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1. 发明授权

US08679621B2 Materials and methods for autonomous restoration of electrical conductivity 有权
标题翻译：自主恢复导电性的材料和方法
公开(公告)号：US08679621B2
公开(公告)日：2014-03-25
申请号：US13164144
申请日：2011-06-20
申请人： Benjamin J. Blaiszik , Susan A. Odom , Mary M. Caruso , Aaron C. Jackson , Marta B. Baginska , Joshua A. Ritchey , Aaron D. Finke , Scott R. White , Jeffrey S. Moore , Nancy R. Sottos , Paul V. Braun , Khalil Amine
发明人： Benjamin J. Blaiszik , Susan A. Odom , Mary M. Caruso , Aaron C. Jackson , Marta B. Baginska , Joshua A. Ritchey , Aaron D. Finke , Scott R. White , Jeffrey S. Moore , Nancy R. Sottos , Paul V. Braun , Khalil Amine
IPC分类号： H01B3/30
CPC分类号： H01B1/02 , Y10T428/249997
摘要： An autonomic conductivity restoration system includes a solid conductor and a plurality of particles. The particles include a conductive fluid, a plurality of conductive microparticles, and/or a conductive material forming agent. The solid conductor has a first end, a second end, and a first conductivity between the first and second ends. When a crack forms between the first and second ends of the conductor, the contents of at least a portion of the particles are released into the crack. The cracked conductor and the released contents of the particles form a restored conductor having a second conductivity, which may be at least 90% of the first conductivity.
摘要翻译：自主导电恢复系统包括固体导体和多个颗粒。颗粒包括导电流体，多个导电微粒和/或导电材料形成剂。固体导体具有在第一和第二端之间的第一端，第二端和第一导电性。当在导体的第一和第二端之间形成裂纹时，至少一部分颗粒的内容物被释放到裂纹中。破裂的导体和释放的颗粒的内容物形成具有第二导电性的恢复的导体，其可以是第一导电率的至少90％。

2. 发明申请

US20120067615A1 Materials and Methods for Autonomous Restoration of Electrical Conductivity 有权
标题翻译：电导率自动恢复的材料与方法
公开(公告)号：US20120067615A1
公开(公告)日：2012-03-22
申请号：US13164144
申请日：2011-06-20
申请人： Benjamin J. Blaiszik , Susan A. Odom , Mary M. Caruso , Aaron C. Jackson , Marta B. Baginska , Joshua A. Ritchey , Aaron D. Finke , Scott R. White , Jeffrey S. Moore , Nancy R. Sottos , Paul V. Braun , Khalil Amine
发明人： Benjamin J. Blaiszik , Susan A. Odom , Mary M. Caruso , Aaron C. Jackson , Marta B. Baginska , Joshua A. Ritchey , Aaron D. Finke , Scott R. White , Jeffrey S. Moore , Nancy R. Sottos , Paul V. Braun , Khalil Amine
IPC分类号： H01B3/30
CPC分类号： H01B1/02 , Y10T428/249997
摘要： An autonomic conductivity restoration system includes a solid conductor and a plurality of particles. The particles include a conductive fluid, a plurality of conductive microparticles, and/or a conductive material forming agent. The solid conductor has a first end, a second end, and a first conductivity between the first and second ends. When a crack forms between the first and second ends of the conductor, the contents of at least a portion of the particles are released into the crack. The cracked conductor and the released contents of the particles form a restored conductor having a second conductivity, which may be at least 90% of the first conductivity.
摘要翻译：自主导电恢复系统包括固体导体和多个颗粒。颗粒包括导电流体，多个导电微粒和/或导电材料形成剂。固体导体具有在第一和第二端之间的第一端，第二端和第一导电性。当在导体的第一和第二端之间形成裂纹时，至少一部分颗粒的内容物被释放到裂纹中。破裂的导体和释放的颗粒的内容物形成具有第二导电性的恢复的导体，其可以是第一导电率的至少90％。

