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1. 发明授权

US4622390A Water-soluble disazo compounds containing an amino naphthol-disulfonic acid moiety as a coupling component and fibre-reactive groups 失效
标题翻译：含有氨基萘酚 - 二磺酸部分作为偶联成分的水溶性双偶氮化合物和纤维反应性基团
公开(公告)号：US4622390A
公开(公告)日：1986-11-11
申请号：US774171
申请日：1985-09-09
申请人： Fritz Meininger , Ernst Hoyer , Joachim W. Otten, deceased , by Ursula Otten, heir , by Anna G. Rudolph nee Otten, heir , Rudolf Fass
发明人： Fritz Meininger , Ernst Hoyer , Joachim W. Otten, deceased , by Ursula Otten, heir , by Anna G. Rudolph nee Otten, heir , Rudolf Fass
IPC分类号： C09B62/513 , C09B62/09 , C09B62/44 , D06P1/38 , C09B62/453 , C09B62/533 , D06P1/382
CPC分类号： C09B62/09 , C09B62/4415
摘要： Water-soluble disazo dyestuffs of the formula ##STR1## which contain a 1-amino-8-naphthol-3,6- or -4,6-disulfonic acid moiety as a bivalent coupling component and which contain diazo components with fibre-reactive groups characterized by the inclusion of one or two chloro-triazinyl groups and one or two of the six groups defined by the substituent Z, namely, ##STR2## each of which are connected to the benzene moiety of the diazo component; the chloro-triazinyl group is further substituted by a substituted or unsubstituted phenylamino or substituted or unsubstituted naphthylamino group, a substitutent of which may be one of the six groups defined by the Z substituent; if there is only one chloro-triazinyl group in the compound, then the diazo component is also substituted by one of the Z substituents; these compounds are dyestuffs which exhibit a good fixation degree of the dyestuffs in fabrics.
摘要翻译：含有作为二价偶联组分的1-氨基-8-萘酚-3,6-或-4,6-二磺酸部分并含有具有纤维反应性基团的重氮组分的式“IMAGE”的水溶性双偶氮染料其特征在于包含一个或两个氯 - 三嗪基和由取代基Z限定的六个基团中的一个或两个，即，＆lt; IMAGE＆gt; CH2SO2CH2CH2OSO3H; SO2CHCH2; + TR＆lt; IMAGE＆gt;各自与重氮组分的苯部分相连; 氯代三嗪基进一步被取代或未取代的苯基氨基或取代或未取代的萘基氨基取代，其取代基可以是由Z取代基限定的六个基团之一; 如果化合物中只有一个氯三嗪基，则重氮组分也被Z取代基之一取代; 这些化合物是在织物中表现出良好的染料固着度的染料。

2. 发明授权

US4649193A Water-soluble dyestuffs containing fibre-reactive groups of the vinylsulfone series and the fluoro-s-triazinyl-amino series 失效
标题翻译：含有乙烯基砜系列的纤维反应性基团和氟代-s-三嗪基 - 氨基系列的水溶性染料
公开(公告)号：US4649193A
公开(公告)日：1987-03-10
申请号：US519211
申请日：1983-08-01
申请人： Fritz Meininger , Joachim W. Otten, deceased , by Ursula Otten, heir , by Anna G. Rudolph nee Otten, heir
发明人： Fritz Meininger , Joachim W. Otten, deceased , by Ursula Otten, heir , by Anna G. Rudolph nee Otten, heir
IPC分类号： C09B62/503 , C09B62/44 , D06P1/384 , C09B62/06 , C09B62/085 , C09B62/095 , C09B62/10
CPC分类号： C09B62/4403
摘要： Water-soluble fibre-reactive dyestuffs containing one or two fibre-reactive groups of the vinylsulfone series and one or two fibre-reactive groups of the fluoro-s-triazinyl-amino series. These dyestuffs can be applied on fibre materials containing hydroxy and/or carbonamide groups by known application and fixation techniques for fibre-reactive dyes to yield deep and fast dyeings on these materials.
摘要翻译：含有一个或两个乙烯基砜系列的纤维反应性基团和氟代-s-三嗪基 - 氨基系列的一个或两个纤维反应性基团的水溶性纤维活性染料。这些染料可以通过纤维活性染料的已知应用和固色技术应用于含有羟基和/或碳酰胺基团的纤维材料上，以在这些材料上产生深色和快速的染色。

