![一种除草剂原药的合成方法](/CN/2016/1/155/images/201610778663.jpg)
基本信息:
- 专利标题: 一种除草剂原药的合成方法
- 专利标题(英):Method for synthesizing herbicide raw medicine
- 申请号:CN201610778663.5 申请日:2016-08-30
- 公开(公告)号:CN106496076A 公开(公告)日:2017-03-15
- 发明人: 李建新
- 申请人: 枣阳市先飞高科农药有限公司
- 申请人地址: 湖北省襄樊市枣阳市寺沙路813号
- 专利权人: 枣阳市先飞高科农药有限公司
- 当前专利权人: 枣阳市先飞高科农药有限公司
- 当前专利权人地址: 湖北省襄樊市枣阳市寺沙路813号
- 代理机构: 上海精晟知识产权代理有限公司
- 代理人: 冯子玲
- 主分类号: C07C303/22
- IPC分类号: C07C303/22 ; C07C309/48
The invention discloses a method for synthesizing a herbicide raw medicine, and relates to the pesticide production field. The method includes six technological processes of raw material preparation, reaction kettle mixing preheating, solution neutralizing treatment, sulfonation reaction, amination reaction and washing layering treatment; with use of the sulfonation reaction of 2,6-dinitro p-tert chlorobenzene and sodium pyrosulfite and the amination reaction of 2,6-dinitro p-tert chlorobenzene and sec-butylamine, the herbicide raw medicine with relatively high purity can be prepared; moreover, with multiple use of clear water for washing, the production process is simple and reliable, recrystallization is not needed, the high-purity product can be obtained, the yield and the product purity are high, an efficient herbicide product can be obtained, and the method is worthy of promotion.
IPC结构图谱:
C | 化学;冶金 |
--C07 | 有机化学 |
----C07C | 无环或碳环化合物 |
------C07C303/00 | 硫酸酯或硫酸酰胺的制备;磺酸或其酯、卤化物、酐或酰胺的制备 |
--------C07C303/02 | .磺酸或其卤化物的 |
----------C07C303/22 | ..由磺酸经不涉及形成磺基或卤代磺酰基的反应 |