![一种以微波水热法制备氟化石墨烯的方法](/CN/2013/1/34/images/201310172936.jpg)
基本信息:
- 专利标题: 一种以微波水热法制备氟化石墨烯的方法
- 专利标题(英):Method for preparing fluorinated graphene through microwave hydrothermal method
- 申请号:CN201310172936.8 申请日:2013-05-10
- 公开(公告)号:CN103288069A 公开(公告)日:2013-09-11
- 发明人: 李贺军 , 罗慧娟 , 付前刚 , 沈庆凉
- 申请人: 西北工业大学
- 申请人地址: 陕西省西安市友谊西路127号
- 专利权人: 西北工业大学
- 当前专利权人: 西北工业大学
- 当前专利权人地址: 陕西省西安市友谊西路127号
- 代理机构: 西北工业大学专利中心
- 代理人: 王鲜凯
- 主分类号: C01B31/00
- IPC分类号: C01B31/00
The invention provides a method for preparing fluorinated graphene through a microwave hydrothermal method. The fluorinated graphene is prepared by employing the microwave hydrothermal method and is rapidly heated by utilizing the change of the electric field and magnetic field in the space, the low-temperature (150-200 DEG C) temperature is realized, the reaction time (30-60 minutes) is greatly shortened, the energy consumption is reduced, and the preparation efficiency is improved. The adopted preparation method does not have temperature gradient in the reaction process, a hysteresis effect is avoided, and the reaction process is easy to control and fewer in influence factors; and the prepared fluorinated graphene is uniform in fluorine doping and high in experimental repeatability. The process conditions such as raw material ratio, reaction temperature and reaction time are adjusted, and the fluorinated graphene of different fluorine contents can be prepared. The prepared fluorinated graphene is high in yield, and the yield is up to 90-95 percent. The preparation method is easily popularized and applied.