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1. 发明授权

US3849524A O-ethyl-o-(3-methyl-4-methylmercaptophenyl)phosphoric acid diester chloride 失效
标题翻译： O-乙基-O-（3-甲基-4-甲基戊酸）磷酸二氯甲酯
公开(公告)号：US3849524A
公开(公告)日：1974-11-19
申请号：US29872872
申请日：1972-10-18
申请人： BAYER AG
发明人： MAURER F , ROHE L , COLLN R , HOFER W
IPC分类号： A01N57/34 , C07F9/14 , C07F9/146 , C07F9/24
CPC分类号： C07F9/1406 , C07F9/242
摘要： 1. O - ETHYL - O -(3-METHYL-4-METHYLMERCAPTOPHENYL)PHOSPHORIC ACID DIESTER CHLORIDE OF THE FORMULA

H3C-S-(2-(H3C-)-1,4-PHENYLENE)-O-P(=O)(-CL)-O-C2H5

2. 发明授权

US3787539A Thionothiolphosphoric acid o,s-diester amides 失效
标题翻译：硫代羟基磷酸，S-二氧化钛
公开(公告)号：US3787539A
公开(公告)日：1974-01-22
申请号：US3787539D
申请日：1971-12-08
申请人： BAYER AG
发明人： UNTERSTENHAFER G , BEHRENZ W , COLLN R , HAMMANN I
IPC分类号： C07F9/24 , A01N9/36 , C07F9/16
CPC分类号： C07F9/24
摘要： REACTING GASEOUS AMMONIA, THIONOTHIOLPHOSPHORIC ACID S-ESTER DICHLORIDE AND A HYDROXY COMPOUND; I.E. GASEOUS AMMONIA, THIONOTHIOLPHOSPHORIC ACID-S(ALKYL, ALKENYL, HALOALKYL, ALKOXY-ALKYL, ALKYLMERCAPTOALKYL, CYCLOALKYL, PHENYLALKYL, PHENYL AND HALOPHENYL)-ESTER DICHLORIDE, ESPECIALLY THIONOTHIOLPHOSPHORIC ACID-S(ALKYL, PHENYLALKYL, PHENYL AND CHLOROPHENYL)-ESTER DICHLORIDE, AND AN ALKANOL, ALKENOL, HALOALKANOL, PHENYLAKAAKANOL, ALKYLMERCAPTO-ALKANOL, CYCLOALKANOL, PHENALKANOL, PHENOL OR HALOPHENOL, ESPECIALLY AN ALKANOL, ALKENOL, CHLOROALKANOL, ALKOXY-ALKANOL, ALKYLMERCAPTO-ALKANOL, CYCLOALKANOL, PHENOL OR CHLOROPHENOL; BY INTRODUCING GASEOUS AMMONIA UNTIL SATURATION INTO A MIXTURE OF SUCH S-ESTER DICHLORIDE AND HYDROXY COMPOUND, AT A TEMPERATURE OF ABOUT -10 TO +20*C., OP TIONALLY IN THE PRESENCE OF AN INERT ORGANIC SOLVENT OR DILUENT; TO FORM THE CORRESPONDING THIONOTHIOLPHOSPHORIC ACID O,S-DI(ALKYL, ALKENYL, HALOALKYL, ALKOXY-ALKYL, ALKYLMERCAPTO-ALKYL, CYCLOALKYL PHENYLALKYL PHENYL AND/OR HALOPHENYL) ESTER AMIDES SOME OF WHICH ARE NEW COMPOUNDS AND ALL OF WHICH POSSES INSECTICIDAL ACARICIDAL AND BIRD AND RODENT-REPELLENT PROPERTIES.

3. 发明授权

US3839512A Process for the preparation of thiolphosphoric acid o,s-dialkyl ester amides 失效
标题翻译：制备硫代磷酸，S-二烷基酯酰胺的方法
公开(公告)号：US3839512A
公开(公告)日：1974-10-01
申请号：US79387369
申请日：1969-01-24
申请人： BAYER AG
发明人： COLLN R
IPC分类号： C07F9/24 , C07F9/16
CPC分类号： C07F9/2408
摘要： 1. PROCESS FOR THE PRODUCTION OF THIOLPHOSPHORIC ACID O,S-DIALKYL ESTER AMIDE OF THE FORMULA

R-S-P(=O)(-NH2)-O-R1

IN WHICH R AND R'', EACH INDIVIDUALLY, IS LOWER ALKYL, WHICH COMPRISES REACTING THIOLPHOSPHORIC ACID S-ALKYL ESTER DICHLORIDE OR THE FORMULA

R-S-P(=O)(-CL)2

IN WHICH R IS THE SAME AS DEFINED ABOVE, SIMULTANEOUSLY WITH AMMONIA AND A LOWER ALKANOL OF TE FORMULA R''OH IN WHICH R'' IS THE SAME AS DEFINED ABOVE, AT A TEMPERAUTE SUBSTANTIALLY BETWEEN ABOUT -10 AND +20: C., TO FORM THE CORRESPONDING THIOPHOSPHORIC ACID O,S-DIALKYL ESTER AMIDE.

