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1. 发明申请

WO2012115795A3 IMPROVED FRIT MATERIALS AND/OR METHOD OF MAKING VACUUM INSULATING GLASS UNITS INCLUDING THE SAME 审中-公开
公开(公告)号：WO2012115795A3
公开(公告)日：2012-08-30
申请号：PCT/US2012/024598
申请日：2012-02-10
申请人： GUARDIAN INDUSTRIES CORP. , DENNIS, Timothy, A.
发明人： DENNIS, Timothy, A.
IPC分类号： C03C8/24 , C03C27/06 , C03C8/04
摘要： Certain example embodiments relate to frit materials containing Bi2O3, ZnO, B2O3, AI2O3 and MgO that have an improved IR absorption property. Certain examples relate to frit materials that substantially melt in about 3 minutes at a temperature of about 525°C. Certain examples relate to a method of making an edge seal by using IR energy. Certain examples relate to adjusting the IR energy applied to a frit material to form an edge seal. Certain examples also relate to making a VIG unit by applying IR energy and adjusting the amount of IR energy over multiple periods of time, e.g., in an oscillating manner.

2. 发明申请

WO2013173172A1 METHOD AND APPARATUS FOR MAKING VACUUM INSULATED GLASS (VIG) WINDOW UNIT INCLUDING PUMP-OUT TUBE 审中-公开
标题翻译：用于制造真空绝缘玻璃（VIG）窗口单元的方法和装置，包括泵出管
公开(公告)号：WO2013173172A1
公开(公告)日：2013-11-21
申请号：PCT/US2013/040463
申请日：2013-05-10
申请人： GUARDIAN INDUSTRIES CORP.
发明人： DENNIS, Timothy, A. , PANTKE, Andrew, W.
IPC分类号： E06B3/66 , E06B3/677
CPC分类号： E06B3/6775 , E06B3/6612 , Y02A30/25 , Y02B80/24 , Y10T29/49826 , Y10T428/24273
摘要： A vacuum insulated glass (VIG) window assembly and method for making same is provided in which dimensions of a hole formed in a glass substrate in which a pump-out tube is to be inserted is selected such that it provides sufficient clearance for efficient insertion and accommodates sufficient adhesive material (e.g., frit inclusive paste), while at the same time providing sufficient support to resist substantial tilting or tipping of the pump-out tube when inserted in the hole. In addition, a length of the pump-out tube is selected so that a distance between a top of the pump-out tube (which is later subjected to heat sealing, e.g., by a laser or the like) and an interface between the pump-out tube and the frit material proximate the hole exiting the glass substrate is in a range that reduces the likelihood of heat conduction sufficient to cause cracking of the pump-out tube at the pump-out tube/frit interface caused, for example, by thermal shock due to a temperature differential between the glass of the pump-out tube and the frit material.
摘要翻译：提供一种真空绝缘玻璃（VIG）窗组件及其制造方法，其中形成在其中要插入抽出管的玻璃基板中的孔的尺寸被选择为使得其提供足够的间隙以有效地插入，容纳足够的粘合剂材料（例如，含玻璃料的糊状物），同时提供足够的支撑以防止当插入孔中时抽出管的显着倾斜或倾翻。另外，抽出管的长度被选择为使得排出管的顶部（其稍后经过热密封，例如通过激光等）和泵之间的界面之间的距离离开玻璃基板的孔附近的玻璃料材料处于一个范围内，这样可以降低热传导的可能性，足以引起排出管/玻璃料界面处的抽出管的破裂，例如由由于抽出管的玻璃与玻璃料之间的温度差导致的热冲击。

