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1. 发明授权

US5244989A Method for producing a stereospecific polyolefin 失效
公开(公告)号：US5244989A
公开(公告)日：1993-09-14
申请号：US841508
申请日：1992-02-26
申请人： Daiji Hara , Morihiko Sato , Mitsuhiro Mori , Yozo Kondo
发明人： Daiji Hara , Morihiko Sato , Mitsuhiro Mori , Yozo Kondo
IPC分类号： C08F4/658 , C08F4/60 , C08F10/00
CPC分类号： C08F10/00
摘要： A method for producing a stereospecific polyolefin in the presence of a catalyst comprising a transition metal compound and an organometallic compound, wherein a catalyst system is used which comprises: (A) a solid catalyst component prepared by reacting (i) a homogeneous solution prepared by reacting (i-1) magnesium and a hydroxylated organic compound, (i-2) an oxygen-containing organic compound of titanium and/or (i-3) an oxygen-containing organic compound of silicon, with an oxygen-containing organic compound of aluminum and/or a boron compound, with (ii) at least one aluminum halide compound to obtain a solid product, reacting to this solid product (iii) an electron-donative compound and (iv) a titanium halide compound to obtain a solid component, and further reacting to this solid component (v) silicon tetrachloride and/or an alkyl-substituted product of silicon tetrachloride, (B) at least one member selected from the group consisting of organometallic compounds of Groups IA, IIA, IIB, IIIB and IVB of the Periodic Table, and (C) an electron-donative compound.

2. 发明授权

US5489634A Method for producing a stereospecific polyolefin 失效
标题翻译：立体特异性聚烯烃的制造方法
公开(公告)号：US5489634A
公开(公告)日：1996-02-06
申请号：US281134
申请日：1994-07-27
申请人： Daiji Hara , Morihiko Sato , Mitsuhiro Mori
发明人： Daiji Hara , Morihiko Sato , Mitsuhiro Mori
IPC分类号： C08F10/00 , C08F4/651 , C08F4/654
CPC分类号： C08F10/00 , Y10S526/904
摘要： A method for producing a stereospecific polyolefin in the presence of a catalyst comprising a transition metal compound and an organometallic compound, wherein a catalyst system is used which comprises (A) a solid catalyst component prepared by reacting a homogeneous solution containing (i) at least one member selected from the group consisting of metal magnesium and a hydroxylated organic compound, and oxygen-containing organic compounds of magnesium, (ii) an oxygen-containing organic compound of aluminum and (iii) an oxygen-containing organic compound of titanium, with (iv) at least one aluminum halide compound to obtain a solid product, and further reacting to this solid product, (v) an electron-donative compound and (vi) a titanium halide compound, (B) at least one member selected from the group consisting of organometallic compounds of Groups IA, IIA, IIB, IIIB and IVB of the Periodic Table, and (C) an oxygen-containing organic compound of silicon which has no aromatic substituent and which has at least one hydrocarbon group containing a secondary or tertiary carbon directly bonded to a silicon atom.
摘要翻译：在含有过渡金属化合物和有机金属化合物的催化剂存在下制备立体有择性聚烯烃的方法，其中使用催化剂体系，其包括（A）固体催化剂组分，其通过使含有（i）至少选自金属镁和羟基化有机化合物的一种成员和镁的含氧有机化合物，（ii）铝的含氧有机化合物和（iii）含氧有机化合物的钛，与（iv）至少一种卤化铝化合物，以获得固体产物，并进一步与该固体产物反应，（v）给电子化合物和（vi）卤化钛化合物，（B）至少一种选自由元素周期表的IA，IIA，IIB，IIIB和IVB族的有机金属化合物组成的组，和（C）不含芳族取代基的硅的含氧有机化合物并且其具有至少一个含有直接键合到硅原子上的仲或叔碳的烃基。

