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1. 发明授权

US5976284A Patterned conducting polymer surfaces and process for preparing the same and devices containing the same 失效
标题翻译：图案化导电聚合物表面及其制备方法和含有其的装置
公开(公告)号：US5976284A
公开(公告)日：1999-11-02
申请号：US855018
申请日：1997-05-12
申请人： Jeffrey M. Calvert , Terrence G. Vargo , Ranganathan Shashidhar , Mu-San Chen
发明人： Jeffrey M. Calvert , Terrence G. Vargo , Ranganathan Shashidhar , Mu-San Chen
IPC分类号： G02F1/1333 , G02F1/1343 , G03F7/00 , H01B1/12 , H05K3/02 , H01B7/02
CPC分类号： H05K3/02 , G02F1/13439 , G03F7/00 , G03F7/0007 , H01B1/125 , H01B1/127 , H01B1/128 , H01G11/48 , H01G11/56 , G02F1/133305 , Y02E60/13
摘要： Patterned conducting polymer surfaces exhibiting excellent properties may be prepared by:(a) forming a surface of a conducting polymer on a surface of a substrate;(b) forming a surface of a blocking material on said surface of said conducting polymer in a pattern-wise fashion, to obtain a first patterned surface containing regions of exposed conducting polymer and regions of blocking material;(c) treating said first patterned surface with an agent which: (i) removes said conducting polymer from said regions of exposed conducting polymer; (ii) decreases the conductivity of said conducting polymer in said regions of exposed conducting polymer; or (iii) increases the conductivity of said conducting polymer in said regions of exposed conducting polymer; and(d) removing said blocking material to obtain a second patterned surface containing an exposed pattern of conducting polymer.
摘要翻译：表现出优异性能的图案化的导电聚合物表面可以通过以下步骤制备：（a）在基材的表面上形成导电聚合物的表面; （b）以图案方式在所述导电聚合物的所述表面上形成阻挡材料的表面，以获得含有暴露的导电聚合物区域和阻挡材料区域的第一图案化表面; （c）用试剂处理所述第一图案化表面，所述试剂：（i）从暴露的导电聚合物的所述区域除去所述导电聚合物; （ii）降低所述导电聚合物在所述暴露的导电聚合物区域中的导电性; 或（iii）增加所述导电聚合物在暴露的导电聚合物的所述区域中的导电性; 和（d）去除所述阻挡材料以获得包含暴露的导电聚合物图案的第二图案化表面。

2. 发明授权

US5945486A Fluoropolymeric substrates with metallized surfaces and methods for producing the same 失效
标题翻译：具有金属化表面的含氟聚合物基材及其制备方法
公开(公告)号：US5945486A
公开(公告)日：1999-08-31
申请号：US939490
申请日：1997-09-29
申请人： Terrence G. Vargo , Jeffrey M. Calvert , Joseph A. Gardella, Jr. , Mu-San Chen
发明人： Terrence G. Vargo , Jeffrey M. Calvert , Joseph A. Gardella, Jr. , Mu-San Chen
IPC分类号： C08F8/42 , C23C18/16 , H05K3/38
CPC分类号： B82Y30/00 , C08F8/42 , C23C18/1605 , C23C18/2086 , C23C18/30 , H05K3/381 , H05K3/389
摘要： Fluoropolymeric substrates with metallized surfaces may be prepared by self-assembly of a chemisorbed layer of a metal ion-chelating organosilane onto a fluoropolymer surface after radio-frequency glow discharge plasma surface hydroxylation. The silane covalently binds an aqueous palladium catalyst and subsequent electroless deposition yields homogeneous or patterned metal deposits that exhibit excellent adhesion to the fluoropolymer.
摘要翻译：具有金属化表面的含氟聚合物基材可以通过在射频辉光放电等离子体表面羟基化之后将金属离子螯合有机硅烷的化学吸附层自组装到含氟聚合物表面上来制备。硅烷共价结合钯催化剂水溶液，随后的无电沉积产生均匀或图案化的金属沉积物，其对含氟聚合物表现出优异的附着力。