3. 发明申请

US20130171484A1 Materials and Methods for Autonomous Battery Shutdown 审中-公开
标题翻译：自主电池关机的材料和方法
公开(公告)号：US20130171484A1
公开(公告)日：2013-07-04
申请号：US13489871
申请日：2012-06-06
申请人： Marta B. Baginska , Benjamin J. Blaiszik , Aaron Esser-Kahn , Susan A. Odom , Wei Weng , Zhengcheng Zhang , Nancy R. Sottos , Scott R. White , Jeffrey S. Moore , Khalil Amine
发明人： Marta B. Baginska , Benjamin J. Blaiszik , Aaron Esser-Kahn , Susan A. Odom , Wei Weng , Zhengcheng Zhang , Nancy R. Sottos , Scott R. White , Jeffrey S. Moore , Khalil Amine
IPC分类号： H01M10/056 , H01M10/0525
CPC分类号： H01M10/056 , H01M10/0525 , H01M10/4235
摘要： An autonomous battery shutdown system includes a battery including an anode and a cathode, and an electrolyte composition between the anode and the cathode. The electrolyte composition includes an ionically conductive liquid containing lithium ions, and temperature-sensitive particles including a polymer having a melting temperature between 60° C. and 120° C. When the temperature of the battery exceeds 120° C., the temperature-sensitive particles form an ion barrier that traverses the battery. The resulting shutdown battery may have a specific charge capacity that is more than 98% lower than the specific charge capacity of the original battery.
摘要翻译：自主的电池关闭系统包括包括阳极和阴极的电池，以及在阳极和阴极之间的电解质组合物。电解质组合物包含含有锂离子的离子导电性液体，以及包含熔点为60℃〜120℃的聚合物的温度敏感性粒子。当电池温度超过120℃时，温度敏感颗粒形成穿过电池的离子屏障。所产生的关闭电池可能具有比原始电池的特定充电容量低98％以上的特定充电容量。

4. 发明授权

US08846404B2 System for visual indication of mechanical damage 有权
标题翻译：机械损伤视觉指示系统
公开(公告)号：US08846404B2
公开(公告)日：2014-09-30
申请号：US13168166
申请日：2011-06-24
申请人： Susan A. Odom , Mary M. Caruso , Aaron D. Finke , Aaron C. Jackson , Jeffrey S. Moore , Nancy R. Sottos , Scott R. White
发明人： Susan A. Odom , Mary M. Caruso , Aaron D. Finke , Aaron C. Jackson , Jeffrey S. Moore , Nancy R. Sottos , Scott R. White
IPC分类号： G01N31/22 , G01N21/78 , B29C73/22
CPC分类号： G01N21/78
摘要： A self-indicating material system may include a solid polymer matrix having a first color, a first plurality of capsules in the matrix, and a plurality of particles in the matrix. The first plurality of capsules includes a first reactant, and the plurality of particles includes a second reactant, which forms a product when in contact with the first reactant. When a crack forms in the polymer matrix, at least a portion of the first plurality of capsules is ruptured, the first and second reactants form the product in the matrix, and the portion of the polymer matrix containing the product has a second color different from the first color. A self-indicating material system may include a solid polymer matrix, a plurality of capsules in the matrix, and an activator in the matrix, where the polymer matrix includes a first polymer and has a first color, the plurality of capsules includes a polymerizer, and the activator is an activator for the polymerizer. When a crack forms in the polymer matrix, at least a portion of the plurality of capsules is ruptured, the polymerizer and the activator form a second polymer in the crack, and the second polymer has a second color different from the first color.
摘要翻译：自指示材料系统可以包括具有第一颜色的固体聚合物基质，基质中的第一多个胶囊和基质中的多个颗粒。第一多个胶囊包括第一反应物，并且多个颗粒包括第二反应物，其在与第一反应物接触时形成产物。当在聚合物基体中形成裂纹时，第一多个胶囊的至少一部分破裂，第一和第二反应物在基质中形成产物，并且含有产物的聚合物基质的部分具有不同于第一种颜色。自指示材料系统可以包括固体聚合物基质，基质中的多个胶囊和基质中的活化剂，其中聚合物基质包括第一聚合物并且具有第一颜色，所述多个胶囊包括聚合反应器，并且活化剂是聚合反应器的活化剂。当在聚合物基质中形成裂纹时，多个胶囊的至少一部分破裂，聚合器和活化剂在裂纹中形成第二聚合物，并且第二聚合物具有与第一颜色不同的第二颜色。