3. 发明授权

US5594079A Method for producing a polyolefin 失效
标题翻译：聚烯烃的制造方法
公开(公告)号：US5594079A
公开(公告)日：1997-01-14
申请号：US601473
申请日：1996-02-14
申请人： Daiji Hara , Masahiro Adachi , Mitsuhiro Mori
发明人： Daiji Hara , Masahiro Adachi , Mitsuhiro Mori
IPC分类号： C08F4/658 , C08F4/60 , C08F4/646 , C08F10/00 , C08F4/653 , C08F4/655 , C08F10/06
CPC分类号： C08F10/00
摘要： A method for producing a stereoregular polyolefin in the presence of a catalyst comprising a transition metal compound and an organometallic compound, which comprises polymerizing at least one olefin in the presence of a catalyst system comprising:(A) a solid catalyst component comprising Mg, Ti, halogen and an electron donative compound,(B) at least one member selected from the group consisting of organometallic compounds of metals of Groups IA, IIA, IIB, IIIB and IVB of the Periodic Table,(C) an electron donative compound, and(D) a boron compound of the formula R.sup.1.sub.n BX.sub.3-n wherein R.sup.1 is a hydrocarbon group and/or a halogenated hydrocarbon group, X is a halogen atom, and 0.ltoreq.n.ltoreq.3.
摘要翻译：一种在包含过渡金属化合物和有机金属化合物的催化剂存在下制备立构规则聚烯烃的方法，其包括在催化剂体系存在下聚合至少一种烯烃，所述催化剂体系包含：（A）包含Mg，Ti ，卤素和给电子化合物，（B）选自元素周期表第IA，IIA，IIB，IIIB和IVB族金属的有机金属化合物中的至少一种，（C）给电子化合物，和（D）式R1nBX3-n的硼化合物，其中R1是烃基和/或卤代烃基，X是卤素原子，且0

4. 发明授权

US5229476A Method for producing a stereospecific polyolefin 失效
标题翻译：生产立体聚烯烃的方法
公开(公告)号：US5229476A
公开(公告)日：1993-07-20
申请号：US749132
申请日：1991-08-23
申请人： Daiji Hara , Mitsuhiro Mori , Yozo Kondo
发明人： Daiji Hara , Mitsuhiro Mori , Yozo Kondo
IPC分类号： C08F4/60 , C08F4/658 , C08F10/00
CPC分类号： C08F10/00 , Y10S526/903 , Y10S526/904
摘要： A method for producing a stereospecific polyolefin in the presence of a catalyst comprising a transition metal compound and an organometallic compound, wherein a catalyst system is used which comprises: (A) a solid catalyst component prepared by reacting a homogeneous solution containing (i-1) magnesium and a hydroxylated organic compound, (i-2) an oxygen-containing organic compound of titanium and/or (i-3) an oxygen-containing organic compound of silicon and an oxygen-containing organic compound of aluminum and/or a boron compound, with (ii) at least one aluminum halide compound to obtain a solid product, and further reacting to this solid product (iii) an electron-donative compound, (iv) a titanium halide compound, and (v) ethylene and/or an .alpha.-olefin having at least 3 carbon atoms, (B) at least one member selected from the group consisting of organometallic compounds of Groups IA, IIA, IIB, IIIB and IVB of the Periodic Table, and (C) an electron-donative compound. A highly stereospecific polymer having good configuration of particles can be obtained in good yield by the method of the present invention.

5. 发明授权

US5112927A Method for producing a stereoregular polyolefin 失效
标题翻译：用于生产异构多聚烯烃的方法
公开(公告)号：US5112927A
公开(公告)日：1992-05-12
申请号：US454401
申请日：1989-12-21
申请人： Daiji Hara , Mitsuhiro Mori , Yozo Kondo
发明人： Daiji Hara , Mitsuhiro Mori , Yozo Kondo
IPC分类号： C08F4/656 , C08F10/00
CPC分类号： C08F10/00
摘要： A method for producing a stereoregular polyolefin in the presence of a catalyst comprising a transition metal compound and an organometallic compound, wherein a catalyst system is employed which comprises (i), (ii) and (iii): (A) a solid catalyst component obtained by reacting to a uniform solution containing (i) at least one member selected from the group consisting of metallic magnesium and an organic hydroxide compound and an oxygen-containing organic magnesium compound, (ii) a compound of Group IIIB of the Periodic Table, and (iii) an oxygen-containing organic silicon compound, (iv) at least one aluminum halide, to obtain a solid product, and reacting to the solid product, (v) an electron donative compound, and (vi) a titanium halide compound; (B) at least one member selected from the group consisting of organometallic compounds of metals of Groups IA, IIA, IIB, IIIB and IVB of the Periodic Table; and (C) an electron donative compound.