3. 发明授权

US5696207A Fluroropolymeric substrates with metallized surfaces and methods for producing the same 失效
标题翻译：具有金属化表面的含氟聚合物基材及其制备方法
公开(公告)号：US5696207A
公开(公告)日：1997-12-09
申请号：US697933
申请日：1996-09-03
申请人： Terrence G. Vargo , Jeffrey M. Calvert , Joseph A. Gardella, Jr. , Mu-San Chen
发明人： Terrence G. Vargo , Jeffrey M. Calvert , Joseph A. Gardella, Jr. , Mu-San Chen
IPC分类号： C08F8/42 , C23C18/16 , H05K3/38
CPC分类号： B82Y30/00 , C08F8/42 , C23C18/1605 , C23C18/2086 , C23C18/30 , H05K3/381 , H05K3/389
摘要： Fluoropolymeric substrates with metallized surfaces may be prepared by self-assembly of a chemisorbed layer of a metal ion-chelating organosilane onto a fluoropolymer surface after radio-frequency glow discharge plasma surface hydroxylation. The silane covalently binds an aqueous palladium catalyst and subsequent electroless deposition yields homogeneous or patterned metal deposits that exhibit excellent adhesion to the fluoropolymer.
摘要翻译：具有金属化表面的含氟聚合物基材可以通过在射频辉光放电等离子体表面羟基化之后将金属离子螯合有机硅烷的化学吸附层自组装到含氟聚合物表面上来制备。硅烷共价结合钯催化剂水溶液，随后的无电沉积产生均匀或图案化的金属沉积物，其对含氟聚合物表现出优异的附着力。

4. 发明授权

US5828432A Conducting substrate, liquid crystal device made therefrom and liquid crystalline composition in contact therewith 失效
标题翻译：导电基板，由其制成的液晶装置和与其接触的液晶组合物
公开(公告)号：US5828432A
公开(公告)日：1998-10-27
申请号：US882297
申请日：1997-06-25
申请人： Ranganathan Shashidhar , Jeffrey M. Calvert , Renate J. Crawford , Kenneth J. Wynne , Terrence G. Vargo , Alan G. MacDiarmid , Jamshid K. Avlyanov
发明人： Ranganathan Shashidhar , Jeffrey M. Calvert , Renate J. Crawford , Kenneth J. Wynne , Terrence G. Vargo , Alan G. MacDiarmid , Jamshid K. Avlyanov
IPC分类号： G02F1/1333 , G02F1/1343
CPC分类号： G02F1/13439 , G02F1/133305
摘要： Conducting substrate for use in display device having a conducting polymer on the surface of a rigid or flexible, flat, curved or bent substrate.
摘要翻译：用于具有导电聚合物的显示装置的导电基底，其在刚性或柔性，平坦，弯曲或弯曲的基底的表面上。

5. 发明授权

US06548590B1 Polymer and inorganic-organic hybrid composites and methods for making and using same 失效
标题翻译：聚合物和无机 - 有机杂化复合材料及其制备和使用方法
公开(公告)号：US06548590B1
公开(公告)日：2003-04-15
申请号：US09532993
申请日：2000-03-22
申请人： Timothy S. Koloski , Terrence G. Vargo
发明人： Timothy S. Koloski , Terrence G. Vargo
IPC分类号： C08K334
CPC分类号： C08K9/08
摘要： Composites which include a polymer matrix having natural free volume therein and an inorganic or organic material disposed in the natural free volume of the polymer matrix are disclosed. In addition, methods for making a composite are described. A polymer matrix having free volume therein is provided. The free volume is evacuated, and inorganic or organic molecules are infused into the evacuated free volume of the polymer matrix. The inorganic or organic molecules can then be polymerized under conditions effective to cause the polymerized inorganic or organic molecules to assemble into macromolecular networks. Alternatively, where the polymer matrix contains a functionality, the inorganic or organic molecules can be treated under conditions effective to cause the inorganic or organic molecules to interact with the polymer matrix's functionality. Use of the disclosed composites as photoradiation shields and filters, electromagnetic radiation shields and filters, antistatic layers, heterogeneous catalysts, conducting electrodes, materials having flame and heat retardant properties; components in the construction of electrolytic cells, fuel cells, and optoelectronic devices, is also described.
摘要翻译：公开了包括其中具有天然自由体积的聚合物基质和设置在聚合物基质的天然自由体积中的无机或有机材料的复合材料。此外，描述了制备复合材料的方法。提供其中具有自由体积的聚合物基质。抽空自由体积，将无机或有机分子注入聚合物基体的抽真空体积中。然后无机或有机分子可以在有效地使聚合的无机或有机分子组装成大分子网络的条件下聚合。或者，当聚合物基质含有官能团时，可以在有效使无机或有机分子与聚合物基质的官能团相互作用的条件下处理无机或有机分子。使用所公开的复合材料作为光辐射屏蔽和滤光器，电磁辐射屏蔽和滤光器，抗静电层，非均相催化剂，导电电极，具有火焰和阻热特性的材料; 还描述了电解池，燃料电池和光电子器件的构造中的组件。