3. 发明授权

US4515598A Process for dyeing and printing fiber materials containing hydroxy and/or carbonamide groups with reactive dye containing both vinyl sulphonyl and fluoro-triazinyl groups 失效
标题翻译：含有羟基和/或碳酰胺基团的含有乙烯基磺酰基和氟 - 三嗪基的活性染料的纤维材料的染色和印花方法
公开(公告)号：US4515598A
公开(公告)日：1985-05-07
申请号：US550727
申请日：1983-11-10
申请人： Fritz Meininger , Joachim W. Otten, deceased , by Ursula Otten, heir , by Anna G. Rudolph nee Otten, heir
发明人： Fritz Meininger , Joachim W. Otten, deceased , by Ursula Otten, heir , by Anna G. Rudolph nee Otten, heir
IPC分类号： C09B62/503 , C09B62/44 , C09B62/507 , D06P1/38 , D06P1/384 , C09B62/04 , D06P3/66
CPC分类号： C09B62/4403 , D06P1/38 , Y10S8/917 , Y10S8/918 , Y10S8/924
摘要： A process for dyeing or printing fiber materials containing hydroxy and/or carbonamide groups, in which process a fiber-reactive, water-soluble dyestuff of the type defined below is applied to the fiber material and is then fixed on the fiber material at an ordinary or elevated temperature, if appropriate in the presence of agents having an alkaline reaction. This water-soluble dyestuff, which contains at least one sulfonic acid group, contains one or more groupings belonging to the group comprising the formulae (1a), (1b) and (1c)--SO.sub.2 --CH.dbd.CH.sub.2 (1a)--SO.sub.2 --CH.sub.2 --CH.sub.2 --Hal (1b)--SO.sub.2 --CH.sub.2 --CH.sub.2 --A (1c)(in which Hal represents a halogen atom and A represents the acyloxy radical of a monobasic or polybasic acid) and also contains, linked to it, a 6-fluoro-1,3,5-triazin-2-ylamino radical, this monofluorotriazinylamino radical containing, in the 4-position, a substituent which is not an N-phenylamino or N-naphthylamino substituent having a group belonging to the above-mentioned formulae (1) attached to the optionally substituted phenyl radical or optionally substituted naphthyl radical, and is also not an amino substituent containing an azo group. Dyestuffs of this type can belong to a very wide variety of classes of dyestuffs and can be both metal-free dyestuffs and metal complex dyestuffs. With the aid of these dyestuffs and using alkaline agents, this dyeing process produces deep dyeings and prints which have good fastness properties on these fiber materials, even at low temperatures.
摘要翻译：一种用于染色或印刷含有羟基和/或碳酰胺基团的纤维材料的方法，其中将下文定义的纤维反应性水溶性染料施用于纤维材料，然后以普通的方式固定在纤维材料上或升高的温度，如果适当，在具有碱性反应的试剂的存在下。这种含有至少一个磺酸基的水溶性染料含有属于由式（1a），（1b）和（1c）组成的基团的一个或多个基团-SO 2 -CH = CH 2（1a）-SO 2 - CH 2 -CH 2 - Hal（1b）-SO 2 -CH 2 -CH 2 -A（1c）（其中Hal表示卤素原子，A表示一元酸或多元酸的酰氧基），并且还含有6个 - 氟-1,3,5-三嗪-2-基氨基，该单氟三嗪基氨基在4-位含有不是具有属于上述的基团的N-苯基氨基或N-萘基氨基取代基的取代基连接到任选取代的苯基或任选取代的萘基的式（1），并且也不是含有偶氮基的氨基取代基。这种类型的染料可以属于各种各样的染料，并且可以是无金属染料和金属络合染料。借助这些染料和使用碱性剂，这种染色方法即使在低温下也能在这些纤维材料上产生深色染色和印花，这些染色和印花具有良好的坚牢度。

