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1. 发明申请

US20100196765A1 Reducing DC Resistance In Electrochemical Cells By Increasing Cathode Basis Weight 审中-公开
标题翻译：通过增加阴极基重降低电化学电池中的直流电阻
公开(公告)号：US20100196765A1
公开(公告)日：2010-08-05
申请号：US11163644
申请日：2005-10-26
申请人： Marcus Palazzo , Esther Takeuchi , Randolph Leising
发明人： Marcus Palazzo , Esther Takeuchi , Randolph Leising
IPC分类号： H01M6/16 , H01M4/00 , H01M10/26 , H01M4/58 , H01M4/82 , H01M10/04
CPC分类号： H01M6/16 , H01M4/0404 , H01M4/08 , H01M4/483 , H01M4/54 , Y10T29/49115
摘要： The use of an increased cathode weight and thickness or basis weight in a primary electrochemical cell for the purpose of reducing DC resistance (Rdc) is described. This is particularly important when the cell is subjected to high rate discharge conditions of the type typically required for medical device applications, such as activating a cardiac defibrillator. A preferred couple is of a lithium/silver vanadium oxide (Li/SVO) cell or a lithium/copper silver vanadium oxide (Li/CSVO) cell. Reducing cell Rdc by increasing basis weight has the added benefit of increasing the cell's energy density through comparatively greater amounts of active cathode material in a give casing volume.
摘要翻译：描述了用于降低直流电阻（Rdc）的原电化学电池中增加的阴极重量和厚度或基重的用途。当电池经受医疗器械应用通常所需类型的高速率放电条件（例如激活心脏除颤器）时，这尤其重要。优选的一对是锂/银钒氧化物（Li / SVO）电池或锂/铜银钒氧化物（Li / CSVO）电池。通过增加单位面积重量减少细胞Rdc具有增加细胞能量密度的附加益处，通过在给套管体积中相对较大量的活性阴极材料。

2. 发明授权

US07432001B1 Prevention of lithium deposition in nonaqueous electrolyte cells by electrolyte-to-cathode weight ratio 有权
标题翻译：通过电解液 - 阴极重量比防止非水电解质电池中的锂沉积
公开(公告)号：US07432001B1
公开(公告)日：2008-10-07
申请号：US11007933
申请日：2004-12-09
申请人： Esther S. Takeuchi , Randolph Leising , Marcus Palazzo
发明人： Esther S. Takeuchi , Randolph Leising , Marcus Palazzo
IPC分类号： H01M2/22 , H01M4/54
CPC分类号： H01M2/266 , H01M4/131 , H01M4/133 , H01M4/485 , H01M4/54 , H01M4/583 , H01M6/16
摘要： The prevention of lithium clusters from bridging between the negative and positive portions of a cell during discharge is described. This is done by limiting the amount of electrolyte in the cell, thereby eliminating excess electrolyte pooling above the cell stack. It is in this excess electrolyte that a relatively higher Li+ ion concentration can occur, creating an anodically polarized region resulting in the reduction of lithium ions on the negative and positive surfaces as the concentration gradient is relaxed. Typically, a lithium ion concentration gradient sufficient to cause lithium cluster formation is induced by the high rate, intermittent discharge of a lithium/silver vanadium oxide (Li/SVO) cell.
摘要翻译：描述了在放电期间防止锂簇在电池的负极部分和正极部分之间的桥接。这通过限制电池中的电解质的量来实现，从而消除电池堆上方的多余的电解液池。在这种过量的电解质中，可能发生相对较高的Li + +离子浓度，产生阳极极化区域，导致当浓度梯度松弛时，负极和正极表面上的锂离子的还原。通常，通过锂/银钒氧化物（Li / SVO）电池的高速率间歇放电，引起足以引起锂簇形成的锂离子浓度梯度。