6. 发明授权

US5977241A Polymer and inorganic-organic hybrid composites and methods for making same 失效
标题翻译：聚合物和无机 - 有机杂化复合材料及其制备方法
公开(公告)号：US5977241A
公开(公告)日：1999-11-02
申请号：US833290
申请日：1997-04-04
申请人： Timothy S. Koloski , Terrence G. Vargo
发明人： Timothy S. Koloski , Terrence G. Vargo
IPC分类号： C08F283/00 , C09D5/16 , H01M2/16 , H01M4/66 , H01M8/10 , C08L27/12 , C08J7/06
CPC分类号： H01M4/667 , C08F283/00 , C09D5/1612 , H01M8/1004 , H01M2/164 , Y10S525/903 , Y10T428/24999 , Y10T428/249991
摘要： Composites which include a polymer matrix having natural free volume therein and an inorganic or organic material disposed in the natural free volume of the polymer matrix are disclosed. In addition, methods for making a composite are described. A polymer matrix having free volume therein is provided. The free volume is evacuated, and inorganic or organic molecules are infused into the evacuated free volume of the polymer matrix. The inorganic or organic molecules can then be polymerized under conditions effective to cause the polymerized inorganic or organic molecules to assemble into macromolecular networks. Alternatively, where the polymer matrix contains a functionality, the inorganic or organic molecules can be treated underconditions effective to cause the inorganic or organic molecules to interact with the polymer matrix's functionality. Use of the disclosed composites as photoradiation shields and filters, electromagnetic radiation shields and filters, antistatic layers, heterogeneous catalytic substrates, conducting electrodes, materials having flame and heat retardant properties, and components in the construction of electrolytic cells, fuel cells, and optoelectronic devices is also described.
摘要翻译：公开了包括其中具有天然自由体积的聚合物基质和设置在聚合物基质的天然自由体积中的无机或有机材料的复合材料。此外，描述了制备复合材料的方法。提供其中具有自由体积的聚合物基质。抽空自由体积，将无机或有机分子注入聚合物基体的抽真空体积中。然后无机或有机分子可以在有效地使聚合的无机或有机分子组装成大分子网络的条件下聚合。或者，当聚合物基质含有官能团时，无机或有机分子可以在有效地使无机或有机分子与聚合物基质的官能团相互作用的条件下进行处理。使用所公开的复合材料作为光辐射屏蔽和滤光器，电磁辐射屏蔽和滤光器，抗静电层，非均相催化基板，导电电极，具有火焰和阻热性质的材料，以及在电解池，燃料电池和光电子器件的构造中的组件也被描述。

