![带环氧基苯并恶嗪玻璃纤维布层压板的制备方法](/CN/2013/1/22/images/201310111116.jpg)
基本信息:
- 专利标题: 带环氧基苯并恶嗪玻璃纤维布层压板的制备方法
- 专利标题(英):Preparation method of glass fiber cloth laminate with epoxide-group benzoxazine
- 申请号:CN201310111116.8 申请日:2013-04-01
- 公开(公告)号:CN103223762A 公开(公告)日:2013-07-31
- 发明人: 李建学 , 黄洪驰 , 马庆柯 , 李先德 , 彭晓伟 , 杜旻
- 申请人: 四川东材科技集团股份有限公司
- 申请人地址: 四川省绵阳市游仙区三星路188号
- 专利权人: 四川东材科技集团股份有限公司
- 当前专利权人: 四川东材科技集团股份有限公司
- 当前专利权人地址: 四川省绵阳市游仙区三星路188号
- 代理机构: 成都蓉信三星专利事务所
- 代理人: 刘克勤
- 主分类号: B32B37/10
- IPC分类号: B32B37/10 ; B32B37/06 ; B32B27/04 ; B32B17/04 ; B32B15/20 ; C08L79/04 ; C08L61/06 ; C08K5/5399 ; C08G73/06
The invention discloses a preparation method of a glass fiber cloth laminate with epoxide-group benzoxazine. The method is characterized by adding amine compounds, a solvent and an aqueous formaldehyde solution into a reactor, reacting with stirring for 1 hour, adding phenolic compounds, reacting for 3 hours under reflux, adding a catalyst and di-salt hydrogen phosphate, adding an aqueous hydrogen peroxide solution with stirring, reacting for 6-8 hours under 55-70 DEG C, cooling, standing, separating an upper organic phase as a benzoxazine resin solution with the epoxy group, putting the benzoxazine resin solution with the epoxy group, thermoplastic phenolic resin and a solvent into a glue preparing tank, stirring under 20-60 DEG C, adding anilino cyclic phosphazene and a promoter, stirring to prepare a resin glue solution, and performing coating and thermoforming for glass fiber cloth to prepare the glass fiber cloth laminate. The prepared laminate can be used for producing electrical glass fiber cloth laminates, or copper clad laminate substrate, or laminated and molded composite materials for other uses, and is good in performance.
公开/授权文献:
- CN103223762B 带环氧基苯并恶嗪玻璃纤维布层压板的制备方法 公开/授权日:2016-01-20
IPC结构图谱:
B | 作业;运输 |
--B32 | 层状产品 |
----B32B | 层状产品,即由扁平的或非扁平的薄层,例如泡沫状的、蜂窝状的薄层构成的产品 |
------B32B37/00 | 用于层压的方法和装置,例如,通过固化或通过超声黏接 |
--------B32B37/10 | .以压制技术为特征,例如,使用真空或流体压力的直接作用 |