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1. 发明授权

US6124122A Process for preparing optically pure (S)-3-hydroxy-.gamma.-butyrolactone 失效
标题翻译：制备光学纯（S）-3-羟基-γ-丁内酯的方法
公开(公告)号：US6124122A
公开(公告)日：2000-09-26
申请号：US359678
申请日：1999-07-23
申请人： Jongpil Chun , Yik-haeng Cho , Young Mi Park , Kyoung Rok Roh , Hosung Yu , Dae Il Hwang
发明人： Jongpil Chun , Yik-haeng Cho , Young Mi Park , Kyoung Rok Roh , Hosung Yu , Dae Il Hwang
IPC分类号： C07C69/675 , C07B53/00 , C07B61/00 , C07C51/285 , C07C67/08 , C07C69/003 , C07D307/32 , C07D307/33 , C12P7/42 , C12P7/62 , C12P17/04 , C12P19/14 , C12P19/16 , C12P19/22
CPC分类号： C07D307/33 , C12P17/04 , C12P19/14 , C12P19/22 , C12P7/42 , C07B2200/07
摘要： The present invention relates to a process for preparing optically pure (S)-3-hydroxy-.gamma.-butyrolactone expressed by the following Formula 1 and more particularly, to a process that enables preparing optically pure (S)-3-hydroxy-.gamma.-butyrolactone economically in large quantities, by:(a) Preparing .alpha.-(1,4) linked oligosaccharide with adequate sugar distribution by reacting amylopectin which is easily available from natural product with enzyme under a specific condition; and(b) Performing oxidation, esterification and cyclization sequentially under a specific condition. ##STR1##
摘要翻译：本发明涉及一种制备由下式1表示的光学纯的（S）-3-羟基-γ-丁内酯的方法，更具体地说，涉及能够制备光学纯的（S）-3-羟基-γ-丁内酯的方法，通过以下方式经济地制备丁内酯：（a）通过在天然产物中容易获得的支链淀粉与酶在特定条件下反应制备具有足够糖分布的α-（1,4）连接的寡糖; 和（b）在特定条件下依次进行氧化，酯化和环化。

2. 发明授权

US06221639B1 Process for preparing optically pure(S)-3,4-dihydroxybutyric acid derivatives 失效
标题翻译：光学纯（S）-3,4-二羟基丁酸衍生物的制备方法
公开(公告)号：US06221639B1
公开(公告)日：2001-04-24
申请号：US09359679
申请日：1999-07-23
申请人： Yik-haeng Cho , Jongpil Chun , Young Mi Park , Kyoung Rok Roh , Hosung Yu , Dae Il Hwang
发明人： Yik-haeng Cho , Jongpil Chun , Young Mi Park , Kyoung Rok Roh , Hosung Yu , Dae Il Hwang
IPC分类号： C12P762
CPC分类号： C07D307/33 , C07B2200/07 , C12P7/42 , C12P17/04 , C12P19/14 , C12P19/22
摘要： The present invention relates to a process for preparing optically pure (S)-3,4-dihydroxybutyric acid derivatives expressed by the following Formula 1 and more particularly, to a process that enables preparing optically pure (S)-3,4-dihydroxybutyric acid derivatives economically in large quantities, by: (a) Preparing &agr;-(1,4)-linked oligosaccharide with adequate sugar distribution by reacting amylopectin which is easily available from natural product with enzyme under a specific condition; and (b) Performing oxidation and esterification sequentially under a specific condition. wherein, R represents linear or branched alkyl group with 1˜5 carbon atoms.
摘要翻译：本发明涉及一种制备光学纯的（S）-3,4-二羟基丁酸衍生物的方法，该衍生物由下式1表示，更具体地说，涉及能够制备光学纯的（S）-3,4-二羟基丁酸通过以下方式经济地制备衍生物：（a）通过在天然产物中容易获得的支链淀粉与酶在特定条件下反应制备具有足够糖分布的α-（1,4）连接的寡糖; 和（b）在特定条件下依次进行氧化和酯化。其中R表示具有1〜5个碳原子的直链或支链烷基。

