
基本信息:
- 专利标题: 黑檀醇制备方法
- 专利标题(英):Ebanol preparation method
- 申请号:CN201310470822.1 申请日:2013-10-10
- 公开(公告)号:CN103483151A 公开(公告)日:2014-01-01
- 发明人: 张忠富 , 崔荣贵 , 张琦
- 申请人: 浦城县永芳香料科技有限公司
- 申请人地址: 福建省南平市浦城县南浦生态工业园区5号
- 专利权人: 浦城县永芳香料科技有限公司
- 当前专利权人: 浦城县永芳香料科技有限公司
- 当前专利权人地址: 福建省南平市浦城县南浦生态工业园区5号
- 代理机构: 深圳市合道英联专利事务所
- 代理人: 廉红果
- 主分类号: C07C33/12
- IPC分类号: C07C33/12 ; C07C29/143
The invention aims to provide an ebanol preparation method having the advantages of industrialized production realization, simple operation and strong reliability. The method comprises the following steps: 1, condensing methyl ethyl ketone and trimethyl cyclopentenyl acetaldehyde at a low temperature, carrying out rectification, removing methyl ethyl ketone and methanol, cooling a residual liquid, rectifying the obtained separated organic phase to obtain an intermediate 1, adding the intermediate 1 to a -5-0DEG C dimethyl formamide solution of sodium methoxide, rearranging to obtain an intermediate 2, adding the obtained methanol solution of the intermediate 2 to a methanol solution of sodium borohydride for a reaction, carrying out hydrogenation reduction, and rectifying the obtained organic phase to obtain ebanol, wherein a mole ratio of the added trimethyl cyclopentenyl acetaldehyde to methyl ethyl ketone contained in a first solution is less than 1.
公开/授权文献:
- CN103483151B 黑檀醇制备方法 公开/授权日:2015-04-08