![一种电池级磷酸铁合成工艺过程中废水资源化利用的方法](/CN/2019/1/175/images/201910876185.jpg)
基本信息:
- 专利标题: 一种电池级磷酸铁合成工艺过程中废水资源化利用的方法
- 专利标题(英):Method for resource utilization of wastewater in synthetic process of battery-grade iron phosphate
- 申请号:CN201910876185.5 申请日:2019-09-17
- 公开(公告)号:CN110589788A 公开(公告)日:2019-12-20
- 发明人: 宋开荣 , 刘雄才 , 郭勇 , 张红胜 , 王强胜
- 申请人: 襄阳泽东新能源发展有限公司
- 申请人地址: 湖北省襄阳市襄城区余家湖化工工业园11幢401-408号
- 专利权人: 襄阳泽东新能源发展有限公司
- 当前专利权人: 襄阳泽东新能源发展有限公司
- 当前专利权人地址: 湖北省襄阳市襄城区余家湖化工工业园11幢401-408号
- 代理机构: 武汉智嘉联合知识产权代理事务所
- 代理人: 赵泽夏
- 主分类号: C01B25/28
- IPC分类号: C01B25/28 ; C01C1/24 ; C02F9/10 ; C02F101/10 ; C02F101/16
The invention discloses a method for resource utilization of wastewater in the synthetic process of battery-grade iron phosphate. The method comprises the following steps: a, adding ammonia water to adjust the pH value of the wastewater generated in the synthetic process of the iron phosphate to 7-8 to obtain a solution; b, filtering the solution for multiple times to obtain a product, namely a filtrate without suspended solids; c, pumping the filtrate into an ultrahigh-pressure reverse osmosis device, and performing a reaction to obtain concentrated water A and fresh water A; d, introducing the concentrated water A into an MVR evaporative crystallization device, carrying out vacuum concentration evaporative crystallization to obtain an ammonium sulfate and monoammonium phosphate mixture and evaporation condensate water, and carrying out centrifugal separation on the ammonium sulfate and monoammonium phosphate mixture to respectively obtain ammonium sulfate and monoammonium phosphate;e, mixing the fresh water A and the evaporation condensate water, and pumping the mixed water into a primary reverse osmosis device to obtain concentrated water B and fresh water B; and f, pumping theconcentrated water B into an ultrahigh-pressure reverse osmosis device, and recovering the fresh water B. The method has the beneficial effect that the treatment cost of the wastewater can be saved.