3. 发明授权

US06288272B1 Continuous process for preparing optically pure (s)-3,4-dihydroxybutyric acid derivatives 失效
标题翻译：用于制备光学纯的（S）-3,4-二羟基丁酸衍生物的连续方法
公开(公告)号：US06288272B1
公开(公告)日：2001-09-11
申请号：US09359676
申请日：1999-07-23
申请人： Kyoung Rok Roh , Jongpil Chun , Yik-haeng Cho , Young Mi Park , Hosung Yu , Dae Il Hwang
发明人： Kyoung Rok Roh , Jongpil Chun , Yik-haeng Cho , Young Mi Park , Hosung Yu , Dae Il Hwang
IPC分类号： C07C6966
CPC分类号： C07D307/33 , C07B2200/07 , C12P7/42 , C12P17/04 , C12P19/14 , C12P19/22
摘要： The present invention relates to a continuous process for preparing optically pure (S)-3,4-dihydroxybutyric acid derivatives expressed by the following Formula 1 and more particularly, to the continuous process which enables preparing optically pure (S)-3,4-dihydroxybutyric acid derivatives economically in large quantities, by: (a) Preparing &agr;-(1,4) linked oligosaccharide having adequate sugar distribution by reacting amylopectin which is easily available from natural product with enzyme under a specific condition; and (b) Performing oxidatioin by running basic anion exchange resin with an oxidant to give (S)-3,4-dihydroxybutyric acid-anion exchange resin complex, dissociating the (S)-3,4-dihydroxybutyric acid from anion exchange resin complex and esterification sequentially under a specific condition. wherein Represents linear or branched alkyl group with 1˜5 carbon atoms.
摘要翻译：本发明涉及用于制备由下式1表示的光学纯的（S）-3,4-二羟基丁酸衍生物的连续方法，更具体地说，涉及能够制备光学纯的（S）-3,4-二羟基丁酸衍生物的连续方法，通过以下方式经济地制备二羟基丁酸衍生物：（a）通过使天然产物容易获得的支链淀粉与酶在特定条件下反应制备具有足够糖分布的α-（1,4）连接的寡糖; 和（b）通过用氧化剂运行碱性阴离子交换树脂来进行氧化，得到（S）-3,4-二羟基丁酸 - 阴离子交换树脂配合物，使（S）-3,4-二羟基丁酸与阴离子交换树脂复合物并在特定条件下依次酯化。其中表示具有1〜5个碳原子的直链或支链烷基。

4. 发明授权

US06586616B1 Process for preparing(R)-4-cyano-3-hydroxybutyric acid ester 失效
标题翻译：制备（R）-4-氰基-3-羟基丁酸酯的方法
公开(公告)号：US06586616B1
公开(公告)日：2003-07-01
申请号：US09889978
申请日：2001-07-25
申请人： Kyoung Rok Roh , Ho Sung Yu , Kyung Il Kim , Won Jang Lee , Dae Il Hwang
发明人： Kyoung Rok Roh , Ho Sung Yu , Kyung Il Kim , Won Jang Lee , Dae Il Hwang
IPC分类号： C07C25300
CPC分类号： C07C253/00 , C07B2200/07 , C07C255/20
摘要： The present invention relates to a process for preparing (R)-4-cyano-3-hydroxybutyric acid ester derivatives and more particularly, to a process for preparing optically pure (R)-4-cyano-3-hydroxybutyric acid ester derivatives expressed by formula (1) in high yield by performing cyanation and sequential esterification of (S)-3,4-epoxybutyric acid salt as a starting material. In said formula, R represents linear or branched alkyl group with 1˜5 carbon atoms or benzyl group.
摘要翻译：本发明涉及一种制备（R）-4-氰基-3-羟基丁酸酯衍生物的方法，更具体地说，涉及制备光学纯的（R）-4-氰基-3-羟基丁酸酯衍生物的方法，该衍生物由通过（S）-3,4-环氧丁酸盐作为起始原料进行氰化和连续酯化，高产率的式（1）。在所述式中，R表示具有1〜5个碳原子的直链或支链烷基或苄基。

5. 发明授权

US06417403B1 Process for preparing chiral (s)-2,3-disubstituted-1-propylamine derivatives 失效
标题翻译：制备手性-2,3-二取代-1-丙胺衍生物的方法
公开(公告)号：US06417403B1
公开(公告)日：2002-07-09
申请号：US09673123
申请日：2000-12-07
申请人： Kyoung Rok Roh , Jung Hwan Lee , Dae Il Hwang , Won Jang Lee , Kyung-Il Kim
发明人： Kyoung Rok Roh , Jung Hwan Lee , Dae Il Hwang , Won Jang Lee , Kyung-Il Kim
IPC分类号： C07C20950
CPC分类号： C07C209/56 , C07C213/02
摘要： A process for the preparation of chiral (S)-2,3-disubstituted-1-propylamine derivatives, in which a carbonyl group of (S) 3,4-disubstituted-1-butanecarbonyl derivatives is converted to an amine group, and the conversion reaction is performed through Curtius rearrangement or Hoffman rearrangement.
摘要翻译：一种制备手性（S）-2,3-二取代-1-丙胺衍生物的方法，其中（S）3,4-二取代-1-丁烷羰基衍生物的羰基转化成胺基，转化反应通过Curtius重排或Hoffman重排进行。

