
基本信息:
- 专利标题: 一种煤沥青临氢催化-供氢处理制备可纺中间相沥青的方法
- 专利标题(英):Method for preparing spinnable mesophase pitch through coal pitch hydrocatalysis-hydrogen supply treatment
- 申请号:CN201910973122.1 申请日:2019-10-14
- 公开(公告)号:CN110699107A 公开(公告)日:2020-01-17
- 发明人: 杜俊涛 , 聂毅 , 郏慧娜 , 张敏鑫 , 孙一凯 , 吕家贺 , 马江凯 , 郑双双
- 申请人: 郑州中科新兴产业技术研究院
- 申请人地址: 河南省郑州市金水区杨金路牛顿国际A座10层
- 专利权人: 郑州中科新兴产业技术研究院
- 当前专利权人: 郑州中科新兴产业技术研究院
- 当前专利权人地址: 河南省郑州市金水区杨金路牛顿国际A座10层
- 代理机构: 郑州优盾知识产权代理有限公司
- 代理人: 王红培
- 主分类号: C10C3/02
- IPC分类号: C10C3/02
The invention discloses a method for preparing spinnable mesophase pitch through coal pitch hydrocatalysis-hydrogen supply treatment. The method comprises the following steps: (1) adding aids into coal pitch, promoting primary inorganic mineral to form a dispersed catalyst in situ under the high-temperature hydrogen condition, performing hydrocatalysis treatment on the coal pitch, performing reduced pressure distillation after reaction to remove a fraction with low boiling point to obtain primary hydrogenated pitch; (2) adding a hydrogen supply agent into the primary hydrogenated pitch, performing hydrocatalysis-hydrogen supply cooperative treatment under the high-temperature hydrogen condition, and performing reduced pressure distillation to remove a fraction with low boiling point to obtain secondary hydrogenated pitch; (3) removing a quinoline insoluble substance from the secondary hydrogenated pitch to obtain refined hydrogenated pitch; and (4) performing thermal polymerization reaction on the refined hydrogenated pitch to obtain the spinnable mesophase pitch. Through hydrocatalysis-hydrogen supply combined treatment, formation and transformation of the mesophase pitch can be effectively regulated and controlled; and the obtained spinnable mesophase pitch has excellent quality, moderate softening point and high mesophase content and can be applied to preparation of high-performance pitch-based carbon fiber.
公开/授权文献:
- CN110699107B 一种煤沥青临氢催化-供氢处理制备可纺中间相沥青的方法 公开/授权日:2020-06-12
IPC结构图谱:
C | 化学;冶金 |
--C10 | 石油、煤气及炼焦工业;含一氧化碳的工业气体;燃料;润滑剂;泥煤 |
----C10C | 焦油、焦油沥青、石油沥青、天然沥青的加工;焦木酸 |
------C10C3/00 | 焦油沥青、石油沥青、天然沥青的加工 |
--------C10C3/02 | .用化学方法 |