![一种芳烃化合物等温管式反应制备硝基化合物的方法](/CN/2016/1/244/images/201611223865.jpg)
基本信息:
- 专利标题: 一种芳烃化合物等温管式反应制备硝基化合物的方法
- 申请号:CN201611223865.X 申请日:2016-12-27
- 公开(公告)号:CN108238944B 公开(公告)日:2019-09-17
- 发明人: 杨忠林 , 金汉强 , 丁红霞 , 孙盛凯 , 赵思远 , 季峰崎
- 申请人: 中国石油化工股份有限公司 , 南化集团研究院
- 申请人地址: 江苏省南京市六合区葛关路699号
- 专利权人: 中国石油化工股份有限公司,南化集团研究院
- 当前专利权人: 中国石油化工股份有限公司,南化集团研究院
- 当前专利权人地址: 江苏省南京市六合区葛关路699号
- 代理机构: 南京天翼专利代理有限责任公司
- 代理人: 汤志武
- 主分类号: C07C201/08
- IPC分类号: C07C201/08 ; C07C205/06 ; C07C205/12 ; B01J19/24 ; B01J14/00
The invention belongs to the technical field of organic chemistry and particularly relates to a method for preparing a nitro compound from an aromatic hydrocarbon compound through isothermic tubular reaction. The method is characterized by comprising the following steps: adequately mixing two phases, namely a nitration raw material and mixed acid by virtue of a static mixer in a tubular reactor soas to realize simultaneous flow, reaction and heat exchange in a shell of the tubular reactor, and carrying out nitration separation, alkali washing, washing and refining, so as to obtain the nitro compound, wherein row tubes which can be controlled in different regions are arranged in the tubular reactor and are used for removing reaction heat. The method for preparing the nitro compound has thebeneficial effects that the flow is simple, the continuous production is realized, the reaction process is easy to control, the heat transfer efficiency is high, the situation that byproducts are increased due to the overheat in the reaction can be effectively avoided, the energy consumption and the raw material consumption are low, and the production process is safe and reliable.
公开/授权文献:
- CN108238944A 一种芳烃化合物等温管式反应制备硝基化合物的方法 公开/授权日:2018-07-03
IPC结构图谱:
C | 化学;冶金 |
--C07 | 有机化学 |
----C07C | 无环或碳环化合物 |
------C07C201/00 | 硝酸酯或亚硝酸酯的制备,或硝基或亚硝基直接连在碳架上的化合物的制备 |
--------C07C201/06 | .硝基化合物的制备 |
----------C07C201/08 | ..用硝基取代氢原子 |