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1. 发明申请

US20110112348A1 PROCESS FOR MAKING STYRENE USING MIRCOHANNEL PROCESS TECHNOLOGY 审中-公开
标题翻译：使用MIRCOHANNEL工艺技术制造苯乙烯的方法
公开(公告)号：US20110112348A1
公开(公告)日：2011-05-12
申请号：US12958461
申请日：2010-12-02
申请人： Anna Lee Tonkovich , Kai Tod Paul Jarosch , Bin Yang , Francis P. Daly , Thomas P. Hickey , Jeffrey Marco , Timothy J. LaPlante , Richard Q. Long
发明人： Anna Lee Tonkovich , Kai Tod Paul Jarosch , Bin Yang , Francis P. Daly , Thomas P. Hickey , Jeffrey Marco , Timothy J. LaPlante , Richard Q. Long
IPC分类号： C07C5/367 , B01J19/00 , C07C5/333
CPC分类号： B01J19/0093 , B01F5/0475 , B01F5/0478 , B01F5/0483 , B01F5/061 , B01F5/0646 , B01F5/0655 , B01F13/0059 , B01F2005/0621 , B01F2005/0636 , B01F2215/0036 , B01J2219/00783 , B01J2219/00804 , B01J2219/0081 , B01J2219/00822 , B01J2219/00824 , B01J2219/00826 , B01J2219/00828 , B01J2219/00831 , B01J2219/00833 , B01J2219/00835 , B01J2219/00844 , B01J2219/0086 , B01J2219/00869 , B01J2219/00873 , B01J2219/00876 , B01J2219/00878 , B01J2219/00889 , B01J2219/00891 , C07C2/66 , C07C5/277 , C07C5/3332 , C07C5/48 , C07C15/46 , C07C2521/02 , C07C2521/06 , C07C2521/08 , C07C2521/10 , C07C2523/02 , C07C2523/04 , C07C2523/10 , C07C2523/18 , C07C2523/22 , C07C2523/26 , C07C2523/28 , C07C2523/30 , C07C2523/42 , C07C2523/44 , C07C2523/46 , C07C2523/745 , C07C2523/847 , C07C2523/881 , C07C2523/883 , C07C2523/888 , C07C2527/167 , F28D9/00 , F28F3/048 , F28F3/086 , F28F13/12 , F28F21/04 , F28F21/081 , F28F2260/02 , F28F2270/00 , Y02P20/52 , Y02P20/582 , Y10S585/921 , C07C15/073 , C07C11/04
摘要： The disclosed invention relates to a process for converting ethylbenzene to styrene, comprising: flowing a feed composition comprising ethylbenzene in at least one process microchannel in contact with at least one catalyst to dehydrogenate the ethylbenzene and form a product comprising styrene; exchanging heat between the process microchannel and at least one heat exchange channel in thermal contact with the process microchannel; and removing product from the process microchannel. Also disclosed is an apparatus comprising a process microchannel, a heat exchange channel, and a heat transfer wall positioned between the process microchannel and heat exchange channel wherein the heat transfer wall comprises a thermal resistance layer.
摘要翻译：所公开的本发明涉及将乙苯转化为苯乙烯的方法，包括：使包含乙苯的进料组合物在至少一个与至少一种催化剂接触的工艺微通道中流动以使乙苯脱氢并形成包含苯乙烯的产物; 在工艺微通道和与工艺微通道热接触的至少一个热交换通道之间交换热量; 并从工艺微通道中除去产物。还公开了一种装置，其包括工艺微通道，热交换通道和位于工艺微通道和热交换通道之间的传热壁，其中传热壁包括热电阻层。

