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    • 2. 发明公开
    • METHOD AND APPARATUS FOR PRODUCING METAL OXIDE PARTICLES
    • 生产金属氧化物颗粒的方法和设备
    • EP2544994A2
    • 2013-01-16
    • EP11713095.5
    • 2011-03-07
    • National University Corporation Hokkaido UniversityShowa Denko K.K.
    • OHTANI BunshoSUGISHITA NoriyukiKURODA Yasushi
    • C01B13/22C01G23/07C01G1/02
    • C01B13/22C01G1/02C01G23/07C01P2002/30C01P2004/03C01P2006/12C01P2006/90
    • There is provided a method and an apparatus for producing metal oxide particles, which produce metal oxide particles having a high photocatalytic activity with high yield. The method for producing metal oxide particles of the invention is characterized by including combining, in a reaction tube, a preheated metal chloride-containing gas with a preheated first gas which does not contain the metal chloride at a first junction to obtain a first combined gas, and combining the first combined gas with a preheated second gas which does not contain the metal chloride, at a second junction which is further downstream of the first junction, to obtain a second combined gas, wherein at least one of the metal chloride-containing gas and the first gas contains oxygen, and wherein the preheated metal chloride-containing gas is further heated in a region between the first junction and the second junction (referred to as first reaction zone), by combining the first gas with the metal chloride-containing gas at the first junction while setting the preheat temperature of the first gas at a temperature equal to or higher than the preheat temperature of the metal chloride-containing gas, and the first combined gas is further heated in a region downstream of the second junction by combining the second gas with the first combined gas at the second junction while setting the preheat temperature of the second gas at a temperature equal to or higher than the temperature of the first combined gas.
    • 提供一种制造金属氧化物粒子的方法和装置,其以高收率制造光催化活性高的金属氧化物粒子。 本发明的金属氧化物粒子的制造方法的特征在于,在反应管中,将含有预热金属氯化物的气体与在第一接合部不含有金属氯化物的预热后的第一气体组合,得到第一合成气体 ,并且在第一结的更下游的第二结处将第一结合气与预热的不含金属氯化物的第二气体结合以获得第二结合气,其中至少一种含金属氯化物的 气体并且第一气体含有氧,并且其中预热的含金属氯化物的气体在第一结和第二结之间的区域(称为第一反应区)中进一步加热,通过将第一气体与金属氯化物 - 同时将第一气体的预热温度设定为等于或高于金属氯化物-c的预热温度的温度 并且通过在第二结合处将第二气体与第一合并气体合并,同时将第二气体的预热温度设定为等于或高于第二结合处的温度 第一组合气体的温度。