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1. 发明授权

US08618199B2 Functionalized high cis-1,4-polybutadiene prepared using novel functionalizing agents 有权
公开(公告)号：US08618199B2
公开(公告)日：2013-12-31
申请号：US13711701
申请日：2012-12-12
申请人： Yoichi F. Ozawa , H. Jerrold Miller , Koji Masaki , Koichi Morita , Tatsuo Fujimaki , Tetsuya Omura , Takuo Sone , Iwakazu Hattori
发明人： Yoichi F. Ozawa , H. Jerrold Miller , Koji Masaki , Koichi Morita , Tatsuo Fujimaki , Tetsuya Omura , Takuo Sone , Iwakazu Hattori
IPC分类号： C08K5/13 , C08C19/22
CPC分类号： C08F136/14 , C08C19/00 , C08C19/22 , C08C19/44 , C08F36/04 , C08F136/06 , C08K3/04 , C08K3/045 , C08K3/36 , C08L21/00 , C08L91/00 , C08F4/545 , C08L15/00
摘要： A method for preparing a functionalized polymer comprising the steps of preparing a polymer by polymerizing conjugated diene monomer with a lanthanide-based catalyst, wherein the lanthanide-based catalyst comprises (a) a lanthanide compound, (b) an alkylating agent, and (c) a source of halogen, and reacting the pseudo-living polymer with at least one amide-containing functionalizing agent.

2. 发明申请

US20120131847A1 Low sulfur tall oil fatty acid 审中-公开
标题翻译：低硫妥尔油脂肪酸
公开(公告)号：US20120131847A1
公开(公告)日：2012-05-31
申请号：US13369945
申请日：2012-02-09
申请人： Charles M. Pollock , H. Jerrold Miller , M. David Peterson
发明人： Charles M. Pollock , H. Jerrold Miller , M. David Peterson
IPC分类号： C10L1/188
CPC分类号： C10L1/02 , C10G25/00 , C10G2300/1014 , C10G2300/202 , C10G2300/44 , C10L1/1888 , C10L1/2381 , C11B13/00 , Y02P30/20 , Y02W30/74
摘要： The invention relates to tall oil fatty acid compositions having low sulfur content, as well as methods of using and making the same.
摘要翻译：本发明涉及具有低硫含量的妥尔油脂肪酸组合物，以及其使用和制备方法。

3. 发明授权

US06596825B1 Low gel high cis polydiene 有权
标题翻译：低凝胶高顺式聚二烯
公开(公告)号：US06596825B1
公开(公告)日：2003-07-22
申请号：US10208520
申请日：2002-07-30
申请人： H. Jerrold Miller
发明人： H. Jerrold Miller
IPC分类号： C08F242
CPC分类号： C08F36/04 , C08F4/7098 , C08F2/42
摘要： The present invention is directed to a process for forming a high-cis polydiene. The process includes catalyzing a diene polymerization, and terminating the polymerization with an amine-water termination mixture, preferably a TMEDA-water termination mixture. The catalyst system is a mixture of (a) organoaluminum compounds; (b) organonickel compounds; and (c) fluorine-containing compounds.
摘要翻译：本发明涉及形成高顺式聚二烯的方法。该方法包括催化二烯聚合，并用胺 - 水终止混合物，优选TMEDA-水终止混合物终止聚合。催化剂体系是（a）有机铝化合物的混合物; （b）有机锡化合物; 和（c）含氟化合物。