6. 发明授权

US08907038B2 Typical metal containing polysiloxane composition, process for its production, and its uses 有权
标题翻译：典型的含金属聚硅氧烷组合物，其生产方法及其用途
公开(公告)号：US08907038B2
公开(公告)日：2014-12-09
申请号：US13704014
申请日：2011-06-08
申请人： Daiji Hara , Masato Shimizu
发明人： Daiji Hara , Masato Shimizu
IPC分类号： C08G77/12 , H01L23/29 , C08G77/18 , C08L83/04 , C09D183/04 , C08G77/20 , H01L33/56
CPC分类号： C08G77/18 , C08G77/12 , C08G77/20 , C08L83/04 , C09D183/04 , H01L23/296 , H01L33/56 , H01L2924/0002 , H01L2924/12044 , C08L83/00 , H01L2924/00
摘要： A material suitable for sealing an LED element or for a gas barrier layer for a resin component, and an LED device, an FPD device and a semiconductor device using it. A process for producing a polymer composition, which includes mixing and reacting as component (A), an unsaturated group-containing siloxane compound of the following formula (1): wherein the siloxane structure is a chain or cyclic structure, as component (B), a siloxane compound having a structure of the following formula (2) wherein hydrogen is directly bonded to silicon, wherein the siloxane structure is a chain or cyclic structure, as component (C), at least one member selected from the group consisting of organic metal compounds of Group 1, 2, 12, 13 and 14 metals of the periodic table, and as component (D), a metal catalyst of Group 8, 9 or 10 metal of the periodic table.
摘要翻译：适用于密封LED元件或用于树脂部件的阻气层的材料，以及LED器件，FPD器件和使用它的半导体器件。聚合物组合物的制造方法，其包含将（A）成分与下述式（1）所示的不饱和基团的硅氧烷化合物混合反应：其中，硅氧烷结构为链状或环状结构，作为（B）成分，，具有下式（2）结构的硅氧烷化合物，其中氢直接与硅结合，其中硅氧烷结构为链或环状结构，作为组分（C），选自有机元素周期表第1,2,12,13,14族金属的金属化合物和组分（D），元素周期表第8,9或10族金属的金属催化剂。

7. 发明授权

US08513448B2 Cyclic siloxane compound, a material for forming Si-containing film, and its use 有权
标题翻译：环状硅氧烷化合物，用于形成含Si膜的材料及其用途
公开(公告)号：US08513448B2
公开(公告)日：2013-08-20
申请号：US11815194
申请日：2006-01-17
申请人： Daiji Hara , Mayumi Takamori
发明人： Daiji Hara , Mayumi Takamori
IPC分类号： C07F7/00
CPC分类号： C07F7/21 , C23C16/401 , H01L21/02123 , H01L21/02216 , H01L21/02274 , H01L21/31604
摘要： The present invention has the objects to provide a novel material for forming Si-containing film, especially a material containing a cyclic siloxane compound suitable to a PECVD equipment for low dielectric constant insulating film, and to provide an Si-containing film using the same, and a semiconductor device containing those films. The present invention relates to a material for forming Si-containing film, containing a cyclic siloxane compound represented by the following general formula (1) (In the formula, A represents a group containing at least one selected from the group consisting of an oxygen atom, a boron atom and a nitrogen atom, n is 1 or 2, and x is an integer of from 2 to 10.), and its use.
摘要翻译：本发明的目的是提供一种用于形成含Si膜的新型材料，特别是含有适用于低介电常数绝缘膜的PECVD设备的环状硅氧烷化合物的材料，并提供使用该Si的膜的含Si膜，以及包含这些膜的半导体器件。本发明涉及含有由以下通式（1）表示的环状硅氧烷化合物的含Si膜的材料（式中，A表示含有选自氧原子中的至少一种的基团），硼原子和氮原子，n为1或2，x为2至10的整数）及其用途。

8. 发明授权

US09970103B2 Film deposition material, sealing film using the same and use thereof 有权
公开(公告)号：US09970103B2
公开(公告)日：2018-05-15
申请号：US15212895
申请日：2016-07-18
申请人： Daiji Hara , Masato Shimizu
发明人： Daiji Hara , Masato Shimizu
IPC分类号： C23C16/40 , H01L21/02 , C23C16/30 , C23C16/50
CPC分类号： C23C16/401 , C23C16/30 , C23C16/50 , H01L21/02126 , H01L21/02216 , H01L21/02274
摘要： The present invention relates to a film composed of a carbon-containing silicon oxide formed by CVD using, as the raw material, an organosilicon compound having a secondary hydrocarbon group directly bonded to at least one silicon atom and having an atomic ratio of 0.5 or less oxygen atom with respect to 1 silicon atom, which is used as a sealing film for a gas barrier equipment and materials, an FPD device, a semiconductor device and the like.