6. 发明授权

US08475995B2 Toner having core-shell structure and method of preparing the same 有权
标题翻译：具有核 - 壳结构的调色剂及其制备方法
公开(公告)号：US08475995B2
公开(公告)日：2013-07-02
申请号：US12739706
申请日：2008-10-22
申请人： Dae Il Hwang , Woo Young Yang , Keon Il Kim , Il Hyuk Kim , Jae Bum Park , Il Sun Hwang , Jae Kwang Hwang , Dae Woong Choi , Dong Won Kim , Duck Kyun Ahn
发明人： Dae Il Hwang , Woo Young Yang , Keon Il Kim , Il Hyuk Kim , Jae Bum Park , Il Sun Hwang , Jae Kwang Hwang , Dae Woong Choi , Dong Won Kim , Duck Kyun Ahn
IPC分类号： G03G9/093
CPC分类号： G03G9/09392 , G03G9/09328 , G03G9/09342 , G03G9/09371 , G03G9/09378 , G03G9/09385
摘要： A toner has a core-shell structure including a toner core portion having a resin with an active hydrogenactive hydrogen containing group, a colorant and at least one additive, and a toner shell portion surrounding the toner core portion, wherein the toner shell portion includes a cross-linked resin prepared by reaction of at least a portion of the active hydrogen containing group and the cross-linking agent.
摘要翻译：调色剂具有芯壳结构，其包括具有含活性氢活性氢基团的树脂的调色剂核心部分，着色剂和至少一种添加剂，以及包围调色剂核心部分的调色剂壳体部分，其中调色剂壳体部分包括通过至少一部分含活性氢的基团与交联剂的反应制备的交联树脂。

7. 发明申请

US20100098462A1 METHOD OF PREPARING TONER USING MICRO-SUSPENSION PARTICLES AND TONER PREPARED USING THE METHOD DIGITAL IMAGE DATA 有权
标题翻译：使用微悬浮颗粒制备调色剂的方法和使用方法数字图像数据制备的调色剂
公开(公告)号：US20100098462A1
公开(公告)日：2010-04-22
申请号：US12528314
申请日：2008-02-20
申请人： Woo Young Yang , Keon Il Kim , Dae Il Hwang , Jae Bum Park , Il Sun Hwang , Jun Hee Lee , Jae Kwang Hwang , Dong Won Kim , Duck Kyun Ahn
发明人： Woo Young Yang , Keon Il Kim , Dae Il Hwang , Jae Bum Park , Il Sun Hwang , Jun Hee Lee , Jae Kwang Hwang , Dong Won Kim , Duck Kyun Ahn
IPC分类号： G03G15/08 , G03G9/08 , G03G9/09 , G03G9/087
CPC分类号： G03G9/0804 , G03G9/08755 , G03G9/08791 , G03G9/08795 , G03G9/08797
摘要： A method of preparing a toner using a micro-suspension particle, includes preparing a mixture by mixing a resin having acidic groups, a master batch of coloring pigment, and at least one additive with an organic solvent, and then neutralizing the acid groups of the resin with a base; forming a micro-suspension by adding the prepared mixture to a dispersion medium; and forming a toner composition by removing the organic solvent from the prepared micro-suspension. Therefore, the method of preparing a toner using the disclosed micro-suspension particle and a toner prepared using the same can save manufacturing costs, and can improve charging ability and cleaning properties of the toner.
摘要翻译：使用微悬浮颗粒制备调色剂的方法包括通过将具有酸性基团的树脂，着色颜料的母料和至少一种添加剂与有机溶剂混合制备混合物，然后中和酸性基团树脂与底座; 通过将制备的混合物加入到分散介质中形成微悬浮液; 以及通过从制备的微悬浮液中除去有机溶剂来形成调色剂组合物。因此，使用所公开的微悬浮颗粒制备调色剂的方法和使用其制备的调色剂可以节省制造成本，并且可以改善调色剂的充电能力和清洁性能。