2. 发明授权

US07847138B2 Process for making styrene using mircochannel process technology 有权
标题翻译：使用微通道工艺技术制造苯乙烯的工艺
公开(公告)号：US07847138B2
公开(公告)日：2010-12-07
申请号：US11690319
申请日：2007-03-23
申请人： Anna Lee Tonkovich , Kai Tod Paul Jarosch , Bin Yang , Francis P. Daly , Thomas P. Hickey , Jeffrey Marco , Timothy J. LaPlante , Richard Q. Long
发明人： Anna Lee Tonkovich , Kai Tod Paul Jarosch , Bin Yang , Francis P. Daly , Thomas P. Hickey , Jeffrey Marco , Timothy J. LaPlante , Richard Q. Long
IPC分类号： C07C2/66 , C07C5/333
CPC分类号： B01J19/0093 , B01F5/0475 , B01F5/0478 , B01F5/0483 , B01F5/061 , B01F5/0646 , B01F5/0655 , B01F13/0059 , B01F2005/0621 , B01F2005/0636 , B01F2215/0036 , B01J2219/00783 , B01J2219/00804 , B01J2219/0081 , B01J2219/00822 , B01J2219/00824 , B01J2219/00826 , B01J2219/00828 , B01J2219/00831 , B01J2219/00833 , B01J2219/00835 , B01J2219/00844 , B01J2219/0086 , B01J2219/00869 , B01J2219/00873 , B01J2219/00876 , B01J2219/00878 , B01J2219/00889 , B01J2219/00891 , C07C2/66 , C07C5/277 , C07C5/3332 , C07C5/48 , C07C15/46 , C07C2521/02 , C07C2521/06 , C07C2521/08 , C07C2521/10 , C07C2523/02 , C07C2523/04 , C07C2523/10 , C07C2523/18 , C07C2523/22 , C07C2523/26 , C07C2523/28 , C07C2523/30 , C07C2523/42 , C07C2523/44 , C07C2523/46 , C07C2523/745 , C07C2523/847 , C07C2523/881 , C07C2523/883 , C07C2523/888 , C07C2527/167 , F28D9/00 , F28F3/048 , F28F3/086 , F28F13/12 , F28F21/04 , F28F21/081 , F28F2260/02 , F28F2270/00 , Y02P20/52 , Y02P20/582 , Y10S585/921 , C07C15/073 , C07C11/04
摘要： The disclosed invention relates to a process for converting ethylbenzene to styrene, comprising: flowing a feed composition comprising ethylbenzene in at least one process microchannel in contact with at least one catalyst to dehydrogenate the ethylbenzene and form a product comprising styrene; exchanging heat between the process microchannel and at least one heat exchange channel in thermal contact with the process microchannel; and removing product from the process microchannel. Also disclosed is an apparatus comprising a process microchannel, a heat exchange channel, and a heat transfer wall positioned between the process microchannel and heat exchange channel wherein the heat transfer wall comprises a thermal resistance layer.
摘要翻译：所公开的本发明涉及将乙苯转化为苯乙烯的方法，包括：使包含乙苯的进料组合物在至少一个与至少一种催化剂接触的工艺微通道中流动以使乙苯脱氢并形成包含苯乙烯的产物; 在工艺微通道和与工艺微通道热接触的至少一个热交换通道之间交换热量; 并从工艺微通道中除去产物。还公开了一种装置，其包括工艺微通道，热交换通道和位于工艺微通道和热交换通道之间的传热壁，其中传热壁包括热电阻层。

3. 发明授权

US09150494B2 Process using microchannel technology for conducting alkylation or acylation reaction 有权
标题翻译：使用微通道技术进行烷基化或酰化反应的方法
公开(公告)号：US09150494B2
公开(公告)日：2015-10-06
申请号：US11271154
申请日：2005-11-11
申请人： Anna Lee Tonkovich , Steven T. Perry , Timothy J. LaPlante , Kai Tod Paul Jarosch , Thomas P. Hickey , Sean Patrick Fitzgerald , Dongming Qiu , Ravi Arora , Timothy J. Sullivan , Paul Neagle
发明人： Anna Lee Tonkovich , Steven T. Perry , Timothy J. LaPlante , Kai Tod Paul Jarosch , Thomas P. Hickey , Sean Patrick Fitzgerald , Dongming Qiu , Ravi Arora , Timothy J. Sullivan , Paul Neagle
IPC分类号： C07C2/56 , C07C209/68 , B01F5/04 , B01F13/00 , B01J19/00 , C07C2/66 , C07C2/70 , C07C37/14 , B01J29/40 , B01J37/02 , B01J38/10
CPC分类号： C07C209/68 , B01F5/0475 , B01F13/0059 , B01J19/0093 , B01J29/40 , B01J37/0225 , B01J38/10 , B01J2219/00783 , B01J2219/00822 , B01J2219/00826 , B01J2219/00828 , B01J2219/00831 , B01J2219/00833 , B01J2219/00835 , B01J2219/00837 , B01J2219/00844 , B01J2219/0086 , B01J2219/00873 , B01J2219/00889 , B01J2219/00891 , B01J2219/00905 , C07C2/66 , C07C2/70 , C07C37/14 , C07C2529/40 , Y02P20/582 , Y02P20/584 , C07C15/073 , C07C211/46 , C07C211/47 , C07C211/50 , C07C211/51 , C07C39/06 , C07C39/07
摘要： The disclosed invention relates to a process, comprising: flowing a first reactant feed stream comprising a reactant substrate and a second reactant feed stream comprising an alkylating agent, an acylating agent or a mixture thereof, in a process microchannel in contact with each other to form a product comprising at least one alkylation product, at least one acylation product, or a mixture thereof; transferring heat from the process microchannel to a heat sink; and removing the product from the process microchannel.
摘要翻译：所公开的发明涉及一种方法，其包括：将包含反应物底物的第一反应物进料流和包含烷基化试剂，酰化剂或其混合物的第二反应物进料流在彼此接触的工艺微通道中流动以形成包含至少一种烷基化产物，至少一种酰化产物或其混合物的产品; 将热量从工艺微通道转移到散热器; 并从工艺微通道中除去产品。

