基本信息:
- 专利标题： 고순도 2-(트리시클로［5.2.1.02,6］데칸-3-엔-8-일옥시)에탄올의 제조방법
- 专利标题（英）：Manufacturing method of highly pure 2-(tricyclo[5.2.1.02,6] dec-3-en-8-yloxy)ethanol
- 专利标题（中）：高纯度2-（三环[5.2.1.0 2,6]癸-3-烯-8-基氧基）乙醇的制备方法
- 申请号：KR1020120045669 申请日：2012-04-30
- 公开(公告)号：KR101395729B1 公开(公告)日：2014-05-19
- 发明人： 조양래 , 정선이 , 허정희 , 유혜리 , 손효빈 , 정현윤 , 박정배
- 申请人： (주)위즈켐 , 조양래
- 申请人地址： 울산광역시 울주군 온산읍 회학*길 **-**
- 专利权人： (주)위즈켐,조양래
- 当前专利权人： (주)위즈켐,조양래
- 当前专利权人地址： 울산광역시 울주군 온산읍 회학*길 **-**
- 代理人： 김수진; 윤의섭
- 主分类号： C07C41/58
- IPC分类号： C07C41/58 ; C07C41/32 ; C07C43/18 ; C07B41/04
또한, 본 발명은 디시클로펜타디엔과 에틸렌글리콜의 부가반응으로 생성되는 액상의 불순한 2-(트리시클로[5.2.1.02,6]데칸-3-엔-8-일옥시)에탄올을 9-안트라센카보닐 클로라이드와의 에스테르화 반응으로 2-(트리시클로[5.2.1.02,6]데칸-3-엔-8-일옥시)에틸 9-안트라센카복실레이트를 결정고체로 제조하고 이를 재결정 정제한 후 가수분해를 통하여 고 순도의 2-(트리시클로[5.2.1.02,6]데칸-3-엔-8-일옥시)에탄올을 제조하는 신규의 제조방법을 제공한다.
The present invention is highly pure 2- (tricyclo decane-3-en-8-yloxy) of the major monomer relates to a method of producing ethanol, useful polymers, etc. and more particularly paints, adhesives, building sealants, anti-corrosion coating agent 2- (tricyclo [5.2.1.0 2,6] decane-3-en-8-yloxy) ethyl methacrylate or 2- (tricyclo [5.2.1.0 2,6] decane-3-en-8-yloxy ) relates to a method for producing a method, the main ingredient of 2- (tricyclo [5.2.1.0 2,6] decane-3-en-8-yloxy) ethanol in the manufacture of ethyl acrylate with high purity.
The present invention is dicyclopentadiene and impure 2 of the liquid generated by the addition reaction of ethylene glycol (tricyclo [5.2.1.0 2,6] decane-3-en-8-yloxy) ethanol 9-anthracene-carbonitrile the esterification reaction between the carbonyl chloride 2- (tricyclo [5.2.1.0 2,6] decane-3-en-8-yloxy) acetate produced a 9-anthracene-carboxylate as a crystalline solid, and re-crystallization was purified and then hydrolised a high-2- (tricyclo [5.2.1.0 2,6] decane-3-en-8-yloxy) with a purity of over provides a process for the preparation of novel for producing ethanol.
公开/授权文献:
- KR1020130122384A 고순도 2-(트리시클로［5.2.1.02,6］데칸-3-엔-8-일옥시)에탄올의 제조방법 公开/授权日：2013-11-07