基本信息:
- 专利标题： 一种微波合成辛酸‑癸酸甘油酯的方法
- 专利标题（英）：Method for microwave synthesis of glyceryl caprylate-caprate
- 申请号：CN201611257447.2 申请日：2016-12-30
- 公开(公告)号：CN106699555A 公开(公告)日：2017-05-24
- 发明人： 李建 , 孟巨光 , 郑成 , 莫林峰
- 申请人： 广州星业科技股份有限公司
- 申请人地址： 广东省广州市永和经济开发区沧海二路七号
- 专利权人： 广州星业科技股份有限公司
- 当前专利权人： 广州星业科技股份有限公司
- 当前专利权人地址： 广东省广州市永和经济开发区沧海二路七号
- 代理机构： 广东广信君达律师事务所
- 代理人： 杨晓松
- 主分类号： C07C67/08
- IPC分类号： C07C67/08 ; C07C69/30
The invention provides a preparation method for microwave synthesis of glyceryl caprylate-caprate. Caprylate-caprate and glycerin are reacted in the presence of a compound catalyst, and a glyceryl caprylate-caprate product is prepared by microwave synthesis. According to the method, the molar ratio of caprylate and caprate in the glyceryl caprylate-caprate is regulated, catalysis of the compound catalyst is combined, and a frequency band of 300 to 3,000MHz is adopted for microwave synthesis, so that the high-quality glyceryl caprylate-caprate of which the molar ratio of the caprylate and the caprate is controllable can be efficiently and rapidly prepared. According to the method, a high esterification rate can be achieved, and meanwhile, the energy consumption and the production cost of a reaction process can be remarkably reduced.