基本信息:
- 专利标题: 精製ナフタレンジカルボン酸の製造方法
- 专利标题(英):Method for producing a purified naphthalenedicarboxylic acid
- 专利标题(中):用于制备纯化的萘二羧酸的方法
- 申请号:JP2013518138 申请日:2012-05-30
- 公开(公告)号:JPWO2012165506A1 公开(公告)日:2015-02-23
- 发明人: 秀治 倉島 , 秀治 倉島 , 正義 林 , 正義 林 , 橋本 晃男 , 晃男 橋本 , 重松 隆助 , 隆助 重松
- 申请人: 三菱瓦斯化学株式会社
- 专利权人: 三菱瓦斯化学株式会社
- 当前专利权人: 三菱瓦斯化学株式会社
- 优先权: JP2011120464 2011-05-30
- 主分类号: C07C51/487
- IPC分类号: C07C51/487 ; C07C51/43 ; C07C63/38
Naphthalenedicarboxylic acid containing raw material and a mixture of the amine to obtain crystals of naphthalenedicarboxylic acid amine salt step in a mixture of water and an organic solvent; and purifying naphthalenedicarboxylic from crystals of naphthalenedicarboxylic acid amine salt obtained in the above step comprising the step of obtaining the acid, a method for producing a purified naphthalenedicarboxylic acid, (1) water, with the addition of an amine to a slurry containing an organic solvent and naphthalene dicarboxylic acid in the process of forming the naphthalene dicarboxylic acid amine salts, amine addition rate of per minute from 0.002 to 0.4 mol of naphthalene dicarboxylic acid 1 mol, or (2) a naphthalene dicarboxylic acid amine salt to an aqueous solution prepared by dissolving in water or an aqueous solution thereof solid a liquid obtained by liquid separation, the addition of amine to precipitate by insolubilize the metal content, precipitated are removed by solid-liquid separation of the metal component that is, to provide a method of manufacturing a purified naphthalenedicarboxylic acid.
公开/授权文献:
- JP5994774B2 精製ナフタレンジカルボン酸の製造方法 公开/授权日:2016-09-21
信息查询:
EspacenetIPC结构图谱:
C | 化学;冶金 |
--C07 | 有机化学 |
----C07C | 无环或碳环化合物 |
------C07C51/00 | 羧酸或它们的盐、卤化物或酐的制备 |
--------C07C51/42 | .分离;纯化;稳定化;添加剂的使用 |
----------C07C51/487 | ..用使发生化学改性的处理 |