4. 发明申请

US20100071410A1 DISTILLATION PROCESS USING MICROCHANNEL TECHNOLOGY 审中-公开
标题翻译：使用微通道技术的蒸馏工艺
公开(公告)号：US20100071410A1
公开(公告)日：2010-03-25
申请号：US12611427
申请日：2009-11-03
申请人： Anna Lee Tonkovich , Wayne W. Simmons , Laura J. Silva , Dongming Qiu , Steven J. Perry , Thomas Yuschak , Thomas P. Hickey , Ravi Arora , Amanda Smith , Robert Dwayne Litt , Paul Neagle
发明人： Anna Lee Tonkovich , Wayne W. Simmons , Laura J. Silva , Dongming Qiu , Steven J. Perry , Thomas Yuschak , Thomas P. Hickey , Ravi Arora , Amanda Smith , Robert Dwayne Litt , Paul Neagle
IPC分类号： F25J3/00
CPC分类号： F25J3/04896 , B01D3/146 , C07C7/04 , F25J3/0209 , F25J3/0219 , F25J3/0233 , F25J3/0238 , F25J3/0242 , F25J3/0247 , F25J3/0295 , F25J3/04624 , F25J3/04975 , F25J5/007 , F25J2200/80 , F25J2200/90 , F25J2210/12 , F25J2215/62 , F25J2270/90 , F25J2290/20 , F25J2290/42 , F25J2290/44 , Y10S62/902 , C07C11/02 , C07C9/04
摘要： The disclosed invention relates to a distillation process for separating two or more components having different volatilities from a liquid mixture containing the components. The process employs microchannel technology for effecting the distillation and is particularly suitable for conducting difficult separations, such as the separation of ethane from ethylene, wherein the individual components are characterized by having volatilities that are very close to one another.
摘要翻译：所公开的发明涉及用于从含有这些组分的液体混合物中分离具有不同挥发性的两种或更多种组分的蒸馏方法。该方法采用微通道技术进行蒸馏，特别适用于进行困难的分离，例如从乙烯中分离乙烷，其中各组分的特征在于彼此非常接近的挥发性。

5. 发明授权

US07610775B2 Distillation process using microchannel technology 有权
标题翻译：蒸馏工艺采用微通道技术
公开(公告)号：US07610775B2
公开(公告)日：2009-11-03
申请号：US11177941
申请日：2005-07-08
申请人： Anna Lee Tonkovich , Wayne W. Simmons , Laura J. Silva , Dongming Qiu , Steven T. Perry , Thomas Yuschak , Thomas P. Hickey , Ravi Arora , Amanda Smith , Robert Dwayne Litt , Paul Neagle
发明人： Anna Lee Tonkovich , Wayne W. Simmons , Laura J. Silva , Dongming Qiu , Steven T. Perry , Thomas Yuschak , Thomas P. Hickey , Ravi Arora , Amanda Smith , Robert Dwayne Litt , Paul Neagle
IPC分类号： F25J3/00
CPC分类号： F25J3/0209 , B01D3/146 , F25J3/0219 , F25J3/0233 , F25J3/0238 , F25J3/0242 , F25J3/0247 , F25J3/0295 , F25J3/04624 , F25J3/04896 , F25J3/04975 , F25J5/007 , F25J2200/80 , F25J2200/90 , F25J2210/12 , F25J2215/62 , F25J2270/90 , F25J2290/20 , F25J2290/44 , Y10S62/902
摘要： The disclosed invention relates to a distillation process for separating two or more components having different volatilities from a liquid mixture containing the components. The process employs microchannel technology for effecting the distillation and is particularly suitable for conducting difficult separations, such as the separation of ethane from ethylene, wherein the individual components are characterized by having volatilities that are very close to one another.
摘要翻译：所公开的发明涉及用于从含有这些组分的液体混合物中分离具有不同挥发性的两种或更多种组分的蒸馏方法。该方法采用微通道技术进行蒸馏，特别适用于进行困难的分离，例如从乙烯中分离乙烷，其中各组分的特征在于彼此非常接近的挥发性。

