang-Hyo Ryu , Hyun-Kyung Sung , Namsun Choi , Wan Sung Lee , Dong Hwan Kim , Youngchan Jang
IPC分类号： D01F9/12 , B01J37/08 , B01J21/02 , B82Y30/00
CPC分类号： B82Y40/00 , B01J23/745 , B01J23/75 , B01J23/78 , B01J23/8872 , B01J35/002 , B01J37/082 , B82Y30/00 , D01F9/12 , D01F9/127 , D01F9/1273 , Y10S977/74 , Y10S977/742 , Y10S977/84 , Y10S977/842 , Y10T428/298
摘要： The present invention relates to a process for preparing catalyst composition for the synthesis of carbon nanotube with high yields using the spray pyrolysis method. More particularly, this invention relates to a process for preparing catalyst composition for the synthesis of carbon nanotube comprising the steps of i) dissolving multi-component metal precursors of catalyst composition in de-ionized water; ii) spraying obtained catalytic metal precursor solution into the high temperature reactor by gas atomization method; iii) forming the catalyst composition powder by pyrolysis of gas atomized material; and iv) obtaining the catalyst composition powder, wherein said catalyst composition comprises i) main catalyst selected from Fe or Co, ii) Al, iii) optional co-catalyst at least one selected from Ni, Cu, Sn, Mo, Cr, Mn, V, W, Ti, Si, Zr or Y, iv) inactive support of Mg. Further, the catalyst composition prepared by this invention has a very low apparent density of 0.01˜0.50 g/ml as well as the catalyst composition affords high production yield (1,000˜1,800%) of carbon nanotube.
摘要翻译：本发明涉及使用喷雾热解法制备高收率合成碳纳米管的催化剂组合物的方法。更具体地说，本发明涉及制备用于合成碳纳米管的催化剂组合物的方法，包括以下步骤：i）将催化剂组合物的多组分金属前体溶解在去离子水中; ii）通过气体雾化法将得到的催化金属前体溶液喷涂到高温反应器中; iii）通过气体雾化材料的热解形成催化剂组合物粉末; 和iv）获得催化剂组合物粉末，其中所述催化剂组合物包含i）选自Fe或Co的主催化剂，ii）Al，iii）任选的助催化剂，选自Ni，Cu，Sn，Mo，Cr，Mn ，V，W，Ti，Si，Zr或Y，iv）Mg的非活性载体。此外，本发明制备的催化剂组合物具有非常低的表观密度为0.01〜0.50g / ml，催化剂组合物提供了高生产率（1,000〜1300％）的碳纳米管。

4. 发明授权

US09006132B2 Process for preparing catalyst composition for the synthesis of carbon nanotube with high yields using the spray pyrolysis method 有权
标题翻译：使用喷雾热解法制备高收率合成碳纳米管的催化剂组合物的方法
公开(公告)号：US09006132B2
公开(公告)日：2015-04-14
申请号：US13105663
申请日：2011-05-11
申请人： Sang-Hyo Ryu , Hyun-Kyung Sung , Namsun Choi , Wan Sung Lee , Dong Hwan Kim , Youngchan Jang
发明人： Sang-Hyo Ryu , Hyun-Kyung Sung , Namsun Choi , Wan Sung Lee , Dong Hwan Kim , Youngchan Jang
IPC分类号： B01J23/58 , B82Y40/00 , B01J23/745 , B01J23/75 , B01J23/78 , B01J23/887 , B01J35/00 , B01J37/08 , B82Y30/00 , D01F9/12 , D01F9/127
CPC分类号： B82Y40/00 , B01J23/745 , B01J23/75 , B01J23/78 , B01J23/8872 , B01J35/002 , B01J37/082 , B82Y30/00 , D01F9/12 , D01F9/127 , D01F9/1273 , Y10S977/74 , Y10S977/742 , Y10S977/84 , Y10S977/842 , Y10T428/298
摘要： The present invention relates to a process for preparing catalyst composition for the synthesis of carbon nanotube with high yields using the spray pyrolysis method. More particularly, this invention relates to a process for preparing catalyst composition for the synthesis of carbon nanotube comprising the steps of i) dissolving multi-component metal precursors of catalyst composition in de-ionized water; ii) spraying obtained catalytic metal precursor solution into the high temperature reactor by gas atomization method; iii) forming the catalyst composition powder by pyrolysis of gas atomized material; and iv) obtaining the catalyst composition powder, wherein said catalyst composition comprises i) main catalyst selected from Fe or Co, ii) Al, iii) optional co-catalyst at least one selected from Ni, Cu, Sn, Mo, Cr, Mn, V, W, Ti, Si, Zr or Y, iv) inactive support of Mg. Further, the catalyst composition prepared by this invention has a very low apparent density of 0.01˜0.50 g/ml as well as the catalyst composition affords high production yield (1,000˜1,800%) of carbon nanotube.
摘要翻译：本发明涉及使用喷雾热解法制备高收率合成碳纳米管的催化剂组合物的方法。更具体地说，本发明涉及制备用于合成碳纳米管的催化剂组合物的方法，包括以下步骤：i）将催化剂组合物的多组分金属前体溶解在去离子水中; ii）通过气体雾化法将得到的催化金属前体溶液喷涂到高温反应器中; iii）通过气体雾化材料的热解形成催化剂组合物粉末; 和iv）获得催化剂组合物粉末，其中所述催化剂组合物包含i）选自Fe或Co的主催化剂，ii）Al，iii）任选的助催化剂，选自Ni，Cu，Sn，Mo，Cr，Mn ，V，W，Ti，Si，Zr或Y，iv）Mg的非活性载体。此外，本发明制备的催化剂组合物具有非常低的表观密度为0.01〜0.50g / ml，催化剂组合物提供了高生产率（1,000〜1300％）的碳纳米管。