3. 发明申请

WO2013165827A1 METHOD AND APPARATUS FOR MAKING VACUUM INSULATED GLASS (VIG) WINDOW UNIT INCLUDING CLEANING CAVITY THEREOF 审中-公开
标题翻译：用于制造真空绝缘玻璃（VIG）窗户的方法和装置，其中包括其清洁空气
公开(公告)号：WO2013165827A1
公开(公告)日：2013-11-07
申请号：PCT/US2013/038333
申请日：2013-04-26
申请人： GUARDIAN INDUSTRIES CORP.
发明人： DENNIS, Timothy, A. , PANTKE, Andrew, W. , JONES, Jeffrey, A.
IPC分类号： E06B3/66 , E06B3/677 , C03C23/00 , E06B3/663
CPC分类号： C03C23/0075 , E06B3/6612 , E06B3/66304 , E06B3/6775 , Y02A30/25 , Y02B80/24
摘要： A method and apparatus for cleaning a cavity of a vacuum insulated glass window assembly is provided in which a cleaning gas mixture of or including ozone is introduced into the cavity of the vacuum insulated glass assembly and allowed to react with residual materials, such as, for example, hydrocarbons and/or polymers. Reacted hydrocarbons and/or polymers are then removed from the vacuum cavity along with any residual cleaning gas mixture. The cleaning method is preferably performed at substantially ambient temperatures or at least temperatures below about 250°C. The ozone cleaning cycle may be repeated multiple times and followed by additional purges with other gases, such as for example nitrogen. Additional energy may be provided by heating, RF plasma; corona discharge, UV lamp, and/or the like.
摘要翻译：提供一种用于清洁真空绝热玻璃窗组件的空腔的方法和装置，其中将包括臭氧的或包括臭氧的清洁气体混合物引入真空绝热玻璃组件的空腔中，并使其与残留材料反应，例如例如烃和/或聚合物。然后将所得的烃和/或聚合物与任何残留的清洁气体混合物一起从真空腔中除去。清洁方法优选在基本环境温度或低于约250℃的至少温度下进行。臭氧清洁循环可以重复多次，随后用其它气体，例如氮气进行附加清洗。可通过加热，RF等离子体提供额外的能量; 电晕放电，UV灯等。

4. 发明申请

WO2013101748A1 VANADIUM-BASED FRIT MATERIALS, SEALING MATERIAL AND METHODS OF MAKING THE SAME AND USING THE SAME FOR SEALING VACUUM INSULATING GLASS 审中-公开
标题翻译：基于VANADIUM的自由材料，密封材料及其制造方法和使用它们来密封真空绝缘玻璃
公开(公告)号：WO2013101748A1
公开(公告)日：2013-07-04
申请号：PCT/US2012/071324
申请日：2012-12-21
申请人： GUARDIAN INDUSTRIES CORP.
发明人： DENNIS, Timothy, A.
IPC分类号： C03C3/12 , C03C8/04 , C03C8/24 , E06B3/66 , C03C3/062
CPC分类号： E06B3/6775 , C03B23/24 , C03C3/062 , C03C3/122 , C03C8/04 , C03C8/06 , C03C8/24 , C03C27/06 , C03C2207/00 , E06B3/6612 , E06B3/673 , E06B3/67334 , Y02A30/25 , Y02B80/24
摘要： Certain example embodiments relate to seals for glass articles. Certain example embodiments relate to a composition used for sealing an insulted glass unit. In certain example embodiments the composition includes vanadium oxide, barium oxide, zinc oxide, and at least one additional additive. For instance, another additive that is a different metal oxide or different metal chloride may be provided. In certain example embodiments, a composition may be combined with a binder solution that substantially or completely burns out by the time the composition is melted. In certain example embodiments, a vacuum insulated glass unit includes first and second glass substrates that are sealed together with a seal that includes the above-described composition.
摘要翻译：某些示例实施例涉及玻璃制品的密封件。某些示例性实施方案涉及用于密封被侮辱玻璃单元的组合物。在某些示例性实施方案中，组合物包括氧化钒，氧化钡，氧化锌和至少一种另外的添加剂。例如，可以提供作为不同金属氧化物或不同金属氯化物的另外的添加剂。在某些示例性实施方案中，组合物可以与在组合物熔融时基本上或完全烧尽的粘合剂溶液组合。在某些示例性实施例中，真空绝热玻璃单元包括与包括上述组成的密封件密封在一起的第一和第二玻璃基板。