6. 发明授权

US5925685A Method for carrying out heterogeneous catalysis 失效
标题翻译：进行非均相催化的方法
公开(公告)号：US5925685A
公开(公告)日：1999-07-20
申请号：US943212
申请日：1997-10-06
申请人： John R. Adams , Thomas P. Hickey
发明人： John R. Adams , Thomas P. Hickey
IPC分类号： B01J8/22 , B01D3/00 , B01J8/02 , B01J10/00 , C07B61/00 , C07C27/06 , C07C29/151 , C07C29/152 , C07C29/80 , C07C31/04 , C07C27/00 , B01J8/04
CPC分类号： C07C29/1512 , B01D3/009 , B01J8/0242 , B01J2208/00274 , B01J2208/00283 , Y02P20/127
摘要： Catalytic distillation reactions are improved by having an inert condensing component present in the reaction which is boiling and condensing within the reaction which washes the catalyst in the system and, in the case of gaseous reactants, occludes a portion of the reactants to facilitate the reaction without unduly high pressures. The inert condensing component is boiling at the conditions within the reactor and is taken overhead for condensation and return as reflux. The inert condensing component may occlude the gaseous reactants allowing for better contact with the catalyst and provides the benefits of concurrent reaction and distillation, for example, the reaction of CO and H.sub.2 over a copper catalyst to produce methanol using propane as the inert condensing component.
摘要翻译：催化蒸馏反应通过在反应中存在的惰性缩合组分得到改善，该反应在反应中沸腾和冷凝，其在系统中洗涤催化剂，并且在气态反应物的情况下，封闭一部分反应物以促进反应而没有压力过高惰性冷凝组分在反应器内的条件下沸腾，并在塔顶馏去冷凝并作为回流返回。惰性冷凝组分可以堵塞气态反应物，从而允许更好地与催化剂接触，并且提供同时反应和蒸馏的优点，例如CO和H 2在铜催化剂上的反应，以使用丙烷作为惰性冷凝组分来生产甲醇。

7. 发明授权

US5961815A Hydroconversion process 失效
标题翻译：加氢转化过程
公开(公告)号：US5961815A
公开(公告)日：1999-10-05
申请号：US717935
申请日：1996-09-23
申请人： Thomas P. Hickey , Dennis Hearn , Hugh M. Putman
发明人： Thomas P. Hickey , Dennis Hearn , Hugh M. Putman
IPC分类号： B01J23/85 , B01D3/00 , B01J8/02 , B01J23/88 , C10G45/00 , C10G47/00 , C10G47/02 , C10G11/02 , C10G29/04
CPC分类号： B01D3/009 , C10G47/00
摘要： The hydroconversion of heavy petroliferous stocks boiling mainly above 400.degree. F. is carried out in a distillation column reactor where concurrently a petroleum stream is fed into a feed zone; hydrogen is fed at a point below said feed zone; the petroleum stream is distilled and contacted in the presence of a cracking catalyst prepared in the form of a catalytic distillation structure at total pressure of less than about 300 psig and a hydrogen partial pressure in the range of 1.0 to less than 70 psia and a temperature in the range of 400 to 1000.degree. F. whereby a portion of the petroleum stream is cracked to lighter products boiling below the boiling point of the feed and products are distilled to remove a vaporous overhead stream comprising products mainly boiling below the boiling point of the feed and a liquid bottoms stream.
摘要翻译：主要在400°F以上沸腾的重质含油量的加氢转化在蒸馏塔反应器中进行，同时将石油流进料到进料区; 氢在所述进料区下方的一点进料; 在催化蒸馏结构形式的裂化催化剂存在下蒸馏并接触石油物流，其总压力小于约300psig，氢分压为1.0至小于70psia，温度为在400至1000°F的范围内，由此一部分石油流裂化成低于进料沸点沸点的较轻的产物，并将产物蒸馏以除去蒸气塔顶物流，其包含主要沸点低于饲料和液体底部物流。