9. 发明授权

US07935425B2 Insulating film material containing organic silane or organic siloxane compound, method for producing same, and semiconductor device 有权
标题翻译：含有有机硅烷或有机硅氧烷化合物的绝缘膜材料，其制造方法和半导体器件
公开(公告)号：US07935425B2
公开(公告)日：2011-05-03
申请号：US10536352
申请日：2003-11-28
申请人： Daiji Hara , Keisuke Yoshida
发明人： Daiji Hara , Keisuke Yoshida
IPC分类号： B32B9/04 , C23C16/40
CPC分类号： H01L21/02126 , B05D1/62 , C07F7/1804 , C07F7/1876 , C07F7/21 , C23C16/401 , H01L21/02216 , H01L21/02274 , H01L21/3121 , H01L21/3122 , H01L21/31633 , H01L2924/0002 , H01L2924/00
摘要： A material for insulating film suitable as an interlayer insulating material for a semiconductor device, from which an insulating film is formed by chemical vapor deposition, and an insulating film formed from such a material and a semiconductor device employing an insulating film, are provided.A material for insulating film comprising an organosilicon compound which is one of an organosilane compound in which a secondary hydrocarbon group and an alkenyl group, or an alkenyl group, is directly bonded to a silicon atom, or an organosiloxane compound in which a secondary hydrocarbon group and/or an alkenyl group is directly bonded to a silicon atom, represented by the formulae (1) to (4), from which an insulating film is formed by chemical vapor deposition of the organosilicon compound:
摘要翻译：提供了适合作为半导体器件的层间绝缘材料的绝缘膜的材料，通过化学气相沉积形成绝缘膜，以及由这种材料形成的绝缘膜和采用绝缘膜的半导体器件。或作为其中第二烃基和链烯基或链烯基直接与硅原子结合的有机硅烷化合物的有机硅化合物或其中第二烃基和/或链烯基直接键合到由式（1）至（4）表示的硅原子上，通过有机硅化合物的化学气相沉积形成绝缘膜：

10. 发明申请

US20100052114A1 CYCLIC SILOXANE COMPOUND, A MATERIAL FOR FORMING SI-CONTAINING FILM, AND ITS USE 有权
标题翻译：环状硅氧烷化合物，形成含有电影的材料及其使用
公开(公告)号：US20100052114A1
公开(公告)日：2010-03-04
申请号：US11815194
申请日：2006-01-17
申请人： Daiji Hara , Mayumi Takamori
发明人： Daiji Hara , Mayumi Takamori
IPC分类号： H01L29/00 , H01L21/31 , B01J19/12 , C07F7/08
CPC分类号： C07F7/21 , C23C16/401 , H01L21/02123 , H01L21/02216 , H01L21/02274 , H01L21/31604
摘要： The present invention has the objects to provide a novel material for forming Si-containing film, especially a material containing a cyclic siloxane compound suitable to a PECVD equipment for low dielectric constant insulating film, and to provide an Si-containing film using the same, and a semiconductor device containing those films. The present invention relates to a material for forming Si-containing film, containing a cyclic siloxane compound represented by the following general formula (1) (In the formula, A represents a group containing at least one selected from the group consisting of an oxygen atom, a boron atom and a nitrogen atom, n is 1 or 2, and x is an integer of from 2 to 10.), and its use.
摘要翻译：本发明的目的是提供一种用于形成含Si膜的新型材料，特别是含有适用于低介电常数绝缘膜的PECVD设备的环状硅氧烷化合物的材料，并提供使用该Si的膜的含Si膜，以及包含这些膜的半导体器件。本发明涉及含有由以下通式（1）表示的环状硅氧烷化合物的含Si膜的材料（式中，A表示含有选自氧原子中的至少一种的基团），硼原子和氮原子，n为1或2，x为2至10的整数）及其用途。

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