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1. 发明授权

US5098886A Substituted and unsubstituted alkyl cyclohexylmenthyl and cyclohexenylmethyl carbonates and perfumery uses thereof 失效
标题翻译：取代和未取代的烷基环己基甲基和环己烯基甲基碳酸酯及其香料用途
公开(公告)号：US5098886A
公开(公告)日：1992-03-24
申请号：US666031
申请日：1991-03-17
申请人： Anubhav P. S. Narula , Leroy John , Anton V. Ouwerkerk , Vincent F. Kuczinski , Sophia Grojsman
发明人： Anubhav P. S. Narula , Leroy John , Anton V. Ouwerkerk , Vincent F. Kuczinski , Sophia Grojsman
IPC分类号： A01N47/06 , C07C69/96 , C11B9/00
CPC分类号： C11B9/0034 , A01N47/06 , C07C69/96
摘要： Described are alkyl cyclohexylmethyl and cyclohexenylmethyl carbonates defined according to the structure: ##STR1## wherein R.sub.1 is methyl or ethyl and wherein R.sub.2, R.sub.3, R.sub.4 and R.sub.6 are the same or different hydrogen or methyl and wherein the dashed line is a carbon-carbon single bond or a carbon-carbon double bond and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles such as solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softeners, fabric softener articles, hair sprays, shampoos, bath oils and perfumed polymers.
摘要翻译：描述了根据以下结构定义的烷基环己基甲基和环己烯基甲基碳酸酯：其中R 1是甲基或乙基，并且其中R 2，R 3，R 4和R 6是相同或不同的氢或甲基，并且其中虚线是碳 - 碳单键或碳 - 碳双键，并且其用于增强或增强香料组合物，古龙水和香料制品如固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂，织物柔软剂制品，喷发剂，洗发剂，浴油和加香聚合物。

2. 发明授权

US5100872A Substituted and unsubstituted alkyl cyclohexylmethyl and cyclohexenylmethyl carbonates and perfumery uses thereof 失效
标题翻译：取代和未取代的烷基环己基甲基和环己基甲基碳酸酯及其制备方法
公开(公告)号：US5100872A
公开(公告)日：1992-03-31
申请号：US729381
申请日：1991-07-12
申请人： Anubhav P. S. Narula , Leroy John , Anton V. Ouwerkerk , Vincent F. Kuczinski , Sophia Grojsman
发明人： Anubhav P. S. Narula , Leroy John , Anton V. Ouwerkerk , Vincent F. Kuczinski , Sophia Grojsman
IPC分类号： A01N47/06 , C07C69/96 , C11B9/00
CPC分类号： C11B9/0034 , A01N47/06 , C07C69/96
摘要： Described are alkyl cyclohexylmethyl and cyclohexenylmethyl carbonates defined according to the generic structure: ##STR1## wherein R.sub.1 is methyl or ethyl; R.sub.2, R.sub.3, R.sub.4 and R.sub.6 represents hydrogen or methyl; R.sub.5 represents hydrogen, methyl or methylene; and R.sub.7 represents hydrogen or C.sub.1 -C.sub.4 straight chain lower alkyl or isopropyl or R.sub.7 is no moiety; each of the dashed lines represents a carbon-carbon single bond or a carbon-carbon double bond; the wavy line represents a carbon-carbon single bond or no bond; with the provisos that:(a) at least three of the dashed lines each represents a carbon-carbon single bond;(b) when R.sub.7 is no moiety, the dashed line at the "1-6" position is a carbon-carbon double bond;(c) when the wavy line is a carbon-carbon single bond then R.sub.5 is methylene and the carbon-carbon bond at the "4-5" position and at the "5-6" position is a carbon-carbon single bond;and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles, such as solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softeners, fabric softener articles, hair sprays, shampoos, bath oils and perfumed polymers.
摘要翻译：描述了根据通用结构定义的烷基环己基甲基和环己烯基甲基碳酸酯：其中R 1是甲基或乙基; R2，R3，R4和R6代表氢或甲基; R5代表氢，甲基或亚甲基; 并且R 7表示氢或C 1 -C 4直链低级烷基或异丙基或R 7不是部分; 每个虚线表示碳 - 碳单键或碳 - 碳双键; 波浪线代表碳 - 碳单键或无键; 条件是：（a）至少三个虚线表示碳 - 碳单键; （b）当R7不是部分时，“1-6”位的虚线是碳 - 碳双键; （c）当波浪线为碳 - 碳单键时，R 5为亚甲基，“4-5”位和“5-6”位的碳 - 碳键为碳 - 碳单键; 以及其用于增强或增强香料组合物，古龙水和香料制品如芳香或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂，织物柔软剂制品，喷发剂，洗发剂，浴油和加香聚合物的香气。

