![碳酸氢钠结晶制取设备和利用该设备制取碳酸氢钠结晶的工艺方法](/CN/2013/1/48/images/201310243609.jpg)
基本信息:
- 专利标题: 碳酸氢钠结晶制取设备和利用该设备制取碳酸氢钠结晶的工艺方法
- 专利标题(英):Sodium bicarbonate crystal preparation equipment and process for preparing sodium bicarbonate crystals by utilizing same
- 申请号:CN201310243609.7 申请日:2013-06-19
- 公开(公告)号:CN103303946A 公开(公告)日:2013-09-18
- 发明人: 张建伟 , 牛新平 , 吴利彦 , 刘晓春 , 史永良 , 马文锁 , 刘晓文 , 成东江 , 王荣魁 , 王东 , 康勤阁 , 胡志肖
- 申请人: 石家庄天人化工设备集团有限公司
- 申请人地址: 河北省石家庄市藁城市工业东路004号
- 专利权人: 石家庄天人化工设备集团有限公司
- 当前专利权人: 石家庄天人化工设备集团有限公司
- 当前专利权人地址: 河北省石家庄市藁城市工业东路004号
- 代理机构: 石家庄国域专利商标事务所有限公司
- 代理人: 胡澎
- 主分类号: C01D7/38
- IPC分类号: C01D7/38
The invention discloses sodium bicarbonate crystal preparation equipment and a process for preparing sodium bicarbonate crystals by utilizing the same. The equipment comprises a carbonizer, wherein a tail gas absorption section is arranged at the top of the carbonizer; the part (below the tail gas absorption section) is divided into a first reaction zone, a second reaction zone and a third reaction zone in sequence; and a plurality of ring-shaped tower plates are arranged in each reaction zone. The process is characterized by comprising the following steps: firstly carrying out first-step carbonization and crystallization, then carrying out crystal-slurry separation on reaction solution and enabling the product to leave from the carbonizer and pass through an ammoniating apparatus for ammoniating so that sodium bicarbonate enters an unsaturated zone; then cooling with water and finally sending sodium bicarbonate back to the carbonizer for further carbonization and crystallization. Therefore, the problem of water cooler scabbing is solved, no standby coolers are needed for alternate operation, the prepared sodium bicarbonate crystals have good crystal form, big particles and low moisture content and the energy consumption of the subsequent calcining procedure is also obviously reduced.
公开/授权文献:
- CN103303946B 碳酸氢钠结晶制取设备和利用该设备制取碳酸氢钠结晶的工艺方法 公开/授权日:2015-02-04
IPC结构图谱:
C | 化学;冶金 |
--C01 | 无机化学 |
----C01D | 碱金属,即锂、钠、钾、铷、铯或钫的化合物 |
------C01D7/00 | 钠、钾或一般碱金属的碳酸盐 |
--------C01D7/38 | .制备粒状、片状或其他形状的产品 |