3. 发明授权

US07026791B2 Electrochemical treatment method to reduce voltage delay and cell resistance in lithium/silver vanadium oxide cells 有权
标题翻译：电化学处理方法，以减少锂/银氧化钒电池的电压延迟和电池电阻
公开(公告)号：US07026791B2
公开(公告)日：2006-04-11
申请号：US10763945
申请日：2004-01-22
申请人： Marcus Palazzo , Esther S. Takeuchi , Randolph Leising
发明人： Marcus Palazzo , Esther S. Takeuchi , Randolph Leising
IPC分类号： H02J7/00 , A61N1/18
CPC分类号： H01M10/44 , H01M4/483 , H01M4/54 , H01M6/16
摘要： It is known that reforming implantable defibrillator capacitors at least partially restores and preserves their charging efficiency. An industry-recognized standard is to reform implantable capacitors by pulse discharging the connected electrochemical cell about once every three months throughout the useful life of the medical device. A Li/SVO cell typically powers such devices. The present invention relates to methodologies for significantly minimizing, if not entirely eliminating, the occurrence of voltage delay and irreversible Rdc growth in the about 35% to 70% DOD region by subjecting Li/SVO cells to novel discharge regimes. At the same time, the connected capacitors in the cardiac defibrillator are reformed to maintain them at their rated breakdown voltages.
摘要翻译：众所周知，重组可植入除颤器电容器至少部分恢复并保持其充电效率。行业公认的标准是通过在医疗设备的整个使用寿命期间每三个月大约一次脉冲地排放连接的电化学电池来重建可植入电容器。 Li / SVO单元通常为这些设备供电。本发明涉及通过使Li / SVO细胞经受新颖的放电方式，使大约35％至70％的DOD区域中的电压延迟和不可逆Rdc生长显着最小化（如果不是完全消除）的方法。同时，将心脏除颤器中连接的电容器进行重整，以将其维持在额定击穿电压。

4. 发明授权

US06803147B2 Silver vanadium oxide having low internal resistance and method of manufacture 失效
标题翻译：具有低内阻的银氧化钒和制造方法
公开(公告)号：US06803147B2
公开(公告)日：2004-10-12
申请号：US10037133
申请日：2001-12-27
申请人： Esther S. Takeuchi , Marcus Palazzo
发明人： Esther S. Takeuchi , Marcus Palazzo
IPC分类号： H01M454
CPC分类号： C01G31/00 , C01P2006/40 , H01M4/48 , H01M4/483 , H01M4/5825 , H01M6/16
摘要： The current invention relates to the preparation of an improved cathode active material for non-aqueous lithium electrochemical cell. In particular, the cathode active material comprises &egr;-phase silver vanadium oxide prepared by using a &ggr;-phase silver vanadium oxide starting material. The reaction of &ggr;-phase SVO with a silver salt produces the novel &egr;-phase SVO possessing a lower surface area than &egr;-phase SVO produced from vanadium oxide (V2O5) and a similar silver salt as starting materials. Consequently, the low surface area &egr;-phase SVO material provides an advantage in greater long term stability in pulse dischargeable cells.
摘要翻译：本发明涉及用于非水电解锂电化学电池的改进的阴极活性材料的制备。特别地，正极活性物质包括通过使用γ相银钒氧化物原料制备的ε相银钒氧化物。 γ相SVO与银盐的反应产生具有比由氧化钒（V2O5）和类似的银盐作为起始原料产生的ε相SVO更低的表面积的新型ε相SVO。因此，低表面积ε相SVO材料在脉冲可放电电池的更长的长期稳定性方面提供了优点。

5. 发明授权

US5962720A Method of synthesizing unsymmetric organic carbonates and preparing nonaqueous electrolytes for alkali ion electrochemical cells 失效
标题翻译：合成不对称有机碳酸盐和制备碱性离子电化学电池非水电解质的方法
公开(公告)号：US5962720A
公开(公告)日：1999-10-05
申请号：US865236
申请日：1997-05-29
申请人： Hong Gan , Marcus Palazzo , Esther S. Takeuchi
发明人： Hong Gan , Marcus Palazzo , Esther S. Takeuchi
IPC分类号： C07C68/06 , C07C69/96 , H01M6/16 , H01M10/052 , H01M10/0525 , H01M10/0569 , H01M10/36
CPC分类号： H01M10/052 , C07C68/06 , H01M10/0569 , H01M10/0525 , H01M2300/0025 , Y02P20/582
摘要： The present invention relates to an improved method of synthesizing unsymmetric linear organic carbonates comprising the reaction of two symmetric dialkyl carbonates, R.sup.1 and R.sup.2, in the presence of a nucleophilic reagent or an election donating reductant as a catalyst, wherein R.sup.1 and R.sup.2 can be either saturated or unsaturated alkyl or aryl groups, is described. The present invention further provides a preparation method for a nonaqueous organic electrolyte having an unsymmetric linear organic carbonate as a co-solvent.
摘要翻译：本发明涉及一种合成不对称线性有机碳酸酯的改进方法，其包括在亲核试剂或选择供体还原剂作为催化剂存在下，两种对称的碳酸二烷基酯R 1和R 2的反应，其中R 1和R 2可以是饱和或不饱和的烷基或芳基。本发明还提供了具有不对称线性有机碳酸酯作为助溶剂的非水有机电解质的制备方法。