4. 发明授权

US06992147B1 Modified polymers prepared with lanthanide-based catalysts 有权
标题翻译：用镧系元素催化剂制备的改性聚合物
公开(公告)号：US06992147B1
公开(公告)日：2006-01-31
申请号：US10296084
申请日：2000-11-10
申请人： Yoichi Ozawa , H. Jerrold Miller , Koji Masaki , Tatsuo Fujimaki , Takuo Sone , Iwakazu Hattori , Koichi Morita
发明人： Yoichi Ozawa , H. Jerrold Miller , Koji Masaki , Tatsuo Fujimaki , Takuo Sone , Iwakazu Hattori , Koichi Morita
IPC分类号： C08C19/00 , C08F8/00
CPC分类号： C08C19/44 , C08F136/04 , C08K3/36 , C08L7/00 , C08L9/06 , C08L19/006 , C08F4/545 , C08L2666/08
摘要： A method for preparing a functionalized polymer comprising the steps of preparing a pseudo-living polymer by polymerizing conjugated diene monomer with a lanthanide-based catalyst, and reacting the pseudo-living polymer with at least one functionalizing agent defined by the formula (I) where A is a substituent that will undergo an addition reaction with a pseudo-living polymer, R1 is a divalent organic group, R2 is a monovalent organic group, and each R4, which may be the same or different, is a monovalent organic group or a substituent defined by —OR5 where R5 is a monovalent organic group, with the proviso that A, R1, R2, R4, and R5 are substituents that will not protonate a pseudo-living polymer. Also, the functionalized polymer and a vulcanizable composition containing the polymer.
摘要翻译：一种制备官能化聚合物的方法，包括以下步骤：通过使共轭二烯单体与镧系元素基催化剂聚合制备假活性聚合物，并使假活性聚合物与至少一种由式（I）定义的官能化试剂反应，其中 A是将与假活性聚合物进行加成反应的取代基，R 1是二价有机基团，R 2是一价有机基团，并且每个R 可以相同或不同的一价有机基团或由-OR 5定义的取代基，其中R 5是一价有机基团，条件是A，R 1，R 2，R 4和R 5都是不会将假活性聚合物质子化的取代基。此外，官能化聚合物和含有聚合物的可硫化组合物。

5. 发明授权

US07750087B2 Modified polymers prepared with lanthanide-based catalysts 有权
标题翻译：用镧系元素催化剂制备的改性聚合物
公开(公告)号：US07750087B2
公开(公告)日：2010-07-06
申请号：US11244999
申请日：2005-10-06
申请人： Yoichi Ozawa , H. Jerrold Miller , Koji Masaki , Tatsuo Fujimaki , Takuo Sone , Iwakazu Hattori , Koichi Morita
发明人： Yoichi Ozawa , H. Jerrold Miller , Koji Masaki , Tatsuo Fujimaki , Takuo Sone , Iwakazu Hattori , Koichi Morita
IPC分类号： C08C19/00 , C08F8/00
CPC分类号： C08C19/44 , C08F136/04 , C08K3/36 , C08L7/00 , C08L9/06 , C08L19/006 , C08F4/545 , C08L2666/08
摘要： A method for preparing a functionalized polymer comprising the steps of preparing a pseudo-living polymer by polymerizing conjugated diene monomer with a lanthanide-based catalyst, and reacting the pseudo-living polymer with at least one functionalizing agent defined by the formula (I) where A is a substituent that will undergo an addition reaction with a pseudo-living polymer, R1 is a divalent organic group, R2 is a monovalent organic group, and each R4, which may be the same or different, is a monovalent organic group or a substituent defined by —OR5 where R5 is a monovalent organic group, with the proviso that A, R1, R2, R4, and R5 are substituents that will not protonate a pseudo-living polymer. Also, the functionalized polymer and a vulcanizable composition containing the polymer.
摘要翻译：一种制备官能化聚合物的方法，包括以下步骤：通过使共轭二烯单体与镧系元素基催化剂聚合制备假活性聚合物，并使假活性聚合物与式（I）定义的至少一种官能化试剂反应，其中 A是将与假活性聚合物进行加成反应的取代基，R 1是二价有机基团，R 2是一价有机基团，并且各个可以相同或不同的R 4是一价有机基团或由-OR5定义的取代基，其中R5是一价有机基团，条件是A，R1，R2，R4和R5是不会使假活性聚合物质子化的取代基。此外，官能化聚合物和含有聚合物的可硫化组合物。

6. 发明申请

US20100099826A1 FUNTIONALIZED HIGH CIS-1,4-POLYBUTADIENE PREPARED USING NOVEL FUNCTIONALIZING AGENTS 有权
标题翻译：使用新型功能化剂制备的功能性高的CIS-1,4-聚丁二烯
公开(公告)号：US20100099826A1
公开(公告)日：2010-04-22
申请号：US12644382
申请日：2009-12-22
申请人： Yoichi OZAWA , H. Jerrold Miller , Koji Masaki , Koichi Morita , Tatsuo Fujimaki , Tetsuya Omura , Takuo Sone , Iwakazu Hattori
发明人： Yoichi OZAWA , H. Jerrold Miller , Koji Masaki , Koichi Morita , Tatsuo Fujimaki , Tetsuya Omura , Takuo Sone , Iwakazu Hattori
IPC分类号： C08F136/06
CPC分类号： C08F136/14 , C08C19/00 , C08C19/22 , C08C19/44 , C08F36/04 , C08F136/06 , C08K3/04 , C08K3/045 , C08K3/36 , C08L21/00 , C08L91/00 , C08F4/545 , C08L15/00
摘要： A method for preparing a functionalized polymer comprising the steps of preparing a polymer by polymerizing conjugated diene monomer with a lanthanide-based catalyst, wherein the lanthanide-based catalyst comprises (a) a lanthanide compound, (b) an alkylating agent, and (c) a source of halogen, and reacting the pseudo-living polymer with at least one amide-containing functionalizing agent.
摘要翻译：一种制备官能化聚合物的方法，包括以下步骤：通过使镧系元素基催化剂聚合共轭二烯单体来制备聚合物，其中所述镧系元素基催化剂包含（a）镧系元素化合物，（b）烷基化剂和（c ）卤素源，并使假活性聚合物与至少一种含酰胺官能化试剂反应。