5. 发明授权

US08048821B2 Catalyst composition for the synthesis of thin multi-walled carbon nanotube and its manufacturing method 有权
标题翻译：用于合成薄壁多壁碳纳米管的催化剂组合物及其制备方法
公开(公告)号：US08048821B2
公开(公告)日：2011-11-01
申请号：US12472925
申请日：2009-05-27
申请人： Sang-Hyo Ryu , Dong Hwan Kim , Wan Sung Lee , Namsun Choi , Hyun-Kyung Sung , Youngchan Jang
发明人： Sang-Hyo Ryu , Dong Hwan Kim , Wan Sung Lee , Namsun Choi , Hyun-Kyung Sung , Youngchan Jang
IPC分类号： B01J23/32
CPC分类号： B01J21/185 , B01J23/002 , B01J23/78 , B01J23/862 , B01J23/881 , B01J23/888 , B01J23/8892 , B01J37/03 , B01J2523/00 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/06 , C01B2202/36 , Y10S423/40 , Y10S977/742 , Y10S977/842 , Y10S977/843 , B01J2523/22 , B01J2523/31 , B01J2523/842 , B01J2523/845 , B01J2523/72 , B01J2523/68 , B01J2523/67 , B01J2523/17
摘要： The present invention relates to a catalyst composition for the synthesis of thin multi-walled carbon nanotube (MWCNT) and a method for manufacturing a catalyst composition. More particularly, this invention relates to a multi-component metal catalyst composition comprising i) main catalyst of Fe and Al, ii) inactive support of Mg and iii) optional co-catalyst at least one selected from Co, Ni, Cr, Mn, Mo, W, V, Sn, or Cu. Further, the present invention affords thin multi-walled carbon nanotube having 5˜20 nm of diameter and 100˜10,000 of aspect ratio in a high yield.
摘要翻译：本发明涉及用于合成薄壁多壁碳纳米管（MWCNT）的催化剂组合物及其制备方法。更具体地说，本发明涉及多组分金属催化剂组合物，其包含i）Fe和Al的主要催化剂，ii）Mg的无活性载体和iii）任选的助催化剂，选自Co，Ni，Cr，Mn， Mo，W，V，Sn或Cu。此外，本发明以高产率提供直径5〜20nm，纵横比为100〜10000的薄壁多壁碳纳米管。

6. 发明申请

US20100207053A1 CATALYST COMPOSITION FOR THE SYNTHESIS OF THIN MULTI-WALLED CARBON NANOTUBE AND ITS MANUFACTURING METHOD 有权
标题翻译：用于合成多壁碳纳米管的催化剂组合物及其制造方法
公开(公告)号：US20100207053A1
公开(公告)日：2010-08-19
申请号：US12472925
申请日：2009-05-27
申请人： Sang-Hyo RYU , Dong Hwan Kim , Wang Sung Lee , Namsun Choi , Hyun-Kyung Sung , Youngchan Jang
发明人： Sang-Hyo RYU , Dong Hwan Kim , Wang Sung Lee , Namsun Choi , Hyun-Kyung Sung , Youngchan Jang
IPC分类号： D01F9/12 , B01J23/78 , B01J23/24 , B01J23/34 , B01J23/745 , H01B1/24 , C09K5/00 , C23C16/26
CPC分类号： B01J21/185 , B01J23/002 , B01J23/78 , B01J23/862 , B01J23/881 , B01J23/888 , B01J23/8892 , B01J37/03 , B01J2523/00 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/06 , C01B2202/36 , Y10S423/40 , Y10S977/742 , Y10S977/842 , Y10S977/843 , B01J2523/22 , B01J2523/31 , B01J2523/842 , B01J2523/845 , B01J2523/72 , B01J2523/68 , B01J2523/67 , B01J2523/17
摘要： The present invention relates to a catalyst composition for the synthesis of thin multi-walled carbon nanotube (MWCNT) and a method for manufacturing a catalyst composition. More particularly, this invention relates to a multi-component metal catalyst composition comprising i) main catalyst of Fe and Al, ii) inactive support of Mg and iii) optional co-catalyst at least one selected from Co, Ni, Cr, Mn, Mo, W, V, Sn, or Cu. Further, the present invention affords thin multi-walled carbon nanotube having 5˜20 nm of diameter and 100˜10,000 of aspect ratio in a high yield.
摘要翻译：本发明涉及用于合成薄壁多壁碳纳米管（MWCNT）的催化剂组合物及其制备方法。更具体地说，本发明涉及多组分金属催化剂组合物，其包含i）Fe和Al的主要催化剂，ii）Mg的无活性载体和iii）任选的助催化剂，选自Co，Ni，Cr，Mn， Mo，W，V，Sn或Cu。此外，本发明以高产率提供直径5〜20nm，纵横比为100〜10000的薄壁多壁碳纳米管。

