![LIGNOCELLULOSE PROCESSING](/ep/2014/02/12/EP2694723A1/abs.jpg.150x150.jpg)
基本信息:
- 专利标题: LIGNOCELLULOSE PROCESSING
- 专利标题(中):木质纤维素加工
- 申请号:EP12716644.5 申请日:2012-03-29
- 公开(公告)号:EP2694723A1 公开(公告)日:2014-02-12
- 发明人: HAVERTY, Donncha
- 申请人: University of Limerick
- 申请人地址: Plassey Technological Park Limerick IE
- 专利权人: University of Limerick
- 当前专利权人: University of Limerick
- 当前专利权人地址: Plassey Technological Park Limerick IE
- 代理机构: Weldon, Michael James
- 优先权: IE20110161 20110401
- 国际公布: WO2012131665 20121004
- 主分类号: D21C1/08
- IPC分类号: D21C1/08 ; D21C3/02 ; D21C3/22 ; D21C9/16
摘要:
A method of transforming a lignocellulose material comprises the steps of: a. combining a lignocellulose material with a solution containing hydrogen peroxide and a hydrogen peroxide stabiliser to produce a mixture that is at least 3% by mass hydrogen peroxide, b. feeding said mixture to the entrance of a continuous reactor concomitant with providing an agent that facilitates the rapid decomposition of the hydrogen peroxide in the solution proximal to the entrance of the reactor so as to cause exothermic, explosive decomposition of the hydrogen peroxide to oxygen and water thus forming a mixture of gas, liquid, and solids and increasing the pressure and temperature in the reactor to at least 15 bar, and 70°C respectively without addition of heat from an external source, c. exiting the mixture of gas, water and solids formed in the reactor through an outlet with a pressure change, into a flash vessel wherein the mixture is separated into a liquid phase containing dissolved or suspended solids and a gas phase substantially rich in oxygen, and d. continuously removing from the flash vessel a gas stream substantially rich in oxygen and a separate heated liquid stream having suspended or dissolved therein chemically and physically altered components of the lignocellulose including a substantially cellulosic material with reduced recalcitrance relative to the starting lignocellulose material.
摘要(中):
转化木质纤维素材料的方法包括以下步骤:a。 将木质纤维素材料与含有过氧化氢和过氧化氢稳定剂的溶液混合以产生至少3质量%过氧化氢的混合物,b。 将所述混合物进料到连续反应器的入口,同时提供促进过氧化氢在接近反应器入口的溶液中快速分解的试剂,以引起过氧化氢放热,爆炸性分解成氧和水 从而形成气体,液体和固体的混合物,并且分别将反应器中的压力和温度增加至至少15巴和70℃,而不从外部来源加热,c。 通过压力变化的出口将反应器中形成的气体,水和固体的混合物排出到闪蒸容器中,其中混合物被分离成含有溶解或悬浮的固体和基本上富含氧的气相的液相,d 。 从闪蒸容器中连续地除去基本上富含氧的气流和其中悬浮或溶解有分离的化学和物理改变的木质纤维素组分的单独的加热液体流,所述木质纤维素组分包括相对于起始木质纤维素材料具有降低的不相容性的基本上纤维素材料。
IPC结构图谱:
D | 纺织;造纸 |
--D21 | 造纸;纤维素的生产 |
----D21C | 从含纤维素原料中除去非纤维素物质生产纤维素;制浆药液的再生;所需设备 |
------D21C1/00 | 蒸煮前经过精细分裂的原料的预处理 |
--------D21C1/08 | .用产生氧的化合物 |