5. 发明申请

WO2013043340A1 VANADIUM -BASED FRIT MATERIALS AND METHODS OF MAKING THE SAME 审中-公开
标题翻译： VANADIUM -BASED FRIT材料及其制备方法
公开(公告)号：WO2013043340A1
公开(公告)日：2013-03-28
申请号：PCT/US2012/053010
申请日：2012-08-30
申请人： GUARDIAN INDUSTRIES CORP. , DENNIS, Timothy, A.
发明人： DENNIS, Timothy, A.
IPC分类号： C03C8/04 , C03C8/24
CPC分类号： E06B3/6612 , C03C8/04 , C03C8/24 , E06B3/663 , E06B3/66342 , E06B3/66357 , E06B3/667 , E06B3/677
摘要： Certain example embodiments relate to improved seals for glass articles. Certain example embodiments relate to a composition used for sealing an insulted glass unit. In certain example embodiments the composition includes in mol % 45-50 vanadium oxide, 20-23 barium oxide, 9-12 zinc oxide, and at least four additional additives. For instance, another additive that is a different metal oxide or different metal chloride may be provided. In certain example embodiments, a vacuum insulated glass unit includes first and second glass substrates that are sealed together with a seal that includes the above-described composition.
摘要翻译：某些示例实施例涉及用于玻璃制品的改进的密封件。某些示例性实施方案涉及用于密封被侮辱玻璃单元的组合物。在某些示例性实施方案中，组合物包括摩尔％45-50氧化钒，20-23氧化钡，9-12氧化锌和至少四种另外的添加剂。例如，可以提供作为不同金属氧化物或不同金属氯化物的另外的添加剂。在某些示例性实施例中，真空绝热玻璃单元包括与包括上述组成的密封件密封在一起的第一和第二玻璃基板。

6. 发明申请

WO2012115796A1 VANADIUM -BASED FRIT MATERIALS AND METHODS OF MAKING THE SAME 审中-公开
标题翻译： VANADIUM -BASED FRIT材料及其制备方法
公开(公告)号：WO2012115796A1
公开(公告)日：2012-08-30
申请号：PCT/US2012/024604
申请日：2012-02-10
申请人： GUARDIAN INDUSTRIES CORP. , DENNIS, Timothy, A.
发明人： DENNIS, Timothy, A.
IPC分类号： C03C8/04 , C03C8/24
CPC分类号： C03C8/06 , C03C8/04 , C03C8/24 , C03C27/06 , C03C2205/00 , E06B3/6612 , E06B3/673
摘要： Certain example embodiments relate to improved seals for glass articles. Certain example embodiments relate to a composition used for sealing an insulted glass unit. In certain example embodiments the composition includes vanadium oxide, barium oxide, zinc oxide, and at least one additional additive in particular the fit material comprises in weight%: V2O5, 50-60, BaO, 27-33, ZnO 9-12 and one additive selected from: Ta2O5, Ti2O3, SrCl2, GeO2,CuO, AgO, Nb2O5, MgO, B2O3, SiO2, TI2O3, Υ2O3, SnF2, SnO2, CuCI, SnCl2, CeO2, AgCI, Ιn2O3, SnO, SrO and AI2O3. For instance, another additive that is a different metal oxide or different metal chloride may be provided. In certain example embodiments, a vacuum insulated glass unit includes first and second glass substrates that are sealed together with a seal that includes the above-described composition.
摘要翻译：某些示例实施例涉及用于玻璃制品的改进的密封件。某些示例性实施方案涉及用于密封被侮辱玻璃单元的组合物。在某些示例性实施方案中，组合物包括氧化钒，氧化钡，氧化锌和至少一种另外的添加剂，特别地，配合材料包含重量％：V 2 O 5，50-60，BaO，27-33，ZnO 9-12和一种添加剂选自：Ta2O5，Ti2O3，SrCl2，GeO2，CuO，AgO，Nb2O5，MgO，B2O3，SiO2，TI2O3，α2O3，SnF2，SnO2，CuCl，SnCl2，CeO2，AgCl，ηn2O3，SnO，SrO和Al2O3。例如，可以提供作为不同金属氧化物或不同金属氯化物的另外的添加剂。在某些示例性实施例中，真空绝热玻璃单元包括与包括上述组成的密封件密封在一起的第一和第二玻璃基板。