5. 发明申请

US20120196373A1 System For Visual Indication Of Mechanical Damage 有权
标题翻译：机械损伤视觉指示系统
公开(公告)号：US20120196373A1
公开(公告)日：2012-08-02
申请号：US13168166
申请日：2011-06-24
申请人： Susan A. Odom , Mary M. Caruso , Aaron D. Finke , Aaron C. Jackson , Jeffrey S. Moore , Nancy R. Sottos , Scott R. White
发明人： Susan A. Odom , Mary M. Caruso , Aaron D. Finke , Aaron C. Jackson , Jeffrey S. Moore , Nancy R. Sottos , Scott R. White
IPC分类号： G01N21/75
CPC分类号： G01N21/78
摘要： A self-indicating material system may include a solid polymer matrix having a first color, a first plurality of capsules in the matrix, and a plurality of particles in the matrix. The first plurality of capsules includes a first reactant, and the plurality of particles includes a second reactant, which forms a product when in contact with the first reactant. When a crack forms in the polymer matrix, at least a portion of the first plurality of capsules is ruptured, the first and second reactants form the product in the matrix, and the portion of the polymer matrix containing the product has a second color different from the first color. A self-indicating material system may include a solid polymer matrix, a plurality of capsules in the matrix, and an activator in the matrix, where the polymer matrix includes a first polymer and has a first color, the plurality of capsules includes a polymerizer, and the activator is an activator for the polymerizer. When a crack forms in the polymer matrix, at least a portion of the plurality of capsules is ruptured, the polymerizer and the activator form a second polymer in the crack, and the second polymer has a second color different from the first color.
摘要翻译：自指示材料系统可以包括具有第一颜色的固体聚合物基质，基质中的第一多个胶囊和基质中的多个颗粒。第一多个胶囊包括第一反应物，并且多个颗粒包括第二反应物，其在与第一反应物接触时形成产物。当在聚合物基体中形成裂纹时，第一多个胶囊的至少一部分破裂，第一和第二反应物在基质中形成产物，并且含有产物的聚合物基质的部分具有不同于第一种颜色。自指示材料系统可以包括固体聚合物基质，基质中的多个胶囊和基质中的活化剂，其中聚合物基质包括第一聚合物并且具有第一颜色，所述多个胶囊包括聚合反应器，并且活化剂是聚合反应器的活化剂。当在聚合物基质中形成裂纹时，多个胶囊的至少一部分破裂，聚合器和活化剂在裂纹中形成第二聚合物，并且第二聚合物具有与第一颜色不同的第二颜色。

6. 发明授权

US09108364B2 Solvent-promoted self-healing materials 有权
标题翻译：溶剂促进自愈材料
公开(公告)号：US09108364B2
公开(公告)日：2015-08-18
申请号：US12739537
申请日：2008-10-27
申请人： Mary M. Caruso , David A. Delafuente , Benjamin J. Blaiszik , Jason M. Kamphaus , Nancy R. Sottos , Scott R. White , Jeffrey S. Moore
发明人： Mary M. Caruso , David A. Delafuente , Benjamin J. Blaiszik , Jason M. Kamphaus , Nancy R. Sottos , Scott R. White , Jeffrey S. Moore
IPC分类号： B29C73/22 , B29C73/16
CPC分类号： B29C73/163 , B29C73/22
摘要： A composite material includes a solid polymer matrix, a plurality of capsules and a liquid, in the capsules. The liquid includes from 50 to 100 wt % of a solvent, and from 0 to 50 wt % of a polymerizer. There is no polymerizer outside of the capsules. The solid polymer matrix may include a native activating moiety for the polymerizer. The solvent may have a swelling ratio with the solid polymer matrix of at least 1.1 and/or may have a polarity ET of from 0.10 to 0.50.
摘要翻译：复合材料包括胶囊中的固体聚合物基质，多个胶囊和液体。液体包含50-100重量％的溶剂和0-50重量％的聚合反应器。胶囊外没有聚合反应器。固体聚合物基质可以包括用于聚合反应器的天然活化部分。溶剂可以具有至少1.1的固体聚合物基质的溶胀比和/或可以具有0.10-0.50的极性ET。