8. 发明授权

US5919989A Etherification process 失效
标题翻译：醚化过程
公开(公告)号：US5919989A
公开(公告)日：1999-07-06
申请号：US880145
申请日：1997-06-20
申请人： Amarjit Bakshi , Thomas P. Hickey
发明人： Amarjit Bakshi , Thomas P. Hickey
IPC分类号： C07C41/06 , C07C41/42 , C07C41/00
CPC分类号： C07C41/42 , C07C41/06 , Y02P20/127
摘要： The overheads from an etherification distillation column reactor containing unreacted alcohol and isoolefin are fed to a finishing reactor and then a portion of the effluent from the finishing reactor is returned to the distillation column reactor.
摘要翻译：将含有未反应的醇和异烯烃的醚化蒸馏塔反应器的塔顶馏出物加入到精制反应器中，然后将来自精制反应器的一部分流出物返回到蒸馏塔反应器。

9. 发明授权

US5421972A Process and apparatus for removing soluble contaminants from hydrocarbon streams 失效
标题翻译：从烃流中除去可溶性污染物的方法和设备
公开(公告)号：US5421972A
公开(公告)日：1995-06-06
申请号：US263264
申请日：1994-06-21
申请人： Thomas P. Hickey , John J. Byeseda
发明人： Thomas P. Hickey , John J. Byeseda
IPC分类号： B01D11/04 , C07C7/00 , C10G31/08 , C10G32/02 , B01D17/06
CPC分类号： C07C7/00 , B01D11/0419 , C10G31/08 , C10G32/02
摘要： A method for removing soluble contaminants, such as acetonitrile, from a non-polar hydrocarbon stream into a polar water stream by countercurrent flow between an electrostatic field generated by a pair of parallel electrodes. The electrostatic field is modulated in strength to produce a dispersing, mixing, coalescing, and settling cycle that is effective to mix and separate the fluids.
摘要翻译：一种通过在由一对平行电极产生的静电场之间的逆流来将可溶性污染物例如乙腈从非极性烃流中分离成极性水流的方法。静电场被强度调制以产生有效混合和分离流体的分散，混合，聚结和沉降循环。

10. 发明授权

US5321163A Multi-purpose catalytic distillation column and eterification process using same 失效
标题翻译：多用途催化蒸馏塔及其使用方法
公开(公告)号：US5321163A
公开(公告)日：1994-06-14
申请号：US118311
申请日：1993-09-09
申请人： Thomas P. Hickey , John R. Adams
发明人： Thomas P. Hickey , John R. Adams
IPC分类号： B01D3/16 , B01D3/00 , B01D3/14 , B01J8/04 , B01J23/44 , B01J35/02 , B01J35/04 , C07C41/06 , C07C41/42 , C07C43/04 , C07C319/16 , C07C323/27
CPC分类号： C07C41/06 , B01D3/009 , C07C319/16 , C07C41/42 , Y02P20/127 , Y10S203/06
摘要： A multi-purpose distillation column reactor is disclosed which may be used for the production of tertiary amyl methyl ether from the reaction of the isoamylenes contained in a light naphtha with methanol. Two reaction distillation zones are disposed above a stripping section. The stripping, in addition to removing the TAME product, also removes the C.sub.6 and heavier components. The first reaction distillation zone contains a hydrotreating catalyst for removing diolefins and mercaptans. The second distillation reaction zone contains an acid cation exchange resin for the etherification reaction and the entire column serves to fractionate the multiple component reaction system (reacts, inerts, products and contaminants) concurrently with the multiple reactions.
摘要翻译：公开了一种多用途蒸馏塔反应器，其可用于从轻石脑油中含有的异戊烯与甲醇的反应生产叔戊基甲基醚。两个反应蒸馏区设置在汽提段上方。除了除去TAME产品之外，汽提也可以除去C6和较重的组分。第一反应蒸馏区含有用于除去二烯烃和硫醇的加氢处理催化剂。第二蒸馏反应区包含用于醚化反应的酸性阳离子交换树脂，并且整个塔用于与多重反应同时分馏多组分反应体系（反应，惰性，产物和污染物）。

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