7. 发明申请

WO2015119952A1 FRITS FOR USE IN VACUUM INSULATING GLASS (VIG) UNITS, AND/OR ASSOCIATED METHODS 审中-公开
标题翻译：用于真空绝缘玻璃（VIG）单元，和/或相关方法
公开(公告)号：WO2015119952A1
公开(公告)日：2015-08-13
申请号：PCT/US2015/014269
申请日：2015-02-03
申请人： GUARDIAN INDUSTRIES CORP.
发明人： HOGAN, John, P. , DENNIS, Timothy, A. , PETRMICHL, Rudolph, H. , KEMENAH, Greg
IPC分类号： C03C3/062 , C03C3/066 , C03C3/12 , C03C8/02 , C03C8/04 , C03C8/14 , C03C8/22 , C03C8/24 , C03B27/04 , C03C3/14
CPC分类号： C03C8/24 , C03C3/062 , C03C3/066 , C03C3/122 , C03C3/14 , C03C8/02 , C03C8/04 , C03C8/14 , C03C8/22 , E06B3/6612 , E06B3/6775
摘要： Certain example embodiments of this invention relate to vacuum insulating glass (VIG) units having improved seals made using two different frit-based edge seal materials, and/or methods of making the same. In certain example embodiments, a first frit material is applied around peripheral edges of first and second glass substrates. The first frit material, which may be bismuth-based in certain example embodiments, is fired with a heat treatment (e.g., thermal tempering) process. A second frit material, which may be VBZ-based in certain example embodiments, is applied and at least partially overlaps with the fired first frit material. The first frit material acts as a primer, and the second frit material helps seal together the VIG unit. The second frit material is fired at a significantly lower temperature that enables the glass to retain the temper or other strength imparted by the heat treatment.
摘要翻译：本发明的某些示例性实施例涉及具有使用两种不同的玻璃料型边缘密封材料制成的改进的密封的真空中空玻璃（VIG）单元和/或制造该绝缘玻璃的方法。在某些示例性实施例中，将第一玻璃料材料施加在第一和第二玻璃基板的周边边缘附近。在某些示例性实施方案中可以以铋为基础的第一玻璃料材料通过热处理（例如，热回火）工艺进行烧制。在某些示例性实施方案中可以是基于VBZ的第二玻璃料材料被施加并且与被烧制的第一玻璃料材料至少部分重叠。第一玻璃料用作底漆，第二玻璃料有助于将VIG单元密封在一起。第二玻璃料材料在明显较低的温度下烧制，使得玻璃能够保持回火或通过热处理赋予的其它强度。

8. 发明申请

WO2013180998A1 VACUUM INSULATED GLASS (VIG) WINDOW UNIT WITH REDUCED SEAL HEIGHT VARIATION AND METHOD FOR MAKING SAME 审中-公开
标题翻译：具有减小密封高度变化的真空绝缘玻璃（VIG）窗单元及其制造方法
公开(公告)号：WO2013180998A1
公开(公告)日：2013-12-05
申请号：PCT/US2013/041747
申请日：2013-05-20
申请人： GUARDIAN INDUSTRIES CORP.
发明人： DENNIS, Timothy, A. , PANTKE, Andrew, W.
IPC分类号： E06B3/66 , E06B3/677
CPC分类号： E06B3/66333 , B32B3/085 , B32B7/12 , B32B17/06 , B32B2250/02 , B32B2255/20 , B32B2307/304 , B32B2307/412 , B32B2419/00 , E06B3/6612 , E06B3/663 , E06B3/677 , E06B3/6775 , Y02A30/25 , Y02B80/24
摘要： A vacuum insulated glass (VIG) window assembly and method for making same is provided in which a variation in the final edge seal height is preferably 0.20 mm or less, more preferably about 0.15 mm or less. Controlling final edge seal height variations substantially reduces breakage of the glass substrates of the VIG window assembly during vacuum pump-down of the cavity between the glass substrates. Edge seal height variation may be controlled, for example, by controlling initial dispensing of green frit material, controlling temperature variations during firing, and/or controlling cycle times during firing.
摘要翻译：提供真空绝缘玻璃（VIG）窗组件及其制造方法，其中最终边缘密封高度的变化优选为0.20mm以下，更优选为约0.15mm以下。控制最终边缘密封高度变化在玻璃基板之间的空腔真空抽吸期间大大减少了VIG窗组件的玻璃基板的断裂。可以例如通过控制绿色玻璃料的初始分配，控制烧制期间的温度变化和/或控制烧制期间的循环时间来控制边缘密封高度变化。