4. 发明授权

US3813457A Preparation of n-unsubstituted (thiono)-(thiol)-phosphoric(phosphonic) acid o-ester mono-amides 失效
标题翻译： N-巯基 - （硫代） - 磷酸（磷酸）酸酯单体的制备
公开(公告)号：US3813457A
公开(公告)日：1974-05-28
申请号：US27039072
申请日：1972-07-10
申请人： BAYER AG
发明人： COLLN R
IPC分类号： C07F9/24 , C07F9/44
CPC分类号： C07F9/44 , C07F9/24
摘要： A PROCESS FOR THE PREPARATION OF AN N-UNSUBSITUTED PHOSPHORIC OR PHOSPHONIC ACID O-ESTER MONO-AMIDE, OR THE CORRESPONDING THIONO, THIOL OR THIONOTHIOL O-ESTER MONO-AMIDE, WHICH COMPRISES CONTACTING AT A TEMPERATURE OF ABOUT -10 TO 70*C. THE CORRESPONDING N-UNSUBSTITUTED PHOSPHORIC OR PHOSPHONIC ACID DIAMIDE WITH AT LEAST AN EQUIVALENT AMOUNT OF AN ALCOHOL IN THE PRESENCE OF AN APPROXIMATELY EQUIVALENT AMOUNT OF A STRONG MINERAL ACID. THE STRONG ACID PREFERABLY IS HYDROGEN CHLORIDE WHICH MAY BE ADDED BY BUBBLING IN OR BY DROPWISE ADDITION IN A DILUENT WHICH MAY COMPRISE EXCESS ALCOHOL. THE INITAL DIAMIDE MAY BE USED IN UNPURIFIED FORM IN ADMIXTURE WITH AMMONIUM CHLORIDE AS OBTAINED BY REACTION OF THE CORRESPONDING DIHALIDE WITH AMMONIA. IN CONTRAST WITH SUBSTITUTED AMIDE STARTING MATERIALS THE REACTION IS EXTREMELY SELECTIVE TOWARD PRODUCING THE O-ESTER MONOAMIDE SUBSTANTIALLY FREE OF O,O-DIESTER. THE PRODUCTS EXHIBIT INSECTICIDAL AND ACARICIDAL ACTIVITY AND CAN ALSO BE USED TO SYNTHESIZE OTHER INSECTICIDES AND ACARICIDES.

5. 发明专利

BR7802714A 未知
公开(公告)号：BR7802714A
公开(公告)日：1979-01-23
申请号：BR7802714
申请日：1978-05-02
申请人： BAYER AG
发明人： COLLN R , LURSSEN K
IPC分类号： A01N57/20 , A01N5/00 , A01N9/36

6. 发明专利

SE7602120L 未知
公开(公告)号：SE7602120L
公开(公告)日：1976-09-22
申请号：SE7602120
申请日：1976-02-23
申请人： BAYER AG
发明人： COLLN R , SERRENBERG W , BEHREJ Z W , STENDEL W
IPC分类号： A01N57/20 , A01N57/12 , A01P7/04 , C07F9/38 , C07F9/40
摘要： 1-Hydroxy-2,2,2-trichloroethane-thionophosphonic acid dialkyl esters of the formula (I) in which R and R1 each independently is an alkyl radical with 1 to 4 carbon atoms, which possess arthropodicidal properties.

7. 发明专利

DK133900B 未知
公开(公告)号：DK133900B
公开(公告)日：1976-08-09
申请号：DK551774
申请日：1974-10-22
申请人： BAYER AG
发明人： COLLN R , HAMMANN I
IPC分类号： A01N57/32 , A01P7/02 , A01P7/04 , C07F9/6561 , A01N9/36 , C07F9/65

8. 发明专利

DK132177B 未知
公开(公告)号：DK132177B
公开(公告)日：1975-11-03
申请号：DK32473
申请日：1973-01-19
申请人： BAYER AG
发明人： COLLN R , SIRRENBERG W , BEHRENZ W , HAMMANN I
IPC分类号： A01N57/28 , C07F9/24 , A01N9/36
摘要： 1393632 Pesticidal thionophosphoramidates BAYER AG 19 Jan 1973 [21 Jan 1972] 2892/73 Addition to 1348365 Heading C2P Novel compounds of Formula I where R is CH 3 , C 2 H 5 , n-C 3 H 7 , n-C 4 H 9 , i-C 4 H 9 , i-C 3 H 7 , or n-C 7 H 15 may be prepared by reacting 0-(2,2-dichlorovinyl)-phosphorodiamidothionate with a compound ROH, hydrogen chloride being supplied to the reaction mixture. The compounds of Formula I have insecticidal, acaricidal and fungicidal properties and may be used as the active ingredients in conventional pesticidal compositions.

9. 发明专利

DK551774A 未知
公开(公告)号：DK551774A
公开(公告)日：1975-06-16
申请号：DK551774
申请日：1974-10-22
申请人： BAYER AG
发明人： COLLN R , HAMMANN I
IPC分类号： A01N57/32 , A01P7/02 , A01P7/04 , C07F9/6561 , C07F9/24

10. 发明专利

BR7404980D0 未知
公开(公告)号：BR7404980D0
公开(公告)日：1975-01-07
申请号：BR498074
申请日：1974-06-18
申请人： BAYER AG
发明人： COLLN R , LUERSSEN K
IPC分类号： A01N57/20 , A01P21/00 , C07F9/38 , C07F9/40 , A01N5/00

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