发明申请
WO2019102030A1 PROCESS FOR THE PRODUCTION OF 1,4-BUTANEDIOL FROM RENEWABLE SOURCES AND POLYESTERS OBTAINED THEREFROM
审中-公开
基本信息:
- 专利标题: PROCESS FOR THE PRODUCTION OF 1,4-BUTANEDIOL FROM RENEWABLE SOURCES AND POLYESTERS OBTAINED THEREFROM
- 申请号:PCT/EP2018/082668 申请日:2018-11-27
- 公开(公告)号:WO2019102030A1 公开(公告)日:2019-05-31
- 发明人: COTTI COMETTINI, Marco , VALLERO, Roberto , BASTIOLI, Catia , CAPUZZI, Luigi
- 申请人: NOVAMONT S.P.A.
- 申请人地址: Via G. Fauser, 8 I-28100 Novara IT
- 专利权人: NOVAMONT S.P.A.
- 当前专利权人: NOVAMONT S.P.A.
- 当前专利权人地址: Via G. Fauser, 8 I-28100 Novara IT
- 代理机构: ZANOLI, Enrico et al.
- 优先权: IT102017000135678 20171127
- 主分类号: B01D3/14
- IPC分类号: B01D3/14 ; B01D3/00 ; C07C27/00
摘要:
The invention relates to a process for the production of 1,4-butanediol comprising the preparation of a fermentation broth comprising 1,4- butanediol from renewable sources and water, separation of a liquid fraction comprising said 1,4-butanediol and water from one or more solid fractions, said liquid fraction comprising 2-pyrrolidone in an amount higher than 80 ppm, one or more passages of the resulting liquid fraction through a bed comprising one or more cation-exchange resins thereby providing an output pH of said liquid fraction from 4 to 2, one or more passages of the resulting liquid fraction through a bed comprising one or more anion-exchange resins thereby providing an output pH of said liquid fraction from 8 to 11, and the distillation of the liquid fraction thereby provided so as to obtain a composition having a concentration of said 1,4-butanediol higher than 99.0% by weight and comprising 2-pyrrolidone in an amount lower than 6 ppm. The resulting composition should exhibit an APHA color value after ageing of less than 30.
IPC结构图谱:
B | 作业;运输 |
--B01 | 一般的物理或化学的方法或装置 |
----B01D | 分离 |
------B01D3/00 | 蒸馏或相关的在液体同气体介质相接触的过程中发生交换的方法,例如汽提 |
--------B01D3/14 | .分馏 |