基本信息:
- 专利标题： 煤液化油中碱性氮化合物的分离方法
- 专利标题（英）：Separation method for alkali nitrogen compounds in coal liquefaction oil
- 申请号：CN201310329826.8 申请日：2013-07-31
- 公开(公告)号：CN103396827A 公开(公告)日：2013-11-20
- 发明人： 姜元博 , 李克健 , 高山松 , 李延红 , 杨葛灵 , 章序文 , 李永伦 , 向春兰
- 申请人： 神华集团有限责任公司 , 中国神华煤制油化工有限公司 , 中国神华煤制油化工有限公司上海研究院
- 申请人地址： 北京市东城区安定门西滨河路22号神华大厦
- 专利权人： 神华集团有限责任公司,中国神华煤制油化工有限公司,中国神华煤制油化工有限公司上海研究院
- 当前专利权人： 神华集团有限责任公司,中国神华煤制油化工有限公司,中国神华煤制油化工有限公司上海研究院
- 当前专利权人地址： 北京市东城区安定门西滨河路22号神华大厦
- 代理机构： 北京康信知识产权代理有限责任公司
- 代理人： 吴贵明; 张永明
- 主分类号： C10G17/06
- IPC分类号： C10G17/06 ; C10G17/07 ; C10G53/10
The invention discloses a separation method for alkali nitrogen compounds in coal liquefaction oil. The separation method comprises the following steps of: acid pickling: mixing the coal liquefaction oil with an acidic solution, carrying out vibrating, standing and layering, and separating to obtain a water phase solution; and organic solvent extraction: regulating the pH value of the water phase solution to be 8-10, adding organic solvents after cooling, carrying out mixing, vibrating, standing and layering, and separating to obtain an organic phase solution rich in the alkali nitrogen compounds. By utilizing the separation method disclosed by the invention, the alkali nitrogen compounds in the coal liquefaction oil are processed by utilizing an acid pickling method and an organic solvent extraction method, the effects that the alkali nitrogen compounds in the coal liquefaction oil are good in separation selectivity and high in separation degree and are thoroughly extracted are achieved, and the obtained organic phase solution can be directly used for carrying out sample injection analysis on the alkali nitrogen compounds.
公开/授权文献:
- CN103396827B 煤液化油中碱性氮化合物的分离方法 公开/授权日：2015-12-09