7. 发明授权

US06608129B1 Polymer composites and methods for making and using same 失效
标题翻译：聚合物复合材料及其制造和使用方法
公开(公告)号：US06608129B1
公开(公告)日：2003-08-19
申请号：US09533894
申请日：2000-03-22
申请人： Timothy S. Koloski , Terrence G. Vargo
发明人： Timothy S. Koloski , Terrence G. Vargo
IPC分类号： C08K318
CPC分类号： H01M4/667 , C08F283/00 , C09D5/1612 , H01M2/164 , H01M8/1004
摘要： Composites which include a polymer matrix having natural free volume therein and an inorganic or organic material disposed in the natural free volume of the polymer matrix are disclosed. In addition, methods for making a composite are described. A polymer matrix having free volume therein is provided. The free volume is evacuated, and inorganic or organic molecules are infused into the evacuated free volume of the polymer matrix. The inorganic or organic molecules can then be polymerized under conditions effective to cause the polymerized inorganic or organic molecules to assemble into macromolecular networks. Alternatively, where the polymer matrix contains a functionality, the inorganic or organic molecules can be treated under conditions effective to cause the inorganic or organic molecules to interact with the polymer matrix's functionality. Use of the disclosed composites as photoradiation shields and filters, electromagnetic radiation shields and filters, antistatic layers, heterogeneous catalysts, conducting electrodes, materials having flame and heat retardant properties, components in the construction of electrolytic cells, fuel cells, and optoelectronic devices, and antifouling coatings is also described.
摘要翻译：公开了包括其中具有天然自由体积的聚合物基质和设置在聚合物基质的天然自由体积中的无机或有机材料的复合材料。此外，描述了制备复合材料的方法。提供其中具有自由体积的聚合物基质。抽空自由体积，将无机或有机分子注入聚合物基体的抽真空体积中。然后无机或有机分子可以在有效地使聚合的无机或有机分子组装成大分子网络的条件下聚合。或者，当聚合物基质含有官能团时，可以在有效使无机或有机分子与聚合物基质的官能团相互作用的条件下处理无机或有机分子。使用所公开的复合材料作为光辐射屏蔽和滤光器，电磁辐射屏蔽和滤光器，抗静电层，非均相催化剂，导电电极，具有火焰和阻热性能的材料，电解池结构中的组件，燃料电池和光电器件，以及还描述了防污涂料。

8. 发明授权

US5703173A Transition metallohalopolymers 失效
标题翻译：过渡金属卤素聚合物
公开(公告)号：US5703173A
公开(公告)日：1997-12-30
申请号：US689707
申请日：1996-08-16
申请人： Timothy S. Koloski , Terrence G. Vargo
发明人： Timothy S. Koloski , Terrence G. Vargo
IPC分类号： A01N55/02 , C08F8/00 , C08F8/42 , C08F14/16 , C08F81/42
CPC分类号： C08F8/42 , A01N55/02
摘要： Novel metallohalopolymers comprising an oxyhalopolymer and a transition metal covalently bonded to an oxygen site on the oxyhalopolymer possess desirable properties of inertness, stability, hydrophobicity and high electronegativity like fluoropolymers such as PTFE. The metallohalopolymers also possess unusual superacidic properties making oxygen-containing sites on the polymeric backbone highly nucleophilic and reactive with transition metals for synthesis of stable metallized polymers without requiring exposure to destructive calcining temperatures or intermediate chelating organosilane linking agents. The transition metals can be covalently bonded directly to the polymeric support to form metallohalopolymers for use as catalysts in the synthesis of chemicals, biocides and useful articles of manufacture, such as filtration devices containing the biocidally active metallohalopolymers.
摘要翻译：包含羟基卤聚合物和共价键合到氧基聚合物上的氧位的过渡金属的新型金属卤共聚物具有惰性，稳定性，疏水性和诸如PTFE等含氟聚合物的高电负性的所需性质。金属卤化物还具有不寻常的超酸性质，使聚合物骨架上的含氧位置高度亲核，并与过渡金属反应，用于合成稳定的金属化聚合物，而不需要暴露于破坏性煅烧温度或中间螯合有机硅烷连接剂。过渡金属可以直接共价结合到聚合物载体上以形成用作合成化学品，杀生物剂和有用制品的催化剂的金属卤聚合物，例如含有生物活性金属卤代聚合物的过滤装置。

