
基本信息:
- 专利标题: 一种用纺织碱溶废水处理后的白泥和涤纶废旧丝布降解后的粗PTA精制对苯二甲酸的方法
- 专利标题(英):Method of purifying pure terephthalic acid (PTA) by means of white mud after treatment of textile alkali dissolution waste water and crude terephthalic acid after degradation of waste Dacron silk cloth
- 申请号:CN201611059709.4 申请日:2016-11-28
- 公开(公告)号:CN106588638A 公开(公告)日:2017-04-26
- 发明人: 钱胜文 , 张彩华 , 钱建林 , 黄云志
- 申请人: 钱胜文
- 申请人地址: 江西省萍乡市芦溪县芦溪镇新田村新岗下72号
- 专利权人: 钱胜文
- 当前专利权人: 钱胜文
- 当前专利权人地址: 江西省萍乡市芦溪县芦溪镇新田村新岗下72号
- 代理机构: 萍乡益源专利事务所
- 代理人: 胡宜斌
- 主分类号: C07C51/50
- IPC分类号: C07C51/50 ; C07C51/43 ; C07C51/42 ; C07C63/26
The invention discloses a method of purifying pure terephthalic acid (PTA) by means of white mud after treatment of textile alkali dissolution waste water and crude terephthalic acid after degradation of waste Dacron silk cloth. The method includes the steps of: 1) integration of material addition, slurry blending and pre-heating: adding industrial reclaimed water or fresh industrial water accounting for 75-80% of total weight of raw materials into a slurry blending kettle, starting stirring and successively adding raw materials as well as high temperature activated carbon, a descaling agent, and a composite finishing additive, and feeding high-temperature reclaimed vapor after pressure reduced crystallization or temperature reduced crystallization to dissolve the raw materials and heat the raw materials to 150-180 DEG C to prepare slurry; 2) starting a tubular heater to heat the raw materials, and performing high-temperature and high-pressure filtration, pressure reduced crystallization, cooling and dehydration; and 3) wastewater treatment: neutralizing wastewater by lime, flocculating and discoloring the wastewater by a water purifying agent, and filtering the wastewater to remove residues, so that the purified industrial water can be applied in the material addition and slurry blending step. The method accelerates dissolution and filtration and saves energy cost and changes production from intermittent type into continuous type, thus improving production efficiency. The method has beneficial to balance of production processes, and reduces man-hour cost.
公开/授权文献:
- CN106588638B 一种用纺织碱溶废水处理后的白泥和涤纶废旧丝布降解后的粗PTA精制对苯二甲酸的方法 公开/授权日:2018-12-07
IPC结构图谱:
C | 化学;冶金 |
--C07 | 有机化学 |
----C07C | 无环或碳环化合物 |
------C07C51/00 | 羧酸或它们的盐、卤化物或酐的制备 |
--------C07C51/42 | .分离;纯化;稳定化;添加剂的使用 |
----------C07C51/50 | ..使用添加剂,例如,用于稳定化 |