7. 发明申请

US20100167053A1 Catalyst composition for preparing carbon nanotube 有权
标题翻译：用于制备碳纳米管的催化剂组合物
公开(公告)号：US20100167053A1
公开(公告)日：2010-07-01
申请号：US12453862
申请日：2009-05-26
申请人： Hyun-Kyung Sung , Wan Sung Lee , Namsun Choi , Dong Hwan Kim , Youngchan Jang
发明人： Hyun-Kyung Sung , Wan Sung Lee , Namsun Choi , Dong Hwan Kim , Youngchan Jang
IPC分类号： B32B5/16 , B01J21/08 , B01J21/10 , B01J23/847 , B01J23/22 , B01J23/75 , D01F9/12
CPC分类号： B01J23/8472 , B01J21/185 , B01J23/002 , B01J23/85 , B01J23/8892 , B01J37/03 , B01J37/16 , B01J2523/00 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/34 , C01B2202/36 , Y10S977/742 , Y10S977/843 , Y10T428/2982 , B01J2523/22 , B01J2523/55 , B01J2523/842 , B01J2523/845 , B01J2523/31 , B01J2523/41
摘要： The present invention relates to a catalyst composition for preparing carbon nanotube and a process for preparing carbon nanotube using the same. More particularly, this invention relates to a process for preparing carbon nanotube by the chemical vapor deposition method through the decomposition of lower saturated or unsaturated hydrocarbons using a multi-component metal catalyst composition containing active metal catalyst from Co, V, Al and inactive porous support. Further, the present invention affords the carbon nanotube having 5˜30 nm of diameter and 100˜10,000 of aspect ratio in a high catalytic yield.
摘要翻译：本发明涉及一种制备碳纳米管的催化剂组合物及其制备方法。更具体地说，本发明涉及一种通过化学气相沉积法使用含有Co，V，Al的活性金属催化剂和无活性多孔载体的多组分金属催化剂组合物分解低级饱和或不饱和烃制备碳纳米管的方法。此外，本发明以高催化率提供直径为5〜30nm，纵横比为100〜10000的碳纳米管。

8. 发明授权

US08202818B2 Catalyst composition for preparing carbon nanotube 有权
标题翻译：用于制备碳纳米管的催化剂组合物
公开(公告)号：US08202818B2
公开(公告)日：2012-06-19
申请号：US12453862
申请日：2009-05-26
申请人： Hyun-Kyung Sung , Wan Sung Lee , Namsun Choi , Dong Hwan Kim , Youngchan Jang
发明人： Hyun-Kyung Sung , Wan Sung Lee , Namsun Choi , Dong Hwan Kim , Youngchan Jang
IPC分类号： B01J21/00 , B01J23/20 , B01J23/00 , B01J23/32 , B01J23/58 , B01J23/70 , D01C5/00 , B32B5/16
CPC分类号： B01J23/8472 , B01J21/185 , B01J23/002 , B01J23/85 , B01J23/8892 , B01J37/03 , B01J37/16 , B01J2523/00 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/34 , C01B2202/36 , Y10S977/742 , Y10S977/843 , Y10T428/2982 , B01J2523/22 , B01J2523/55 , B01J2523/842 , B01J2523/845 , B01J2523/31 , B01J2523/41
摘要： The present invention relates to a catalyst composition for preparing carbon nanotube and a process for preparing carbon nanotube using the same. More particularly, this invention relates to a process for preparing carbon nanotube by the chemical vapor deposition method through the decomposition of lower saturated or unsaturated hydrocarbons using a multi-component metal catalyst composition containing active metal catalyst from Co, V, Al and inactive porous support. Further, the present invention affords the carbon nanotube having 5˜30 nm of diameter and 100˜10,000 of aspect ratio in a high catalytic yield.
摘要翻译：本发明涉及一种制备碳纳米管的催化剂组合物及其制备方法。更具体地说，本发明涉及一种通过化学气相沉积法使用含有Co，V，Al的活性金属催化剂和无活性多孔载体的多组分金属催化剂组合物分解低级饱和或不饱和烃制备碳纳米管的方法。此外，本发明以高催化率提供直径为5〜30nm，纵横比为100〜10000的碳纳米管。