3. 发明授权

US5039659A 2,2,3-trimethylcyclopentenyl acetone derivatives, organoleptic uses thereof and process for preparing same 失效
标题翻译： 2,2,3-三甲基环戊烯基丙酮衍生物，其感官用途及其制备方法
公开(公告)号：US5039659A
公开(公告)日：1991-08-13
申请号：US563607
申请日：1990-08-07
申请人： Anubhav P. S. Narula , John J. De Virgilio , Vincent F. Kuczinski , Anton V. Ouwerkerk , Charles E. J. Beck , Kathleen E. Boardwick , Marie R. Hanna
发明人： Anubhav P. S. Narula , John J. De Virgilio , Vincent F. Kuczinski , Anton V. Ouwerkerk , Charles E. J. Beck , Kathleen E. Boardwick , Marie R. Hanna
IPC分类号： C07C43/303 , C07C45/00 , C07C45/51 , C07C49/21 , C11B9/00 , C11D3/50
CPC分类号： C11D3/50 , C07C43/303 , C07C45/00 , C07C45/515 , C07C49/21 , C11B9/003 , C07C2101/10
摘要： Described are 2,2,3-trimethylcyclopentenyl acetone derivatives defined according to one or a mixture of compounds having the structures: ##STR1## organoleptic uses thereof, processes for preparing same using as a starting material the compound having the structure: ##STR2## which is reacted to form the compound having the structure: ##STR3## which is further reacted to form the novel intermediate: ##STR4## which is then converted to the 2,2,3-trimethylcyclopentenyl acetone derivatives or our invention using the allylic alcohol having the structure: ##STR5## wherein R.sub.3, R.sub.4, and R.sub.5 are the same or different hydrogen or methyl; R.sub.6 represents hydrogen, methyl, ethyl, or propyl or isopropyl; x is 0, 1 or 2; R.sub.7 is methyl or ethyl; R.sub.7 ' and R.sub.7 " represent methyl or ethyl or R.sub.7 ', (CH.sub.2).sub.x and R.sub.7 " taken together represents C.sub.2 -C.sub.6 alkylene; M represents Li, Mg, X or MgX; and X represents chloro or bromo.

4. 发明授权

US5087707A Substituted cyclopentenyl-oxabicyclooctanes, cyclopentenyl-formylcyclohexenes and cyclopentenyl-hydroxymethyl cyclohexenes, processes for preparing same and organoleptic uses thereof 失效
标题翻译：取代的环戊烯基 - 氧杂双环辛烷，环戊烯基 - 甲酰基环己烯和环戊烯基 - 羟甲基环己烯，其制备方法和感官用途
公开(公告)号：US5087707A
公开(公告)日：1992-02-11
申请号：US683618
申请日：1991-04-11
申请人： Anubhav P. S. Narula , John J. De Virgilio , Carlos Benaim , Anton V. Ouwerkerk , Olivier Gillotin
发明人： Anubhav P. S. Narula , John J. De Virgilio , Carlos Benaim , Anton V. Ouwerkerk , Olivier Gillotin
IPC分类号： C07C29/14 , C07C33/14 , C07C45/69 , C07C45/75 , C07C47/225 , C07C47/44 , C07D493/08 , C11B9/00 , C11D3/50
CPC分类号： C11D3/50 , C07C29/14 , C07C33/14 , C07C45/69 , C07C45/75 , C07C47/225 , C07C47/44 , C07D493/08 , C11B9/003 , C11B9/0034 , C11B9/0076 , C07C2101/10 , C07C2101/16
摘要： Described are cyclopentenyl-oxabicyclooctanes, cyclopentenyl-formylcyclohexenes and cyclopentylhydroxymethyl cyclohexenes having the generic structures: ##STR1## wherein R.sub.1, R.sub.2, R.sub.3 ', and R.sub.3 " each represents hydrogen or methyl with the provisos:(i) one or two or R.sub.1, R.sub.2, R.sub.3 ' and R.sub.3 " represents methyl;(ii) R.sub.1 and/or R.sub.2 are methyl;(iii) at least one of R.sub.3 ' and R.sub.3 " is hydrogen; and(iv) when R.sub.1 and R.sub.2 is methyl then each of R.sub.3 ' and R.sub.3 " is hydrogenwherein R.sub.4 ' is hydrogen or C.sub.1 -C.sub.5 alkyl, processes for preparing same and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles, e.g., solid or liquid, anionic, cationic, nonionic or zwitterionic detergents, cosmetic preparations, fabric softener compositions, fabric softener articles, hair preparations and perfumed polymers.
摘要翻译：描述的是具有通用结构的环戊烯基 - 氧杂双环辛烷，环戊烯基 - 甲酰基环己烯和环戊基羟甲基环己烯：其中R 1，R 2，R 3'和R 3“各自表示氢或甲基，条件是：（i）一个或两个或R 1，R 2，R 3'和R 3“表示甲基; （ii）R 1和/或R 2为甲基; （iii）R 3'和R 3“中的至少一个是氢; 和（iv）当R 1和R 2为甲基时，R 3'和R 3“中的每一个为氢，其中R 4'为氢或C 1 -C 5烷基，其制备方法及其用于增强或增强香料组合物香气，古龙香和香料制品，例如固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，化妆品制剂，织物柔软剂组合物，织物柔软剂制品，毛发制品和加香聚合物。