7. 发明申请

US20130072596A1 Thermally Robust Capsule System, And Composites Including The Capsules 有权
标题翻译：耐热胶囊系统，以及包括胶囊的复合材料
公开(公告)号：US20130072596A1
公开(公告)日：2013-03-21
申请号：US13421986
申请日：2012-03-16
申请人： Scott R. White , Jeffrey S. Moore , Nancy R. Sottos , Benjamin J. Blaiszik , Mary M. Caruso
发明人： Scott R. White , Jeffrey S. Moore , Nancy R. Sottos , Benjamin J. Blaiszik , Mary M. Caruso
IPC分类号： C08L75/04 , B01J13/20
CPC分类号： C08L75/04 , B01J13/20 , B01J13/22 , Y10T428/2982 , Y10T428/2984 , Y10T428/2989
摘要： A method of making capsules includes forming a mixture including a core liquid, a polyurethane precursor system, a first component of a two-component poly(urea-formaldehyde) precursor system, and a solvent. The method further includes emulsifying the mixture, adding a second component of the two-component poly(urea-formaldehyde) precursor system to the emulsified mixture, and maintaining the emulsified mixture at a temperature and for a time sufficient to form a plurality of capsules that encapsulate at least a portion of the core liquid. The capsules made by the method may include a polymerizer in the capsules, where the capsules have an inner capsule wall including a polyurethane, and an outer capsule wall including a poly(urea-formaldehyde). The capsules may include in the solid polymer matrix of a composite material.
摘要翻译：制备胶囊的方法包括形成包括核心液体，聚氨酯前体体系，双组分聚（脲 - 甲醛）前体体系的第一组分和溶剂的混合物。该方法还包括乳化混合物，向乳化混合物中加入双组分聚（脲 - 甲醛）前体体系的第二组分，并将乳化混合物保持在足以形成多个胶囊的温度和时间封装至少一部分芯液。通过该方法制备的胶囊可以包括在胶囊中的聚合反应器，其中胶囊具有包括聚氨酯的内胶囊壁和包含聚（脲 - 甲醛）的外胶囊壁。胶囊可以包括在复合材料的固体聚合物基质中。

8. 发明授权

US08951639B2 Thermally robust capsule system, and composites including the capsules 有权
标题翻译：热稳定的胶囊系统，以及包括胶囊的复合材料
公开(公告)号：US08951639B2
公开(公告)日：2015-02-10
申请号：US13421986
申请日：2012-03-16
申请人： Scott R. White , Jeffrey S. Moore , Nancy R. Sottos , Benjamin J. Blaiszik , Mary M. Caruso , Christian L. Mangun
发明人： Scott R. White , Jeffrey S. Moore , Nancy R. Sottos , Benjamin J. Blaiszik , Mary M. Caruso , Christian L. Mangun
IPC分类号： C08L75/04 , C08L79/08 , B01J13/20 , B01J13/22
CPC分类号： C08L75/04 , B01J13/20 , B01J13/22 , Y10T428/2982 , Y10T428/2984 , Y10T428/2989
摘要： A method of making capsules includes forming a mixture including a core liquid, a polyurethane precursor system, a first component of a two-component poly(urea-formaldehyde) precursor system, and a solvent. The method further includes emulsifying the mixture, adding a second component of the two-component poly(urea-formaldehyde) precursor system to the emulsified mixture, and maintaining the emulsified mixture at a temperature and for a time sufficient to form a plurality of capsules that encapsulate at least a portion of the core liquid. The capsules made by the method may include a polymerizer in the capsules, where the capsules have an inner capsule wall including a polyurethane, and an outer capsule wall including a poly(urea-formaldehyde). The capsules may include in the solid polymer matrix of a composite material.
摘要翻译：制备胶囊的方法包括形成包括核心液体，聚氨酯前体体系，双组分聚（脲 - 甲醛）前体体系的第一组分和溶剂的混合物。该方法还包括乳化混合物，向乳化混合物中加入双组分聚（脲 - 甲醛）前体体系的第二组分，并将乳化混合物保持在足以形成多个胶囊的温度和时间封装至少一部分芯液。通过该方法制备的胶囊可以包括在胶囊中的聚合反应器，其中胶囊具有包括聚氨酯的内胶囊壁和包含聚（脲 - 甲醛）的外胶囊壁。胶囊可以包括在复合材料的固体聚合物基质中。

