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基本信息:
- 专利标题: 一种磺化缩聚改性腐植酸水煤浆分散剂的制备方法
- 专利标题(英):Method for preparing sulfonation condensation polymerization modified humic acid water-coal-slurry dispersing agent
- 申请号:CN201410161163.8 申请日:2014-04-18
- 公开(公告)号:CN103951836A 公开(公告)日:2014-07-30
- 发明人: 张光华 , 朱妞 , 卫颖菲 , 李俊国 , 朱军锋 , 牛育华
- 申请人: 陕西科技大学
- 申请人地址: 陕西省西安市未央区大学园1号
- 专利权人: 陕西科技大学
- 当前专利权人: 陕西科技大学
- 当前专利权人地址: 陕西省西安市未央区大学园1号
- 代理机构: 西安通大专利代理有限责任公司
- 代理人: 蔡和平
- 主分类号: C08H99/00
- IPC分类号: C08H99/00 ; C07G99/00 ; C10L1/32
The invention discloses a method for preparing a sulfonation condensation polymerization modified humic acid water-coal-slurry dispersing agent. The method comprises the following steps: stirring to dissolve humic acid and urea in water, adding an alkali adjusting agent, further adding a sulfonating agent, heating to 50-55 DEG C, starting dropping a mixture solution of acetone and formaldehyde, controlling the temperature at 55-60 DEG C, stopping adding within about 1-1.5 hours, further heating to 70-80 DEG C, reacting for 1-2 hours at constant temperature, continuously heating to 95-110 DEG C, performing polymerization reaction for 2-3 hours, subsequently cooling and discharging a material, drying and crushing the material so as to obtain a sepia solid powder product. The dispersing agent is a humic acid series water-coal-slurry dispersing agent which contains groups of sulfonyl, carboxyl, hydroxyl, methyl and the like, on the basis that the good dispersity of the humic acid dispersing agent is maintained, the stability is improved, the method disclosed by the invention is simple, the raw materials are easily available, the reaction condition is gentle, and a product can be used for well solving the problem that the stability is poor when the humic acid is used as the water-coal-slurry dispersing agent.
公开/授权文献:
- CN103951836B 一种磺化缩聚改性腐植酸水煤浆分散剂的制备方法 公开/授权日:2016-01-20
IPC结构图谱:
C | 化学;冶金 |
--C08 | 有机高分子化合物;其制备或化学加工;以其为基料的组合物 |
----C08H | 天然高分子化合物的衍生物 |
------C08H99/00 | 本小类其他各组中不包括的技术主题 |