5. 发明授权

US5070073A Substituted cyclopentenyl-oxabicyclooctanes, cyclopentenyl-formylcyclohexenes and cyclopentenyl-hydroxymethyl cyclohexenes, processes for preparing same and organoleptic uses thereof 失效
标题翻译：取代的环戊烯基 - 氧杂双环辛烷，环戊烯基 - 甲酰基环己烯和环戊烯基 - 羟甲基环己烯，其制备方法和感官用途
公开(公告)号：US5070073A
公开(公告)日：1991-12-03
申请号：US684069
申请日：1991-04-11
申请人： Anubhav P. S. Narula , John J. De Virgilio , Carlos Benaim , Anton V. Ouwerkerk , Olivier Gillotin
发明人： Anubhav P. S. Narula , John J. De Virgilio , Carlos Benaim , Anton V. Ouwerkerk , Olivier Gillotin
IPC分类号： C07C29/14 , C07C33/14 , C07C45/69 , C07C45/75 , C07C47/225 , C07C47/44 , C07D493/08 , C11B9/00 , C11D3/50
CPC分类号： C07D493/08 , C07C29/14 , C07C33/14 , C07C45/69 , C07C45/75 , C07C47/225 , C07C47/44 , C11B9/003 , C11B9/0034 , C11B9/0076 , C11D3/50 , C07C2101/10 , C07C2101/16
摘要： Described are cyclopentenyl-oxabicyclooctanes, cyclopentenyl-formylcyclohexenes and cyclopentyl-hydroxymethyl cyclohexenes having the generic structures: ##STR1## wherein R.sub.1, R.sub.2, R.sub.3 ', and R.sub.3 " each represents hydrogen or methyl with the provisos:(i) one or two of R.sub.1, R.sub.2, R.sub.3 ' and R.sub.3 " represents methyl;(ii) R.sub.1 and/or R.sub.2 are methyl;(iii) at least one of R.sub.3 ' and R.sub.3 " is hydrogen; and(iv) when R.sub.1 and R.sub.2 is methyl then each of R.sub.3 ' and R.sub.3 " is hydrogenwherein R.sub.4 ' is hydrogen or C.sub.1 -C.sub.5 alkyl, processes for preparing same and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles, e.g., solid or liquid, anionic, cationic, nonionic or zwitterionic detergents, cosmetic preparations, fabric softener compositions, fabric softener articles, hair preparations and perfumed polymers.
摘要翻译：描述了具有以下通用结构的环戊烯基 - 氧杂双环辛烷，环戊烯基 - 甲酰基环己烯和环戊基 - 羟甲基环己烯：其中R 1，R 2，R 3'和R 3“各自表示氢或甲基与条件是：（i）R1，R2，R3'和R3“中的一个或两个表示甲基; （ii）R 1和/或R 2为甲基; （iii）R 3'和R 3“中的至少一个是氢; 和（iv）当R 1和R 2为甲基时，R 3'和R 3“中的每一个为氢，其中R 4'为氢或C 1 -C 5烷基，其制备方法及其用于增强或增强香料组合物香气，古龙香和香料制品，例如固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，化妆品制剂，织物柔软剂组合物，织物柔软剂制品，毛发制品和加香聚合物。