7. 发明授权

US06977281B1 Modified polymers prepared with lanthanide-based catalysts 有权
公开(公告)号：US06977281B1
公开(公告)日：2005-12-20
申请号：US10296082
申请日：2000-11-10
申请人： Yoichi Ozawa , H. Jerrold Miller , Koji Masaki
发明人： Yoichi Ozawa , H. Jerrold Miller , Koji Masaki
IPC分类号： C08C19/22 , C08C19/44 , C08F8/30 , C08F136/04 , C08L19/00
CPC分类号： C08C19/44 , C08F136/04 , C08L19/006 , C08F4/545
摘要： A method for preparing a functionalized polymer comprising the steps of preparing a pseudo-living polymer by polymerizing conjugated diene monomer with a lanthanide-based catalyst, where said pseudo-living polymer is characterized by having greater than about 85 percent of the polymer in the cis microstructure and less than about 3 percent of the polymer is in the 1,2- or 3,4-microstructure, and reacting the pseudo-living polymer with at least one functionalizing agent defined by the formula (I) or (II) where Z is a substituent that will react or interact with organic or inorganic fillers; R1 is a single bond or a divalent organic group; R2 is a monovalent organic group or a divalent organic group that forms a cyclic organic group with R13 or R14; R3 is a single bond, a divalent organic group, or a trivalent organic group that forms a cyclic organic group with R4 or R5; R13 is a single bond, a divalent organic group, or a trivalent organic group that forms a cyclic organic group with R2 or R14; R4 is a monovalent organic group or a divalent organic group that forms a cyclic organic group with R3 or R5; R14 is a monovalent organic group or a divalent organic group that forms a cyclic organic group with R2 or R13; and R5 is a monovalent organic group or a divalent organic group that forms a cyclic organic group with R3 or R4; with the proviso that each group attached to the imino carbon is attached via a carbon atom and R1, R2, R3, R4, R5, R13, R14 and Z are substituents that will not protonate a pseudo-living polymer.

8. 发明申请

US20130102736A1 FUNCTIONALIZED HIGH CIS-1,4-POLYBUTADIENE PREPARED USING NOVEL FUNCTIONALIZING AGENTS 有权
标题翻译：使用新型功能化剂制备的功能性高的CIS-1,4-聚丁二烯
公开(公告)号：US20130102736A1
公开(公告)日：2013-04-25
申请号：US13711701
申请日：2012-12-12
申请人： Yoichi OZAWA , H. Jerrold MILLER , Koji MASAKI , Koichi MORITA , Tatsuo FUJIMAKI , Tetsuyo OHUMURA , Takuo SONE , Iwakazu HATTORI
发明人： Yoichi OZAWA , H. Jerrold MILLER , Koji MASAKI , Koichi MORITA , Tatsuo FUJIMAKI , Tetsuyo OHUMURA , Takuo SONE , Iwakazu HATTORI
IPC分类号： C08C19/22
CPC分类号： C08F136/14 , C08C19/00 , C08C19/22 , C08C19/44 , C08F36/04 , C08F136/06 , C08K3/04 , C08K3/045 , C08K3/36 , C08L21/00 , C08L91/00 , C08F4/545 , C08L15/00
摘要： A method for preparing a functionalized polymer comprising the steps of preparing a polymer by polymerizing conjugated diene monomer with a lanthanide-based catalyst, wherein the lanthanide-based catalyst comprises (a) a lanthanide compound, (b) an alkylating agent, and (c) a source of halogen, and reacting the pseudo-living polymer with at least one amide-containing functionalizing agent.
摘要翻译：一种制备官能化聚合物的方法，包括以下步骤：通过使镧系元素基催化剂聚合共轭二烯单体来制备聚合物，其中所述镧系元素基催化剂包含（a）镧系元素化合物，（b）烷基化剂和（c ）卤素源，并使假活性聚合物与至少一种含酰胺官能化试剂反应。