8. 发明授权

US08389196B2 Method of preparing toner 有权
标题翻译：调色剂的制备方法
公开(公告)号：US08389196B2
公开(公告)日：2013-03-05
申请号：US12678489
申请日：2008-09-19
申请人： Woo Young Yang , Keon Il Kim , Dae Il Hwang , Il Hyuk Kim , Jae Bum Park , Il Sun Hwang , Jae Kwang Hwang , Dae Woong Choi , Dong Won Kim , Duck Kyun Ahn
发明人： Woo Young Yang , Keon Il Kim , Dae Il Hwang , Il Hyuk Kim , Jae Bum Park , Il Sun Hwang , Jae Kwang Hwang , Dae Woong Choi , Dong Won Kim , Duck Kyun Ahn
IPC分类号： G03G9/08
CPC分类号： G03G9/0806 , G03G9/0819 , G03G9/0827
摘要： Provided is a method of preparing a toner, the method including: preparing a solvent emulsion by stirring a medium including a polar medium, an organic solvent, and a surfactant; adding toner components including a resin and a pigment to the solvent emulsion; removing the organic solvent from the solvent emulsion including the toner components; and collecting a toner particle from the solvent emulsion from which the organic solvent is removed.
摘要翻译：提供一种调色剂的制备方法，该方法包括：通过搅拌包含极性介质，有机溶剂和表面活性剂的介质来制备溶剂乳液; 向所述溶剂乳液中添加包括树脂和颜料的调色剂组分; 从包括调色剂组分的溶剂乳液中除去有机溶剂; 并从除去有机溶剂的溶剂乳液中收集调色剂颗粒。

9. 发明申请

US20100232837A1 TONER HAVING CORE-SHELL STRUCTURE AND METHOD OF PREPARING THE SAME 有权
标题翻译：具有芯壳结构的调色剂及其制备方法
公开(公告)号：US20100232837A1
公开(公告)日：2010-09-16
申请号：US12739706
申请日：2008-10-22
申请人： Dae Il Hwang , Woo Young Yang , Keon Il Kim , Il Hyuk Kim , Jae Bum Park , Il Sun Hwang , Jae Kwang Hwang , Dae Woong Choi , Dong Won Kim , Duck Kyun Ahn
发明人： Dae Il Hwang , Woo Young Yang , Keon Il Kim , Il Hyuk Kim , Jae Bum Park , Il Sun Hwang , Jae Kwang Hwang , Dae Woong Choi , Dong Won Kim , Duck Kyun Ahn
IPC分类号： G03G15/08 , G03G9/08 , G03G9/097 , G03G9/09 , G03G9/093
CPC分类号： G03G9/09392 , G03G9/09328 , G03G9/09342 , G03G9/09371 , G03G9/09378 , G03G9/09385
摘要： A toner has a core-shell structure including a toner core portion having a resin with an active hydrogenactive hydrogen containing group, a colorant and at least one additive, and a toner shell portion surrounding the toner core portion, wherein the toner shell portion includes a cross-linked resin prepared by reaction of at least a portion of the active hydrogen containing group and the cross-linking agent.
摘要翻译：调色剂具有芯壳结构，其包括具有含活性氢活性氢基团的树脂的调色剂核心部分，着色剂和至少一种添加剂，以及包围调色剂核心部分的调色剂壳体部分，其中调色剂壳体部分包括通过至少一部分含活性氢的基团与交联剂的反应制备的交联树脂。

10. 发明授权

US08389188B2 Toner using resin having active hydrogen-containing group and method of preparing the same 有权
标题翻译：使用具有含活性氢基团的树脂的调色剂及其制备方法
公开(公告)号：US08389188B2
公开(公告)日：2013-03-05
申请号：US12739699
申请日：2008-10-22
申请人： Dong Won Kim , Woo Young Yang , Keon Il Kim , Dae Il Hwang , Il Hyuk Kim , Jae Bum Park , Il Sun Hwang , Jae Kwang Hwang , Dae Woong Choi , Duck Kyun Ahn
发明人： Dong Won Kim , Woo Young Yang , Keon Il Kim , Dae Il Hwang , Il Hyuk Kim , Jae Bum Park , Il Sun Hwang , Jae Kwang Hwang , Dae Woong Choi , Duck Kyun Ahn
IPC分类号： G03G9/087
CPC分类号： G03G9/08793 , G03G9/0804 , G03G9/0825
摘要： Provided are a toner using a resin having an active hydrogen-containing group, and a method of preparing the toner. The toner using a resin having an active hydrogen-containing group includes a binder resin (A), a cross-linked resin including a THF insoluble content of 99-100 weight %, a colorant, and at least one additive. The cross-linked resin is arranged in the form of a plurality of islands in each particle of the toner.
摘要翻译：提供使用具有含活性氢基团的树脂的调色剂和调色剂的制备方法。使用具有含活性氢基团的树脂的调色剂包括粘合剂树脂（A），包含不饱和THF含量为99-100重量％的交联树脂，着色剂和至少一种添加剂。交联树脂以调色剂的每个颗粒中的多个岛的形式布置。

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