9. 发明申请

US20090053608A1 Anode active material hybridizing carbon nanofiber for lithium secondary battery 审中-公开
标题翻译：用于锂二次电池的阳极活性材料杂化碳纳米纤维
公开(公告)号：US20090053608A1
公开(公告)日：2009-02-26
申请号：US12213830
申请日：2008-06-25
申请人： Im Goo Choi , Seung Yeon Jang , Namsun Choi , Hyun-Kyung Sung , Dong Hwan Kim , Youngchan Jang , Hangi Jung
发明人： Im Goo Choi , Seung Yeon Jang , Namsun Choi , Hyun-Kyung Sung , Dong Hwan Kim , Youngchan Jang , Hangi Jung
IPC分类号： H01M4/40
CPC分类号： H01M4/0428 , H01M4/133 , H01M4/1393 , H01M4/583 , H01M4/661 , H01M10/052
摘要： The present invention provides a composite silicon anode material hybridizing carbon nanofiber for lithium secondary battery prepared by the steps comprising: i) preparing a support made by amorphous silicon alloy after processing amorphous silicon and metal; ii) dispersing the catalyst selected from Fe, Co, Ni, Cu, Mg, Mn, Ti, Sn, Si, Zr, Zn, Ge, Pb or In on the surface of said support made by amorphous silicon alloy; and iii) growing the carbon nanofiber using a carbon source selected from carbon monoxide, methane, acetylene or ethylene on said support by a chemical vapor deposition method, wherein the amount of grown carbon nanofiber is 1˜110 wt % of the amount of said support.
摘要翻译：本发明提供了一种复合硅阳极材料，其与用于锂二次电池的碳纳米纤维杂交，所述复合硅阳极材料通过以下步骤制备，所述步骤包括：i）在加工非晶硅和金属之后制备由非晶硅合金制成的载体; ii）在由非晶硅合金制成的所述载体的表面上分散选自Fe，Co，Ni，Cu，Mg，Mn，Ti，Sn，Si，Zr，Zn，Ge，Pb或In中的催化剂; 以及iii）通过化学气相沉积法在所述载体上使用选自一氧化碳，甲烷，乙炔或乙烯的碳源生长碳纳米纤维，其中生长的碳纳米纤维的量为所述载体的量的1〜110重量％。

10. 发明授权

US06674287B2 Method for grouping unit cells using pattern matching technology of impedance spectrum 失效
标题翻译：使用阻抗谱图案匹配技术对单位单元进行分组的方法
公开(公告)号：US06674287B2
公开(公告)日：2004-01-06
申请号：US10208608
申请日：2002-07-30
申请人： Jee-Hwan Jang , Hyun-Kyung Sung , Sang-Hyo Ryu
发明人： Jee-Hwan Jang , Hyun-Kyung Sung , Sang-Hyo Ryu
IPC分类号： G01N27416
CPC分类号： H01M10/482
摘要： A method for grouping unit cells of a similar impedance spectrum uses pattern matching technology to optimize the performance of a battery pack made of primary or secondary batteries as the unit cells connected in series, in parallel or in combination of them. To make an optimal battery pack with unit cells of a different internal characteristic, the method includes measuring the impedance spectrum of the individual unit cell in a wide frequency region at the same temperature and in the same state of charge (SOC), digitizing the difference in impedance spectrum among the unit cells into a relative value using the pattern matching technology, and selecting unit cells of a most similar impedance spectrum (i.e., a smallest relative difference in impedance spectrum) to make a battery pack.
摘要翻译：用于对类似阻抗谱的单位单元进行分组的方法使用模式匹配技术来优化由主单元或二次电池组成的电池组的性能，所述单电池串联，并联或组合连接。为了制造具有不同内部特性的单位电池的最佳电池组，该方法包括在相同温度和相同充电状态（SOC）的宽频率区域中测量各单元电池的阻抗谱，数字化差分使用模式匹配技术将单位单元之间的阻抗谱转换成相对值，并选择最相似阻抗谱的单位单元（即，阻抗谱中的最小相对差），以制作电池组。

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