基本信息:
- 专利标题: 액상으로의 아민의 포스겐화에 의한 이소시아네이트의 제조 방법
- 专利标题(英):Method for producing isocyanates by phosgenating amines in liquid phase
- 专利标题(中):通过在液相中溶解氨来生产异氰酸酯的方法
- 申请号:KR1020157013391 申请日:2013-10-23
- 公开(公告)号:KR1020150074132A 公开(公告)日:2015-07-01
- 发明人: 마트케토르슈텐 , 힐러마르쿠스 , 파라쉬한스위르겐
- 申请人: 바스프 에스이
- 申请人地址: Carl-Bosch-Str. **, ***** Ludwigshafen am Rhein, Germany
- 专利权人: 바스프 에스이
- 当前专利权人: 바스프 에스이
- 当前专利权人地址: Carl-Bosch-Str. **, ***** Ludwigshafen am Rhein, Germany
- 代理人: 김진회; 김태홍
- 优先权: EP121897656 2012-10-24
- 国际申请: PCT/EP2013/072112 2013-10-23
- 国际公布: WO2014064128 2014-05-01
- 主分类号: C07C263/10
- IPC分类号: C07C263/10 ; C07C263/18 ; C07C265/02 ; C07C265/16
The present invention comprising the steps of: (a) a mixture of a liquid amine-containing reactant stream (1) and the liquid phosgene-containing reactant stream (2) to obtain a reaction mixture; (B) reacting the reaction mixture in the residence time reactor (R) to obtain a reaction mixture (3); (C) reaction by reacting a reaction mixture (3) in a column (K1) to obtain a head stream (4) and a bottom stream (5), the method comprising: feeding the bottom stream (5) in the phosgene / hydrogen chloride stripping column (K2) .; (D) the bottom stream containing the isocyanate and the solvent in the phosgene / hydrogen chloride stripping column (K2) and through the head stream (6) separated by a phosgene and hydrogen chloride by distillation, the phosgene / hydrogen chloride stripping column (K2) of 7 in the obtaining step, and the method steps from the bottom stream (7); (E) separating the solvent by distillation in step, and a method to obtain a marketable product isocyanate; (F) separation column (K3) by thermal fractionation of steam from the phosgene / hydrogen chloride stripping column (K2) in the overhead, hydrogen chloride-containing vapor stream (13), and phosgene, and a bottom stream which is recycled to the containing and method steps a) and the solvent 14 heads in a production process of isocyanates by the reaction of the amine with the phosgene in the carrying the method steps of a step in a liquid state, the method step (f) the phosgene / hydrogen chloride stripping column (K2), the column fractionation in obtaining a compared to pressure it relates to a process for producing an isocyanate, characterized in that for performing the head pressure in the high-separation column (K3).
公开/授权文献:
- KR102209958B1 액상으로의 아민의 포스겐화에 의한 이소시아네이트의 제조 방법 公开/授权日:2021-02-01
信息查询:
EspacenetIPC结构图谱:
C | 化学;冶金 |
--C07 | 有机化学 |
----C07C | 无环或碳环化合物 |
------C07C263/00 | 异氰酸衍生物的制备 |
--------C07C263/10 | .由胺或羧基卤化物,例如与光气反应 |