4. 发明授权

US4361698A Process for the manufacture of dihalogenotriazinylamino-naphthol compounds 失效
标题翻译：制备二卤代三嗪基氨基 - 萘酚化合物的方法
公开(公告)号：US4361698A
公开(公告)日：1982-11-30
申请号：US244612
申请日：1981-03-17
申请人： Joachim W. Otten, deceased , by Ursula Otten, heir , by Anna G. Rudolph nee Otten, heir , by Fritz Meininger
发明人： Joachim W. Otten, deceased , by Ursula Otten, heir , by Anna G. Rudolph nee Otten, heir , by Fritz Meininger
IPC分类号： C07D251/44 , C09B62/04 , C09B62/51
CPC分类号： C09B62/04 , C07D251/44
摘要： Dihalogenotriazinylamino-naphthol compounds of th formula (1) ##STR1## in which the radicals X each mean fluorine, chlorine or bromine, R is hydrogen or alkyl of 1 to 4 C-atoms, M is hydrogen or the equivalent of a metal, and Z is hydrogen or a group of the formula --SO.sub.3 M with M having the abovementioned meaning, are prepared in water as reaction medium by reaction of an aminonaphthol compound of the formula (2) ##STR2## in which R, M and Z have the abovementioned meanings with a cyanuric halide compound of the formula (3) ##STR3## in which the radicals X have the abovementioned meanings, at pH 5 or smaller than 5 by introducing the aminonaphthol compound of the formula (2) in solid, undissolved form into the reaction, and carrying out the reaction in suspension.
摘要翻译：式（1）的二卤代三嗪基氨基 - 萘酚化合物其中基团X各自表示氟，氯或溴，R是氢或1-4个C原子的烷基，M是氢或相当于金属，Z是氢或具有上述含义的M的具有式-SO 3 M的基团，通过式（2）的氨基萘酚化合物（2）制备在水中作为反应介质，其中R， M和Z具有上述含义，其中基团X具有上述含义的通式（3）的三聚氰化物化合物，其中基团X具有上述含义，在pH5或小于5的情况下，通过引入下式的氨基萘酚化合物（ 2）以固体，未溶解的形式进入反应，并进行悬浮反应。

5. 发明授权

US4442288A Anthraquinone compounds 失效
标题翻译：蒽醌化合物
公开(公告)号：US4442288A
公开(公告)日：1984-04-10
申请号：US373789
申请日：1982-04-30
申请人： Fritz Meininger , Joachim W. Otten, deceased , by Ursla Otten, heir , by Anna G. Rudolph, heir
发明人： Fritz Meininger , Joachim W. Otten, deceased , by Ursla Otten, heir , by Anna G. Rudolph, heir
IPC分类号： C09B62/505 , C07D251/50 , C09B62/44
CPC分类号： C09B62/4409
摘要： Water-soluble anthraquinone compounds of the formula (1) ##STR1## wherein M is a hydrogen atom or the equivalent of a metal, such as in particular sodium or potassium, R is a hydrogen atom, a halogen atom, the methyl, ethyl, methoxy, ethoxy or carboxy group, and X is the vinyl group, a .beta.-thiosulfatoethyl, .beta.-sulfatoethyl or the .beta.-chloroethyl group. These compounds may be prepared in a manner know by itself by reacting an anthraquinone compound of the formula (2) ##STR2## wherein M is defined as above, with an equimolar quantity of cyanuric chloride and an amine of the formula (4) ##STR3## wherein R and X are defined as above, or by reacting said anthraquinone compound of the formula (2) with a compound of the formula (5) ##STR4## wherein R and X are defined as above. The new compounds of the formula (1) are valuable dyestuffs having fiber-reactive properties. When applied to materials containing hydroxy and/or carbonamide groups, preferably fiber materials, these dyestuffs yield strong and fast dyeings and prints or high tinctorial strength; for example, they are particularly suitable for dyeing (and printing) cellulose fiber materials and wool having an anti-felt or a felt-reducing finish.
摘要翻译：式（1）的水溶性蒽醌化合物其中M为氢原子或金属当量，特别是钠或钾，R为氢原子，卤素原子，甲基乙基，甲氧基，乙氧基或羧基，X是乙烯基，β-硫代硫代乙基，β-磺基乙基或β-氯乙基。这些化合物可以通过使式（2）的蒽醌化合物（2）其中M如上所定义的蒽醌化合物与等摩尔量的氰尿酰氯和式（4）的胺反应而自己已知的方式制备（4）其中R和X如上定义，或通过使式（2）的所述蒽醌化合物与式（5）化合物反应其中R和X定义为以上。式（1）的新化合物是具有纤维反应性质的有价值的染料。当应用于含有羟基和/或碳酰胺基团的材料时，优选纤维材料，这些染料产生强烈和快速的染色和印花或高着色强度; 例如，它们特别适合用于染色（和印花）纤维素纤维材料和具有抗毛毡或毛毡减少处理的羊毛。

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