![两步法醚化合成均三嗪类紫外线吸收剂UV-1577](/CN/2017/1/134/images/201710674201.jpg)
基本信息:
- 专利标题: 两步法醚化合成均三嗪类紫外线吸收剂UV-1577
- 专利标题(英):Two-step etherification synthesized s-triazine ultraviolet absorbent UV-1577
- 申请号:CN201710674201.3 申请日:2017-08-09
- 公开(公告)号:CN107382888A 公开(公告)日:2017-11-24
- 发明人: 刘威 , 刘恩德 , 韩建国 , 张海涛 , 许汉 , 吴成
- 申请人: 中昊(大连)化工研究设计院有限公司
- 申请人地址: 辽宁省大连市高新园区黄浦路201号
- 专利权人: 中昊(大连)化工研究设计院有限公司
- 当前专利权人: 中昊(大连)化工研究设计院有限公司
- 当前专利权人地址: 辽宁省大连市高新园区黄浦路201号
- 主分类号: C07D251/24
- IPC分类号: C07D251/24
The invention relates to a two-step etherification synthesized s-triazine ultraviolet absorbent UV-1577. The two-step etherification synthesized s-triazine ultraviolet absorbent UV-1577 is prepared by the following steps: utilizing a raw material (shown in the description) 2-(2,4-dihydroxyl)-benzo-4,6-diphenyl s-triazine and a raw material (shown in the description) alkali metal or alkali earth metal hydroxide to react in a water carrying agent at a specific temperature to obtain an intermediate product, removing, by steaming, the water carrying agent, cooling to room temperature, adding N,N-dimethyl formamide (DMF) to react with bromohexane at 70 DEG C to obtain the s-triazine ultraviolet absorbent UV-1577. The preparation method is divided into two steps, compared with the existing production process for synthesizing the UV-1577 in one step, the generation of inorganic salts is reduced, a high-temperature salt pressing link is eliminated, the unsafety factor of the operation by workers can be reduced, and the two-step etherification synthesized triazine ultraviolet absorvent UV-1577 has the characteristic of environmental friendliness, and has the advantaages of simple equipment, advanced technology, convenient operation, capability of cooperatively using a solvent, low cost and easy industrialized production, and the purity of a liquid phase is greater than 99.3 percent.
IPC结构图谱:
C | 化学;冶金 |
--C07 | 有机化学 |
----C07D | 杂环化合物 |
------C07D251/00 | 杂环化合物,含1,3,5-三嗪环 |
--------C07D251/02 | .不与其他环稠合 |
----------C07D251/12 | ..环原子间或环原子与非环原子间有3个双键 |
------------C07D251/14 | ...有氢或碳原子直接连在至少1个环碳原子上 |
--------------C07D251/24 | ....连在3个环碳原子上 |