![一种聚丁二酸丁二醇酯/类石墨烯二硫化钼纳米复合材料的制备方法](/CN/2017/1/205/images/201711029100.jpg)
基本信息:
- 专利标题: 一种聚丁二酸丁二醇酯/类石墨烯二硫化钼纳米复合材料的制备方法
- 专利标题(英):Preparation method for polybutylene succinate/graphene-molybdenum-disulfide-like nanocomposite material
- 申请号:CN201711029100.7 申请日:2017-10-29
- 公开(公告)号:CN107722246A 公开(公告)日:2018-02-23
- 发明人: 陈奎 , 张天云 , 刘广桥 , 董丽梅 , 陈建宏 , 郑小平
- 申请人: 兰州城市学院
- 申请人地址: 甘肃省兰州市安宁区兰州城市学院培黎校区
- 专利权人: 兰州城市学院
- 当前专利权人: 兰州城市学院
- 当前专利权人地址: 甘肃省兰州市安宁区兰州城市学院培黎校区
- 主分类号: C08G63/16
- IPC分类号: C08G63/16 ; C08K3/04 ; C08K3/30
The invention discloses a preparation method for a polybutylene succinate/graphene-molybdenum-disulfide-like nanocomposite material. The preparation method comprises the following steps: adding molybdenum disulfide powder to mixed liquid of butanediol and water, and centrifugally separating after the room temperature liquid phase ultrasonic treatment; adding a succinic acid to upper deep green liquid obtained by the centrifugal separation, strongly and mechanically stirring until no water is generated in 150-225 DEG C of the temperature under the nitrogen protection, to obtain a terminal hydroxyl prepolymer containing the graphene-molybdenum-disulfide-like; rapidly adding a catalyst to the terminal hydroxyl prepolymer under the stirring condition, and warming to 210-250 DEG C, and vacuumizing to 50-250 Pa, continuously stirring until the obvious pole-climbing occurs, and ending the reaction, to obtain the polybutylene succinate/graphene-molybdenum-disulfide-like nanocomposite material.The composite material is capable of improving the crystallization temperature of the polybutylene succinate, shortening the crystallization time, and refining the crystal grains of the polybutylenesuccinate.
公开/授权文献:
- CN107722246B 一种聚丁二酸丁二醇酯/类石墨烯二硫化钼纳米复合材料的制备方法 公开/授权日:2019-11-19
IPC结构图谱:
C | 化学;冶金 |
--C08 | 有机高分子化合物;其制备或化学加工;以其为基料的组合物 |
----C08G | 用碳—碳不饱和键以外的反应得到的高分子化合物 |
------C08G63/00 | 由在高分子主链上形成羧酸酯键的反应制得的高分子化合物 |
--------C08G63/02 | .由羟基羧酸或由多羧酸与多羟基化合物衍行的聚酯 |
----------C08G63/06 | ..由羟基羧酸衍生的 |
------------C08G63/16 | ...二羧酸与二羟基化合物 |