6. 发明授权

US4446125A Use of isomeric farnesene product-by-process for augmenting or enhancing the aroma or taste of foodstuffs, chewing gums, medicinal products and toothpastes 失效
标题翻译：使用异构法呢烯产品逐步增加或增强食品，口香糖，药用产品和牙膏的香气或味道
公开(公告)号：US4446125A
公开(公告)日：1984-05-01
申请号：US461476
申请日：1983-01-27
申请人： Braja D. Mookherjee , Robert W. Trenkle , Bernard J. Chant , Anton V. Ouwerkerk , Venkatesh Kamath , Cynthia J. Mussinan
发明人： Braja D. Mookherjee , Robert W. Trenkle , Bernard J. Chant , Anton V. Ouwerkerk , Venkatesh Kamath , Cynthia J. Mussinan
IPC分类号： C07C1/24 , C11B9/00 , A23L1/226
CPC分类号： C11B9/0007 , C07C1/24 , C07C2527/055
摘要： Described are isomeric mixtures of farnesene prepared by dehydrating nerolidol using potassium bisulfate or paratoluene sulfonic acid and then distilling the resultant product at particular temperature ranges and particular pressure ranges in order to prepare a composition of matter useful for augmenting or enhancing the fresh green, herbaceous aroma and taste nuances of foodstuffs, chewing gums, medicinal products and toothpastes.
摘要翻译：描述了通过使用硫酸氢钾或对甲苯磺酸脱水橙花叔醇制备的法呢烯异构体混合物，然后在特定温度范围和特定压力范围内蒸馏所得产物，以制备用于增强或增强新鲜绿色草本香气的物质组合物并品尝食品，口香糖，药用产品和牙膏的细微差别。

7. 发明授权

US4391717A Use of isomeric farnesene product-by-process for augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles 失效
标题翻译：使用异构法呢烯法逐步增加或增强香水组合物，古龙水和香水制品的香气
公开(公告)号：US4391717A
公开(公告)日：1983-07-05
申请号：US375534
申请日：1982-05-06
申请人： Braja D. Mookherjee , Robert W. Trenkle , Bernard J. Chant , Anton V. Ouwerkerk , Venkatesh Kamath , Cynthia J. Mussinan
发明人： Braja D. Mookherjee , Robert W. Trenkle , Bernard J. Chant , Anton V. Ouwerkerk , Venkatesh Kamath , Cynthia J. Mussinan
IPC分类号： C11B9/00 , D06M13/00 , D06M13/16
CPC分类号： C11B9/0007 , D06M13/005 , C07C2527/055 , Y10S428/905
摘要： Described are isomeric mixtures of farnesene prepared by dehydrating nerolidol using potassium bisulfate or paratoluene sulfonic acid and then distilling the resultant product at particular temperature ranges and particular pressure ranges in order to prepare a composition of matter useful for augmenting or enhancing waxy, white-flowery (magnolia-like, tuberose, gardenia-like) aromas with citrusy (lemon/lime), pettitgrain-like undertones and green top notes in perfume compositions, colognes and perfumed articles (e.g., solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, dryer-added fabric softener articles, cosmetic powders and the like).
摘要翻译：描述了通过使用硫酸氢钾或对甲苯磺酸脱水橙花叔醇制备的法呢烯的异构体混合物，然后在特定温度范围和特定压力范围内蒸馏所得产物，以制备用于增强或增强蜡质，白花（香柠檬，晚香玉，栀子花）芳香与柠檬/柠檬（柠檬/石灰），香草组合物，香水和香水制品（例如固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，干燥剂添加的织物柔软剂制品，化妆品粉末等）。

8. 发明授权

US4390444A Use of isomeric mixtures of farnesene for augmenting or enhancing the aroma of detergent compositions 失效
标题翻译：使用法呢烯的异构体混合物来增强或增强洗涤剂组合物的香气
公开(公告)号：US4390444A
公开(公告)日：1983-06-28
申请号：US375532
申请日：1982-05-06
申请人： Braja D. Mookherjee , Robert W. Trenkle , Bernard J. Chant , Anton V. Ouwerkerk , Venkatesh Kamath , Cynthia J. Mussinan
发明人： Braja D. Mookherjee , Robert W. Trenkle , Bernard J. Chant , Anton V. Ouwerkerk , Venkatesh Kamath , Cynthia J. Mussinan
IPC分类号： C11B9/00 , C11D3/50
CPC分类号： C11D3/50 , C11B9/0007 , C07C2527/055
摘要： Described are isomeric mixtures of farnesene prepared by dehydrating nerolidol using potassium bisulfate or paratoluene sulfonic acid and then distilling the resultant product at particular temperature ranges and particular pressure ranges in order to prepare a composition of matter useful for augmenting or enhancing waxy, white-flowery (magnolia-like, tuberose, gardenia-like) aromas with citrusy (lemon/lime), pettitgrain-like undertones and green top notes in perfume compositions, colognes and perfumed articles (e.g., solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, dryer-added fabric softener articles, cosmetic powders and the like).
摘要翻译：描述了通过使用硫酸氢钾或对甲苯磺酸脱水橙花叔醇制备的法呢烯的异构体混合物，然后在特定温度范围和特定压力范围内蒸馏所得产物，以制备用于增强或增强蜡质，白花（香柠檬，晚香玉，栀子花）芳香与柠檬/柠檬（柠檬/石灰），香草组合物，香水和香水制品（例如固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，干燥剂添加的织物柔软剂制品，化妆品粉末等）。

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