基本信息:
- 专利标题： 一种铜配合物的制备方法及其应用
- 专利标题（英）：Preparation method of copper complex and application thereof
- 申请号：CN201810563915.1 申请日：2018-06-04
- 公开(公告)号：CN108840878A 公开(公告)日：2018-11-20
- 发明人： 李宝红 , 刘建强 , 刘伟聪 , 马爱青 , 罗志董 , 解玉玲 , 郑明彬 , 彭新生 , 施踏青
- 申请人： 广东医科大学
- 申请人地址： 广东省东莞市松山湖科技园新城大道1号
- 专利权人： 广东医科大学
- 当前专利权人： 广东医科大学
- 当前专利权人地址： 广东省东莞市松山湖科技园新城大道1号
- 代理机构： 东莞众业知识产权代理事务所
- 代理人： 何恒韬
- 主分类号： C07F1/08
- IPC分类号： C07F1/08 ; B01J20/22 ; B01J20/28 ; B01J20/30 ; C02F1/28 ; C02F101/34 ; C02F101/36 ; C02F101/38
The invention discloses a preparation method of a copper complex and application thereof. The preparation method comprises the following steps: 1) mixing copper chloride dehydrate with 1,4-di-(triazole-1-yl) terephthalic acid, and adding the mixture into a solvent to be uniformly stirred to obtain a mixed solution A; and then adding nitric acid to stir the solution to obtain a mixed solution B; 2)in a sealing condition, putting the mixed solution B at 110-130 DEG C to react for 10-14 h to obtain crystals C; and 3) cleaning the crystals C with ethanol for three times, then putting the crystalsC in methanol to be soaked for 2 days, then putting the crystals C in dichloromethane to be soaked for 1 day, and finally putting the crystals C in an oven to be dried to obtain the copper complex. The method disclosed by the invention is simple in synthesis and high in yield. The copper complex has high adsorption efficiency on diclofenac sodium and still has good desorption ability and cyclic utilization ability after adsorbing drug pollutants, so that the copper complex has a potential application in adsorbing drug pollutants in a water environment.
公开/授权文献:
- CN108840878B 一种铜配合物的制备方法及其应用 公开/授权日：2020-08-25
IPC结构图谱:
| C | 化学；冶金 |
| --C07 | 有机化学 |
| ----C07F | 含除碳、氢、卤素、氧、氮、硫、硒或碲以外的其他元素的无环，碳环或杂环化合物 |
| ------C07F1/00 | 含周期表第Ⅰ族元素的化合物 |
| --------C07F1/08 | .铜化合物 |