9. 发明授权

US08383697B2 Systems for self-healing composite materials 有权
标题翻译：自愈复合材料系统
公开(公告)号：US08383697B2
公开(公告)日：2013-02-26
申请号：US12769904
申请日：2010-04-29
申请人： Gerald O. Wilson , Mary M. Caruso , Benjamin J. Blaiszik , James W. Henderson , Christopher Britt , Jeffrey S. Moore , Scott R. White , Nancy R. Sottos
发明人： Gerald O. Wilson , Mary M. Caruso , Benjamin J. Blaiszik , James W. Henderson , Christopher Britt , Jeffrey S. Moore , Scott R. White , Nancy R. Sottos
IPC分类号： A61K6/00 , C09K3/00
CPC分类号： A61L27/50 , A61L24/001 , A61L24/0094 , A61L27/48 , C08L33/08
摘要： A composite material precursor composition includes a matrix precursor, a first plurality of capsules including a liquid polymerizer, an activator, and an accelerant. The liquid polymerizer polymerizes when in contact with the activator, and the accelerant is an accelerant for the polymerization of the liquid polymerizer. The composite material precursor may be used to form a composite material that includes a solid polymer matrix, the first plurality of capsules in the solid polymer matrix, the activator in the solid polymer matrix, and the accelerant in the solid polymer matrix.
摘要翻译：复合材料前体组合物包括基质前体，包含液体聚合反应器，活化剂和促进剂的第一多个胶囊。液体聚合反应器在与活化剂接触时聚合，促进剂是液体聚合反应器聚合的促进剂。复合材料前体可以用于形成复合材料，其包括固体聚合物基质，固体聚合物基质中的第一多个胶囊，固体聚合物基质中的活化剂和固体聚合物基质中的促进剂。

10. 发明申请

US20110039980A1 Solvent-Promoted Self-Healing Materials 有权
标题翻译：溶剂促进自愈材料
公开(公告)号：US20110039980A1
公开(公告)日：2011-02-17
申请号：US12739537
申请日：2008-10-27
申请人： Mary M. Caruso , David A. Delafuente , Benjamin J. Blaiszik , Jason M. Kamphaus , Nancy R. Sottos , Scott R. White , Jeffrey S. Moore
发明人： Mary M. Caruso , David A. Delafuente , Benjamin J. Blaiszik , Jason M. Kamphaus , Nancy R. Sottos , Scott R. White , Jeffrey S. Moore
IPC分类号： C08K9/10
CPC分类号： B29C73/163 , B29C73/22
摘要： A composite material includes a solid polymer matrix, a plurality of capsules and a liquid, in the capsules. The liquid includes from 50 to 100 wt % of a solvent, and from 0 to 50 wt % of a polymerizer. There is no polymerizer outside of the capsules. The solid polymer matrix may include a native activating moiety for the polymerizer. The solvent may have a swelling ratio with the solid polymer matrix of at least 1.1 and/or may have a polarity ET of from 0.10 to 0.50. A composite material includes a solid polymer matrix, a plurality of capsules and a liquid, in the capsules. The liquid includes from 50 to 100 wt % of a solvent, and from 0 to 50 wt % of a polymerizer. There is no polymerizer outside of the capsules. The solid polymer matrix may include a native activating moiety for the polymerizer. The solvent may have a swelling ratio with the solid polymer matrix of at least 1.1 and/or may have a polarity ET of from 0.10 to 0.50.
摘要翻译：复合材料包括胶囊中的固体聚合物基质，多个胶囊和液体。液体包含50-100重量％的溶剂和0-50重量％的聚合反应器。胶囊外没有聚合反应器。固体聚合物基质可以包括用于聚合反应器的天然活化部分。溶剂可以具有至少1.1的固体聚合物基质的溶胀比和/或可以具有0.10-0.50的极性ET。复合材料包括胶囊中的固体聚合物基质，多个胶囊和液体。液体包含50-100重量％的溶剂和0-50重量％的聚合反应器。胶囊外没有聚合反应器。固体聚合物基质可以包括用于聚合反应器的天然活化部分。溶剂可以具有至少1.1的固体聚合物基质的溶胀比和/或可以具有0.10-0.50的极性ET。

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