6. 发明授权

US08906549B1 Development of mixed binder system for primary cell cathodes 有权
标题翻译：用于初级电池阴极的混合粘合剂体系的开发
公开(公告)号：US08906549B1
公开(公告)日：2014-12-09
申请号：US13241508
申请日：2011-09-23
申请人： Marcus Palazzo
发明人： Marcus Palazzo
IPC分类号： H01M4/13
CPC分类号： H01M4/661 , H01M4/131 , H01M4/1391 , H01M4/364 , H01M4/5815 , H01M4/622
摘要： The invention is directed to an SVO electrochemical cell having high rate capability. The cathode is produced by coating a mixture of an active material, conductive additives, a mixed binder, and an aluminum foil current collector. The mixed binder consists of a mixture of styrene butadiene with PVDF. The use of the styrene butadiene maintains adhesion to the conductive current collector while the PVDF portion of the binder gives flexibility. A particularly preferred couple is of a lithium/silver vanadium oxide (Li/SVO) chemistry and the binder mixture enables an active slurry of SVO to be coated onto a current collector without delamination.
摘要翻译：本发明涉及具有高速率能力的SVO电化学电池。通过涂覆活性材料，导电添加剂，混合粘合剂和铝箔集电体的混合物来制造阴极。混合的粘合剂由苯乙烯丁二烯与PVDF的混合物组成。苯乙烯丁二烯的使用保持与导电集电体的粘附性，而粘合剂的PVDF部分具有柔性。特别优选的一对是锂/银钒氧化物（Li / SVO）化学，并且粘合剂混合物使SVO的活性浆料能够涂覆在集电器上而不会分层。

7. 发明授权

US06797019B2 Electrochemical cell having an electrode of silver vanadium oxide coated to a current collector 失效
标题翻译：具有涂覆在集电体上的银钒氧化物电极的电化学电池
公开(公告)号：US06797019B2
公开(公告)日：2004-09-28
申请号：US10013287
申请日：2001-12-10
申请人： Esther S. Takeuchi , Randolph A. Leising , Marcus Palazzo
发明人： Esther S. Takeuchi , Randolph A. Leising , Marcus Palazzo
IPC分类号： H01M600
CPC分类号： H01M4/623 , H01M4/0404 , H01M4/48 , H01M4/54 , H01M4/583 , H01M4/621 , H01M4/661 , H01M10/0525 , Y10T29/49115
摘要： The invention is directed to an SVO electrochemical cell having high rate capability. The cathode is produced by coating a mixture of an active material, conductive additives, a mixed binder, and an aluminum foil current collector. The mixed binder consists of a mixture of heat treated polyamic acid with PVDF. The use of heat treated polyamic acid maintains adhesion to the conductive current collector while the PVDF portion of the binder gives flexibility. A particularly preferred couple is of a lithium/silver vanadium oxide (Li/SVO) chemistry and the binder mixture enables an active slurry of SVO to be coated onto a current collector without delamination.
摘要翻译：本发明涉及具有高速率能力的SVO电化学电池。通过涂覆活性材料，导电添加剂，混合粘合剂和铝箔集电体的混合物来制造阴极。混合的粘合剂由热处理的聚酰胺酸与PVDF的混合物组成。使用热处理的聚酰胺酸保持对导电集电体的粘附，同时粘合剂的PVDF部分具有柔性。特别优选的一对是锂/银钒氧化物（Li / SVO）化学，并且粘合剂混合物使SVO的活性浆料能够涂覆在集电器上而不会分层。

8. 发明授权

US06759164B2 Use of heat-treated electrodes containing a polyamic acid-PVDF binder mixture 失效
标题翻译：使用含有聚酰胺酸PVDF粘合剂混合物的热处理电极
公开(公告)号：US06759164B2
公开(公告)日：2004-07-06
申请号：US09995202
申请日：2001-11-27
申请人： Marcus Palazzo , Esther S. Takeuchi
发明人： Marcus Palazzo , Esther S. Takeuchi
IPC分类号： H01M462
CPC分类号： H01M4/621 , C08L27/00 , C08L2666/04 , C09J179/08 , H01M4/0471 , H01M4/1391 , H01M4/1393 , H01M4/1395 , H01M4/1397 , H01M4/405 , H01M4/54 , H01M4/622 , H01M4/623 , H01M6/16 , H01M10/0525 , H01M10/0566
摘要： A mixture of polymeric binders that is insoluble in nonaqueous organic electrolytes activating alkali metal or alkali metal ion electrochemical cells, is described. The mixed binder formulation provides electrodes that are flexible and non-brittle, and cells incorporating the electrodes are dischargeable at elevated temperatures. A preferred binder formulation is a mixture of polyvinylidene and polyimide binders.
摘要翻译：描述了不溶于活化碱金属或碱金属离子电化学电池的非水有机电解质的聚合物粘合剂的混合物。混合粘合剂制剂提供柔性和非脆性的电极，并且结合电极的电池在升高的温度下可放电。优选的粘合剂制剂是聚偏二氟乙烯和聚酰亚胺粘合剂的混合物。

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