![改性十二胺固化剂及其制备方法和应用](/CN/2012/1/25/images/201210129951.jpg)
基本信息:
- 专利标题: 改性十二胺固化剂及其制备方法和应用
- 专利标题(英):Modified lauryl amine hardener, manufacturing method and application of modified lauryl amine hardener
- 申请号:CN201210129951.X 申请日:2012-04-28
- 公开(公告)号:CN102633988A 公开(公告)日:2012-08-15
- 发明人: 黄齐茂 , 苏志雄 , 潘志权 , 李露露
- 申请人: 武汉工程大学
- 申请人地址: 湖北省武汉市洪山区雄楚大街693号
- 专利权人: 武汉工程大学
- 当前专利权人: 武汉工程大学
- 当前专利权人地址: 湖北省武汉市洪山区雄楚大街693号
- 代理机构: 湖北武汉永嘉专利代理有限公司
- 代理人: 崔友明
- 主分类号: C08G59/50
- IPC分类号: C08G59/50 ; C08G18/38 ; C07C251/08 ; C07C249/02 ; C09K8/56 ; C09D175/04 ; C09D7/12 ; C09D5/00 ; C09D163/00 ; C09J175/04 ; C09J11/06 ; C09J163/00
The invention relates to a modified lauryl amine hardener and a manufacturing method and application of the modified lauryl amine hardener. The structural formula of the modified lauryl amine hardener is shown in the description. The manufacturing method of the modified lauryl amine hardener comprises the following steps: (1) adding lauryl amine and methyl isobutyl ketone (MIBK) in molar ratio of 1:1.2-2 in a four-opening flask with a stirring device, a thermometer and a water segregator; (2) stirring, leading counterflow of reaction to start to appear after heating temperature from common temperature to 71-75 DEG C, carrying over generated water by the MIBK with the performance of the reaction, achieving reaction end after gradually heating to 118-121 DEG C and reacting to that fact that water isn't generated any more; and (3) decreasing the temperature to 70-80 DEG C, obtaining excessive MIBK for recycle through reduced pressure distillation, and finally obtaining a modified lauryl amine hardener product. The modified lauryl amine hardener can be applied as a treating agent for solidification in the field of oil field sand prevention and can be manufactured to be a polyurethane waterproofing paint.
公开/授权文献:
- CN102633988B 改性十二胺固化剂及其制备方法和应用 公开/授权日:2014-03-26
IPC结构图谱:
C | 化学;冶金 |
--C08 | 有机高分子化合物;其制备或化学加工;以其为基料的组合物 |
----C08G | 用碳—碳不饱和键以外的反应得到的高分子化合物 |
------C08G59/00 | 每个分子含有1个以上环氧基的缩聚物;环氧缩聚物与单官能团低分子量化合物反应得到的高分子;每个分子含有1个以上环氧基的化合物使用与该环氧基反应的固化剂或催化剂聚合得到的高分子 |
--------C08G59/02 | .每分子含有1个以上环氧基的缩聚物 |
----------C08G59/20 | ..以使用的环氧化合物为特征 |
------------C08G59/50 | ...胺 |