
基本信息:
- 专利标题: 海绵钛真空蒸馏的方法
- 专利标题(英):Vacuum distillation method of sponge titanium
- 申请号:CN201710934506.3 申请日:2017-10-10
- 公开(公告)号:CN107674999A 公开(公告)日:2018-02-09
- 发明人: 李开华 , 李亮 , 盛卓 , 苗庆东
- 申请人: 攀钢集团研究院有限公司
- 申请人地址: 四川省成都市高新区西部园区创新组团攀钢集团研究院有限公司
- 专利权人: 攀钢集团研究院有限公司
- 当前专利权人: 成都先进金属材料产业技术研究院股份有限公司
- 当前专利权人地址: 四川省成都市高新区西部园区创新组团攀钢集团研究院有限公司
- 代理机构: 成都虹桥专利事务所
- 代理人: 梁鑫
- 主分类号: C22B34/12
- IPC分类号: C22B34/12 ; C22B9/02
The invention belongs to the technical field of sponge titanium and particularly relates to a vacuum distillation method of sponge titanium. In order to solve the technical problems that the sponge titanium contains a plurality of impurities and is unstable in quality which are easily caused by the existing vacuum distillation method, the invention provides a vacuum distillation method of sponge titanium. The vacuum distillation method of sponge titanium comprises the following steps: a, putting the sponge titanium in a distillation electric furnace, vacuumizing and distilling, reducing the pressure in the electric furnace to 100Pa in 20-30 hours, then reducing the pressure in the furnace to 8-10Pa in 30-50 hours; b, continuously vacuumizing, reducing the pressure in the furnace from 8-10Pa to be less than 4Pa in 30-50 hours, keeping the pressure for 40-60 hours, and keeping the vacuum degree of the furnace at 8-10Pa for more than or equal to 90 hours. The method is capable of reducingthe content of the impurities in the sponge titanium, improving the quality of the sponge titanium, reducing the distillation time, reducing the energy consumption and reducing the production cost, and has important practical significance.
公开/授权文献:
- CN107674999B 海绵钛真空蒸馏的方法 公开/授权日:2019-10-01