9. 发明申请

WO2013173175A1 METHOD AND APPARATUS FOR MAKING VACUUM INSULATED GALSS (VIG) WINDOW UNIT INCLUDING PUMP-OUT TUBE SEALING TECHNIQUE 审中-公开
标题翻译：用于制造真空绝缘盖（VIG）窗口单元的方法和装置，包括泵出口密封技术
公开(公告)号：WO2013173175A1
公开(公告)日：2013-11-21
申请号：PCT/US2013/040466
申请日：2013-05-10
申请人： GUARDIAN INDUSTRIES CORP.
发明人： DENNIS, Timothy, A. , PANTKE, Andrew, W.
IPC分类号： E06B3/66
CPC分类号： E06B3/6612 , E06B3/6775 , Y02A30/25 , Y02B80/24
摘要： A method for making a vacuum insulated glass window assembly is provided in which an exposed end of a pump-out tube of a vacuum insulated glass window assembly is sealed using a laser that is applied to the end of the pump out tube in controlled sequential manner as opposed to a short duration, high-powered application of a laser. In particular, a method is disclosed in which a multiphase sequential variable power application of laser energy to an exposed end of a pump-out tube for controlled exposure times and decreasing laser trace diameters produces a more controlled melting of the tube glass to reduce or eliminate undesirable outgassing that may occur during a high-power short duration exposure of laser energy to the end of the pump-out tube to seal the tube.
摘要翻译：提供一种制造真空绝缘玻璃窗组件的方法，其中使用以受控顺序方式施加到泵出管端的激光器密封真空绝热玻璃窗组件的抽出管的露出端与激光器的大功率应用相反，短时间内。特别地，公开了一种方法，其中将激光能量施加到泵出管的暴露端以控制曝光时间并减小激光迹线直径的多相顺序可变功率可以产生更受控制的管玻璃熔化以减少或消除在大功率短时间内将激光能量暴露于泵出管的端部以密封管道期间可能发生的不希望的除气。

10. 发明申请

WO2015119914A1 VACUUM INSULATING GLASS (VIG) UNIT WITH LEAD-FREE DUAL-FRIT EDGE SEALS AND/OR METHODS OF MAKING THE SAME 审中-公开
标题翻译：具有无铅双边缘密封件的真空绝缘玻璃（VIG）单元和/或其制造方法
公开(公告)号：WO2015119914A1
公开(公告)日：2015-08-13
申请号：PCT/US2015/014187
申请日：2015-02-03
申请人： GUARDIAN INDUSTRIES CORP.
发明人： HOGAN, John, P. , DENNIS, Timothy, A. , PETRMICHL, Rudolph, H. , KEMENAH, Greg
IPC分类号： C03C3/062 , C03C3/066 , C03C3/12 , C03C3/14 , C03C3/145 , C03C8/02 , C03C8/04 , C03C8/14 , C03C8/22 , C03C8/24 , C03C27/06 , C03B27/04 , E06B3/66 , E06B3/677
CPC分类号： E06B3/66357 , C03B23/203 , C03B27/012 , C03C3/062 , C03C3/066 , C03C3/122 , C03C3/14 , C03C3/145 , C03C8/02 , C03C8/04 , C03C8/14 , C03C8/22 , C03C8/24 , C03C27/06 , E06B3/6612 , E06B3/67334 , E06B3/6736 , E06B3/6775 , Y02A30/25 , Y02B80/24
摘要： Certain example embodiments of this invention relate to vacuum insulating glass (VIG) units having improved seals made using two different frit-based edge seal materials, and/or methods of making the same. In certain example embodiments, a first frit material is applied around peripheral edges of first and second glass substrates. The first frit material, which may be bismuth- based in certain example embodiments, is fired with a heat treatment (e.g., thermal tempering) process. A second frit material, which may be VBZ-based in certain example embodiments, is applied and at least partially overlaps with the fired first frit material. The first frit material acts as a primer, and the second frit material helps seal together the VIG unit. The second frit material is fired at a significantly lower temperature that enables the glass to retain the temper or other strength imparted by the heat treatment.
摘要翻译：本发明的某些示例性实施例涉及具有使用两种不同的玻璃料边缘密封材料制成的改进的密封的真空中空玻璃（VIG）单元和/或制造该绝缘玻璃的方法。在某些示例性实施例中，将第一玻璃料材料施加在第一和第二玻璃基板的周边边缘附近。在某些示例性实施例中可以以铋为基础的第一玻璃料材料通过热处理（例如热回火）工艺进行烧制。在某些示例性实施方案中可以是基于VBZ的第二玻璃料材料被施加并且与被烧制的第一玻璃料材料至少部分重叠。第一玻璃料用作底漆，第二玻璃料有助于将VIG单元密封在一起。第二玻璃料材料在明显较低的温度下烧制，使得玻璃能够保持回火或通过热处理赋予的其它强度。

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