9. 发明授权

US06437205B1 Low molecular weight high-cis polybutadienes and their use in high molecular weight-low molecular weight high-cis polybutadiene blends 有权
标题翻译：低分子量高顺式聚丁二烯及其在高分子量低分子量高顺式聚丁二烯共混物中的应用
公开(公告)号：US06437205B1
公开(公告)日：2002-08-20
申请号：US09600150
申请日：2000-07-10
申请人： H. Jerrold Miller , Tatsuro Hamada , Yoichi Ozawa , Peyman Pakdel
发明人： H. Jerrold Miller , Tatsuro Hamada , Yoichi Ozawa , Peyman Pakdel
IPC分类号： C10L116
CPC分类号： C08L9/00 , C08F36/06 , Y02T10/862 , C08F4/545 , C08L2666/08
摘要： A process for polymerizing 1,3-butadiene into a low molecular weight high-cis polybutadiene is described using a catalyst system comprising: (a) a neodymium-containing compound, (b) an aluminoxane or a trialkyl aluminum compound, (c) an organoaluminum hydride, and (d) a halogen source. A blend of a high molecular weight high-cis polybutadiene and the low molecular weight high-cis polybutadiene is also disclosed for use in pneumatic tire treads. Desirably both the high and the low molecular weight polymers have high cis contents, with the low molecular weight polymer being at least 70 percent cis and the high molecular weight polymer being at least 92 percent cis. Desirably both polymers are made with a neodymium catalyst system. The blends provide a balance of properties including good snow traction, wet traction, and rolling resistance while providing a balance of good physical properties including tension at break, modulus etc.
摘要翻译：使用催化剂体系描述了将1,3-丁二烯聚合成低分子量高顺式聚丁二烯的方法，该催化剂体系包含：（a）含钕化合物，（b）铝氧烷或三烷基铝化合物，（c）有机铝氢化物，（d）卤素源。还公开了高分子量高顺式聚丁二烯和低分子量高顺式聚丁二烯的共混物用于充气轮胎胎面。高分子量聚合物和低分子量聚合物理想地具有高顺式含量，低分子量聚合物为顺式至少70％，高分子量聚合物为顺式至少92％。理想地，两种聚合物都是用钕催化剂体系制成的。混合物提供了平衡的性能，包括良好的积雪牵引力，湿牵引力和滚动阻力，同时提供良好的物理性能，包括断裂张力，模量等的平衡。

10. 发明授权

US08362126B2 Functionalized high cis-1,4-polybutadiene prepared using novel functionalizing agents 有权
标题翻译：使用新型官能化剂制备的官能化高顺式-1,4-聚丁二烯
公开(公告)号：US08362126B2
公开(公告)日：2013-01-29
申请号：US12644382
申请日：2009-12-22
申请人： Yoichi Ozawa , H. Jerrold Miller , Koji Masaki , Koichi Morita , Tatsuo Fujimaki , Tetsuya Omura , Takuo Sone , Iwakazu Hattori
发明人： Yoichi Ozawa , H. Jerrold Miller , Koji Masaki , Koichi Morita , Tatsuo Fujimaki , Tetsuya Omura , Takuo Sone , Iwakazu Hattori
IPC分类号： C08K5/13 , C08F36/00
CPC分类号： C08F136/14 , C08C19/00 , C08C19/22 , C08C19/44 , C08F36/04 , C08F136/06 , C08K3/04 , C08K3/045 , C08K3/36 , C08L21/00 , C08L91/00 , C08F4/545 , C08L15/00
摘要： A method for preparing a functionalized polymer comprising the steps of preparing a polymer by polymerizing conjugated diene monomer with a lanthanide-based catalyst, wherein the lanthanide-based catalyst comprises (a) a lanthanide compound, (b) an alkylating agent, and (c) a source of halogen, and reacting the pseudo-living polymer with at least one amide-containing functionalizing agent.
摘要翻译：一种制备官能化聚合物的方法，包括以下步骤：通过使镧系元素基催化剂聚合共轭二烯单体来制备聚合物，其中所述镧系元素基催化剂包含（a）镧系元素化合物，（b）烷基化剂和（c ）卤素源，并使假活性聚合物与至少一种含酰胺官能化试剂反应。

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