
基本信息:
- 专利标题: 一种含硼碳化硅纤维及其制备方法
- 专利标题(英):Boron-containing silicon carbide fiber and preparation method thereof
- 申请号:CN201911043861.7 申请日:2019-10-30
- 公开(公告)号:CN110629324A 公开(公告)日:2019-12-31
- 发明人: 莫高明 , 宋育杰 , 欧阳琴 , 王艳菲 , 皇甫志云 , 何流 , 黄庆 , 黄政仁
- 申请人: 中国科学院宁波材料技术与工程研究所
- 申请人地址: 浙江省宁波市镇海区庄市大道519号
- 专利权人: 中国科学院宁波材料技术与工程研究所
- 当前专利权人: 中国科学院宁波材料技术与工程研究所
- 当前专利权人地址: 浙江省宁波市镇海区庄市大道519号
- 代理机构: 南京利丰知识产权代理事务所
- 代理人: 王茹; 王锋
- 主分类号: D01F9/10
- IPC分类号: D01F9/10
The invention discloses a boron-containing silicon carbide fiber and a preparation method thereof. The preparation method of the boron-containing silicon carbide fiber comprises the following steps: in a closed reaction container, carrying out synthesis reaction on polysilacarbosilane and a boron-containing monomer at high temperature and under high pressure to generate a boron-containing polycarbosilane crude material, wherein the polysilacarbosilane is a low-molecular product of polydimethylsiloxane subjected to high-temperature cracking, is in a liquid state at room temperature, and has a molecular weight less than 1000 g/mol; dissolving and filtering the boron-containing polycarbosilane crude material to obtain a spinning-grade boron-containing polycarbosilane precursor; and carrying out melt spinning, non-melting, high-temperature sintering and sintering treatment on the spinning-grade boron-containing polycarbosilane precursor to obtain the boron-containing silicon carbide fiber.Compared with the prior art, the preparation method provided by the invention is simple in process and easy to operate, and the synthesized boron-containing polycarbosilane precursor has the advantages of good spinnability, convenience in adjustment of boron content and the like.
公开/授权文献:
- CN110629324B 一种含硼碳化硅纤维及其制备方法 公开/授权日:2022-04-08
IPC结构图谱:
D | 纺织;造纸 |
--D01 | 天然或人造的线或纤维;纺纱或纺丝 |
----D01F | 制作人造长丝、线、纤维、鬃或带子的化学特征;专用于生产碳纤维的设备 |
------D01F9/00 | 其他原料的人造长丝或类似物;其制造;专用于生产碳纤维的设备 |
--------D01F9/08 | .无机原料 |
----------D01F9/10 | ..通过有机物的分解 |