9. 发明授权

US07217754B2 Polymer composites and methods for making and using same 失效
标题翻译：聚合物复合材料及其制造和使用方法
公开(公告)号：US07217754B2
公开(公告)日：2007-05-15
申请号：US10412616
申请日：2003-04-12
申请人： Timothy S. Koloski , Terrence G. Vargo
发明人： Timothy S. Koloski , Terrence G. Vargo
IPC分类号： C08K3/22
CPC分类号： H01M4/667 , C08F283/00 , C08K9/08 , C09D5/1612 , H01M2/164 , H01M8/1004
摘要： Composites which include a polymer matrix having natural free volume therein and an inorganic or organic material disposed in the natural free volume of the polymer matrix are disclosed. In addition, methods for making a composite are described. A polymer matrix having free volume therein is provided. The free volume is evacuated, and inorganic or organic molecules are infused into the evacuated free volume of the polymer matrix. The inorganic or organic molecules can then be polymerized under conditions effective to cause the polymerized inorganic or organic molecules to assemble into nanoparticles or other types of macromolecular networks. Alternatively, where the polymer matrix contains a functionality, the inorganic or organic molecules can be treated under conditions effective to cause the inorganic or organic molecules to interact with the polymer matrix's functionality. Use of the disclosed composites as photoradiation shields and filters, electromagnetic radiation shields and filters, antistatic layers, heterogeneous catalysts, conducting electrodes, materials having flame and heat retardant properties, components in the construction of electrolytic cells, fuel cells, and optoelectronic devices, and antifouling coatings is also described.
摘要翻译：公开了包括其中具有天然自由体积的聚合物基质和设置在聚合物基质的天然自由体积中的无机或有机材料的复合材料。此外，描述了制备复合材料的方法。提供其中具有自由体积的聚合物基质。抽空自由体积，将无机或有机分子注入聚合物基体的抽真空体积中。然后无机或有机分子可在有效地使聚合的无机或有机分子组装成纳米颗粒或其它类型的大分子网络的条件下聚合。或者，当聚合物基质含有官能团时，可以在有效使无机或有机分子与聚合物基质的官能团相互作用的条件下处理无机或有机分子。使用所公开的复合材料作为光辐射屏蔽和滤光器，电磁辐射屏蔽和滤光器，抗静电层，非均相催化剂，导电电极，具有火焰和阻热性能的材料，电解池结构中的组件，燃料电池和光电器件，以及还描述了防污涂料。

10. 发明授权

US06428887B1 Adhesive oxyhalopolymer composites 有权
标题翻译：粘合剂含氧卤聚合物复合材料
公开(公告)号：US06428887B1
公开(公告)日：2002-08-06
申请号：US09239108
申请日：1999-01-27
申请人： Terrence G. Vargo , Douglas J. Naab , Timothy S. Koloski
发明人： Terrence G. Vargo , Douglas J. Naab , Timothy S. Koloski
IPC分类号： B32B1508
CPC分类号： B32B7/12 , C09J7/245 , C09J2427/006 , Y10T156/1097 , Y10T428/28 , Y10T428/31522 , Y10T428/3154
摘要： There is disclosed adhesive-oxyhalopolymer composites having surface hydrogen and oxygen or oxygen functionality groups wherein the oxygen or oxygen functionality sites are chemically bonded to an adhesive material forming a stable and permanent bond with surprisingly and unexpected superior bond strength. The adhesive-oxyhalopolymer composites comprise an oxyhalopolymer prepared from a halopolymer having from about 1 to 100 percent of surface halogens permanently substituted with hydrogen and oxygen or oxygen-containing groups of which from about 3 to about 30 percent of the substituted halogens are replaced with oxygen or oxygen-containing groups and from about 70 to about 97 percent of the substituted halogens are replaced with hydrogen atoms and the oxyhalopolymer is chemically bonded to an adhesive material.
摘要翻译：公开了具有表面氢和氧或氧官能团基团的粘合剂 - 氧基聚合物复合材料，其中氧或氧官能度位点化学键合到形成稳定且永久的粘合剂的粘合剂材料，具有令人惊奇和意想不到的优异的粘结强度。粘合剂 - 氧基聚合物复合材料包含由卤代聚合物制备的氧卤聚合物，所述卤代聚合物具有约1至100％的永久地被氢取代的表面卤素，并且氧或含氧基团，其中约3至约30％的取代的卤素被氧代替或含氧基团，并且约70至约97％的取代的卤素被氢原子替代，并且氧基聚合物与粘合剂材料化学键合。

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