![在四氯化钛制造中通过钛产品中的二氧化硅含量监控利用反馈响应和前馈响应来控制载钛材料流量](/CN/2010/8/9/images/201080049698.jpg)
基本信息:
- 专利标题: 在四氯化钛制造中通过钛产品中的二氧化硅含量监控利用反馈响应和前馈响应来控制载钛材料流量
- 专利标题(英):Titanium Bearing Material Flow Control In The Manufacture Of Titanium Tetrachloride With Silica Content Monitoring Of The Titanium Product Using Feedback And Feed Forward Responses
- 申请号:CN201080049698.6 申请日:2010-09-02
- 公开(公告)号:CN102812095A 公开(公告)日:2012-12-05
- 发明人: J·E·小默克尔 , R·R·小比茨
- 申请人: 纳幕尔杜邦公司
- 申请人地址: 美国特拉华州
- 专利权人: 纳幕尔杜邦公司
- 当前专利权人: 科慕FC有限公司
- 当前专利权人地址: 美国特拉华州
- 代理机构: 中国专利代理(香港)有限公司
- 代理人: 王伦伟; 李炳爱
- 优先权: 61/239,579 2009.09.03 US
- 国际申请: PCT/US2010/047630 2010.09.02
- 国际公布: WO2011/028871 EN 2011.03.10
- 进入国家日期: 2012-05-02
- 主分类号: C09C1/36
- IPC分类号: C09C1/36 ; C01G23/02 ; C01G23/047 ; C01G23/07 ; C22B34/12
This disclosure relates to a process for controlling chlorination reactions in manufacturing titanium tetrachloride in a fluidized bed reactor, followed by processing to form a titanium product comprising an amount of silica, the process comprising: (a) feeding carbonaceous material, titanium bearing material comprising an amount of silica, and chlorine to the fluidized bed reactor to form a gaseous stream, and condensing the gaseous stream to form titanium tetrachloride, a non-condensed gas stream and a condensable product stream; (b) processing the titanium tetrachloride to form a titanium product comprising an amount of silica; (c) analyzing the titanium product comprising an amount of silica to determine the analyzed concentration of silica; (d) identifying a set point concentration of silica; (e) calculating the difference between the analyzed concentration of silica and the set point concentration of silica; (f) measuring the titanium tetrachloride flow to a processing reactor that releases chlorine; (g) measuring the flow of fresh chlorine added to the fluidized bed; (h) measuring the flow of the titanium bearing material added to the fluidized bed reactor and establishing a historic average flow of the titanium bearing material added to the fluidized bed reactor; (i) calculating the chlorine released from the titanium tetrachloride that is processed using the titanium tetrachloride flow data from step (f); (j) calculating the total chlorine flow to the fluidized bed reactor by adding the chlorine flow in step (g) to the chlorine flow calculated in step (i) and establishing a historic average chlorine flow; (k) calculating a unit titanium bearing material consumption per unit chlorine; (l) calculating an estimated current consumption rate of titanium bearing material based on the total chlorine flow from step (j) times the unit titanium bearing material consumption per unit chlorine from step (k).
公开/授权文献:
- CN102812095B 在四氯化钛制造中通过钛产品中的二氧化硅含量监控利用反馈响应和前馈响应来控制载钛材料流量 公开/授权日:2014-08-13
IPC结构图谱:
C | 化学;冶金 |
--C09 | 染料;涂料;抛光剂;天然树脂;黏合剂;其他类目不包含的组合物;其他类目不包含的材料的应用 |
----C09C | 纤维状填料以外的无机材料的处理以增强它们的着色或填充性能;炭黑的制备 |
------C09C1/00 | 纤维状填料以外的特殊无机材料的处理;炭黑的制备 |
--------C09C1/36 | .钛的化合物 |